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Model 200E Instruction Manual
EPA Protocol Calibration
8.6. Summary of Quality Assurance Checks
The following items should be checked on a regularly scheduled basis to assure high quality
data from the M200E. See Table 8-4 for a summary of activities; also the QA Handbook should
be checked for specific procedures.
Table 8-4: Activity Matrix for Data Quality
Characteristic
Acceptance Limits
Frequency and Method
of Measurement
Action if Requirements
are not Met
Shelter
temperature
Mean temperature between
22
°
C and 28
°
C (72
°
and
82
°
F), daily fluctuations not
greater than
±
2
°
C
Check thermograph chart
weekly for variations
greater than ± 2
°
C (4
°
F)
Mark strip chart for the
affected time period
Repair or adjust
temperature control
Sample
introduction
system
No moisture, foreign material,
leaks, obstructions; sample
line connected to manifold
Weekly visual inspection
Clean, repair, or replace
as needed
Recorder
Adequate ink & paper
Legible ink traces
Correct chart speed and range
Correct time
Weekly visual inspection
Replenish ink and paper
supply
Adjust time to agree
with clock; note on chart
Analyzer
operational
settings
TEST measurements at
nominal values
M200E in SAMPLE mode
Weekly visual inspection
Adjust or repair as
needed
Analyzer
operational
check
Zero and span within tolerance
limits as described in
Section 12 of the Q.A.
Handbook
6
Level 1 zero/span every
2 weeks; Level 2 between
Level 1 checks at
frequency desired by user
Find source of error and
repair
After corrective action,
re-calibrate analyzer
Precision check Assess precision as described
in Sections 15&18 of the Q.A.
Handbook
6
Every 2 weeks, Subsec.
3.4.3 (Ibid.)
Calc, report precision,
Section 12 of the Q.A.
Handbook
6
8.7. Short Calibration Checks
A system of Level 1 and Level 2 zero/span checks (Table 8-3) is recommended. These checks
must be conducted in accordance with the specific guidance given in Section 12 of the Q.A.
Handbook
6
. Level 1 zero and span checks must be conducted every two weeks. Level 2 checks
should be conducted in between the Level 1 checks at a frequency desired by the user. Span
concentrations for both levels should be between 70 and 90% of the measurement range.
Zero and span data are to be used to:
•
Provide data to allow analyzer adjustment for zero and span drift;
•
Provide a decision point on when to calibrate the analyzer;
•
Provide a decision point on invalidation of monitoring data.
These items are described in detail in Sections 15&18 of the Q.A. Handbook
6
. Refer to
Chapter 11 of this manual if the instrument is not within the allowed margins. We recommend
to use APICOM and the iDAS for analysis and documentation of zero/span check data.
044100102 Rev A
137
Summary of Contents for 200E
Page 15: ...M200E Documentation Model 200E Instruction Manual USER NOTES xiv 044100102 Rev A ...
Page 19: ...M200E Documentation Model 200E Instruction Manual USER NOTES 4 044100102 Rev A ...
Page 141: ...Calibration Procedures Model 200E Instruction Manual USER NOTES 126 044100102 Rev A ...
Page 203: ...Theory of Operation Model 200E Instruction Manual USER NOTES 188 044100102 Rev A ...
Page 239: ...Troubleshooting Repair Model 200E Instruction Manual USER NOTES 224 044100102 Rev A ...
Page 265: ...APPENDIX A Model 200E Instruction Manual USER NOTES 250 044100110 Rev A ...
Page 271: ...APPENDIX B Model 200E Instruction Manual USER NOTES 256 044100120 Rev A ...
Page 275: ...APPENDIX D Model 200E Instruction Manual 260 044100141 Rev A USER NOTES ...