Seres OL TOC User And Maintenance Manual Download Page 60

 

TOC EVOLUTION: 

USER &  

MAINTENANCE MANUAL 

Page: 

60/74

 

Instructions No.: 10844        

 

 

This document is the property of SERES and cannot be reproduced without authorization

 

 
Example: If the measurement cycle is 5min and you want to set a calibration per month, you will need to enter 
8640 (12cycles * 24H * 30jrs). So the automatic Calibration cycle will perform after 8640 measurement cycles. 

11.2.5

 

 Reagent change 

 

To  change  the  reagent  containers,  wear  appropriate  protection  (gloves,  goggles  and  protective 
clothing). 

 

 

Entirely  replace  the  vials: 

Avoid  "repotting"

  which  can  always  generate  a  contamination  or 

dilution risk. 

 

Insert  the  reagent  pipes  down  to  the  bottom  of  each  reagent  container.  Ensure  that  the  reagent 
container has an air intake (a small opening on the cap is sufficient).

 

 

Check that the sample (or neutral water depending on the configuration) is present at the analyser 
inlet: it is necessary to fill the reactor during the reagent priming phase. 

 

Stop the cycle in progress by pressing Stop

 

Access the Tools tab. 

 

Enter the authorised user code 

 

Access the Electrical test menu

 

 

Press ON to run the pumps and OFF when the priming phase is completed. 

It is necessary to recalibrate after every reagent change.

 

11.2.6

 

   Replacing the pump pipes 

 

Description of the pump pipes 

According to the application, there are several types of pipes: 

0.8mm inner 

Ø

 type 

1.6-mm inner 

Ø

 type. 

The pump piping is usually made of "PHARMED ®", a material resistant to all chemicals except acetic 
acid, solvents and alcohols. 

 

Replacing a SERES peristaltic pump pipe (for reagents) 

The pump pipes are to be changed every three months. 

 

Important before replacing the pump pipes: 

o

 

Before changing a pump pipe, it is preferable to empty it (and/or rinse it with 
demineralised water) to avoid any chemical spraying risk.  

To do so, launch a priming operation with the reagent pipe from the flask or by 

suctioning the demineralised water.  

o

 

Wear appropriate protection (gloves, goggles, protective clothing) as the pipes may still 
contain traces of chemicals. 

Summary of Contents for TOC

Page 1: ...This document is the property of SERES and cannot be reproduced without authorization User and Maintenance Manual TOC Online analyzer for TOC monitoring in water N 10844_revS...

Page 2: ...lime and activated carbon cartridges removal procedure part 11 2 10 BOUTRELLE Julien GOZZI Marc 08 2017 I Without Persulfate deleted DALIA Nicolas GOZZI Marc 09 2017 J UPDATE Drawing DALIA Nicolas GOZ...

Page 3: ...13 6 4 APPLICATION _______________________________________________________________________________ 13 6 5 REAGENTS _________________________________________________________________________________ 13...

Page 4: ...________________________________________48 10 USER MANUAL _______________________________________________________________________________ 50 10 1 PRELIMINARY START UP _________________________________...

Page 5: ...________________________69 11 3 9 Replacing the mass controller ________________________________________________________________________70 11 3 10 Replacing the Air filter_____________________________...

Page 6: ...ed with the equipment can be affected Any spare part has to be replaced exclusively by a qualified person using only the parts specified by the manufacturer It is always recommended that all power sup...

Page 7: ...lectrical hazard IEC 60417 No 6040 Ultraviolet radiation instructional safeguard 3 4 After Sale Service Contact After Sale Service Lagreze Johnny Tel 04 42 97 37 91 psav seres ol com Spare parts Sauri...

Page 8: ...ion access or User W Possible Actions Consulting the measure in process Stop of the measure in process access to the settings menu Thresholds Setting 4 20mA outputs Once the access code is entered if...

Page 9: ...nnot be reproduced without authorization 4 Unpacking book 4 1 Precaution Position the box corectly Up Down Unpack carefully the analyser Check the analyzer for damage o If the device seems to be damag...

Page 10: ...Page 10 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization SECTION 1 EQUIPMENT FILE 5 INTRODUCTION 6 MEASURING PRINCIPLE 7 TECHNICAL SPECIFI...

Page 11: ...nored and the TOC analysis often requires determining each of these forms TOC The TOC EVOLUTION analyser from SERES is designed for determining these different carbonated compounds Non Purgeable Organ...

Page 12: ...essary The sample and filter line is cleaned either by using the Black Cleaning technique counter current cleaning or with compressed air on a case by case basis 6 1 2 Removal of mineral carbon The sa...

Page 13: ...ndustrial sites 0 1 to 5 10 mg l Production of demineralised water for general and chemical uses Condensate waters from vapour production systems Medium Pressure or Very High Pressure systems in therm...

Page 14: ...e characteristic values of the method are expressed as a percentage on Full scale Measuring system NDIR Measuring range Low range configuration 0 2 ppm Limit of Detection 0 01 ppm Repeatability 2 FS A...

Page 15: ...ibration on TOC Phtalate Calibration on TOC End Step 2 may not be implemented in the device depending on the configuration Only for ranges 20ppm The Manual measure on TIC and Zero measure may not be p...

Page 16: ...ing cycle The measuring cycle is included in a 5 to 10 min interval but it also depends on the type of sample used program derivative function and on the parameters being measured Name Reference Valid...

Page 17: ...UTION USER MAINTENANCE MANUAL Page 17 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization 6 9 Hydraulic diagrams Figure 1 Hydraulic diagram 1...

Page 18: ...TOC EVOLUTION USER MAINTENANCE MANUAL Page 18 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization Figure 2 Multi Channel Hydraulic diagram...

Page 19: ...according to the range but it also depends on the nature of the sample and on the type of measurement The spacing between the measurements can be adjusted 7 2 3 Standard dimensions Casing l x h x d 9...

Page 20: ...acuation The gas shall be evacuated into free outside air For Cleaning the Sample Collecting Treatment System Pressure 7 bar maximum Adjustment at 2 5 bar pressure reducer 7 2 8 Electrical connections...

Page 21: ...the top part accommodates the electronic system external communication display and the bottom part the hydraulic system The useful information is displayed via a touch screen located at the front whos...

Page 22: ...C EVOLUTION USER MAINTENANCE MANUAL Page 22 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization Figure 3 General dimensional drawing 1 channe...

Page 23: ...ON USER MAINTENANCE MANUAL Page 23 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization Figure 4 General dimensional drawing Multi channel con...

Page 24: ...is a sampling system when the sample inlet is pressurised The client connects the sample inlet this sample circulates inside the loop and flows in free air via a pan The sample is collected in the dir...

Page 25: ...ried out on the entire system which is protected by the protective cover on which are stuck the safety labels UV and Temperature 8 2 5 The Condenser This system is used to recover the condensation dro...

Page 26: ...pression of a pipe with a medium flowrate enabling the collection of the sample Metering peristaltic pumps SERES low flowrate for the injection of reagents They are volumetric pumps 8 2 9 Air flow rat...

Page 27: ...parts One contains activated carbon and the other soda lime This allows the elimination of CO2 and to have a high quality air carrier A desiccant cartridge is placed upstream of this cartridge Humidi...

Page 28: ...e power supply The entire system is supplied with a switching mode power supply with the following characteristics Input voltage range 100V 230V AC Frequency 50 60hz Output voltage 24 V 13A 300W Prote...

Page 29: ...n This board is directly connected to the power supply observed previously It communicates with the PLC board through an Ethernet connection via an Ethernet Switch 8 2 15 2 The functionalities Figure...

Page 30: ...d by the term 4 20mA 6 digital outputs identified by the terms RELAYS and OUTPUTS VOLTAGE and distributed as follows o 4 Output Relays 24V Dry Contacts at 1A max for information on the status of the m...

Page 31: ...ame Function Analogue Outp ut 2 4 20mA 1 4 20mA Digital 4 20mA 1 4 20mA Digital Channel 2 Measurement 0 24V 1 RELAY 1 2 D C Reserved Threshold 1 RELAY 1 2 D C Reserved Threshold 1 Channel 2 1 RELAY 2...

Page 32: ...exceeding the threshold Multi channel configuration The corresponding threshold 1 overrun channel 2 output is accessible on pins 1 2 3 of connector X3 of board W1128007 as a dry contact relay output...

Page 33: ...channel 2 information is accessible on pins 10 11 12 of connector X3 of board W1128007 as a dry contact 8 2 16 3 6 Wiring of the end of cycle shutdown channel input option INPUT 2 This input is used...

Page 34: ...nel data Calculated data and measurement parameters such as the thresholds and range 8 Measured concentrations Concentration measured per channel 9 Channel in progress Number of the channel in progres...

Page 35: ...Log file copy To load the Log files onto a USB key in order to read the data recorded by the analyser Electrical tests Access to the pumps actuator as EV lamp heating relay 4 20 mA parameter History...

Page 36: ...hannel x tab where we find The command activating or not the channel A light indicating whether the cycle is running A warning light relating to the water fault in channel x Two indicator lights relat...

Page 37: ...ble it In order to enable the Sample peristaltic pump o Press ON to enable the pump or OFF to disable it Sample pump command 8 3 3 1 2 Relay tab In order to test a relay o Press the Relay tab o Press...

Page 38: ...ab o Press ON to enable or OFF to disable 8 3 3 1 4 Actuator tab In order to control the UV lamp heating compressor o Press the Actuator tab o Press ON to enable or OFF to disable 8 3 3 1 5 4 20mA out...

Page 39: ...his window allows you to visualise the state of the inputs This window is empty if no input has been requested by the customer 8 3 3 2 Options Setpoints date time etc It is possible to modify the setp...

Page 40: ...ture setpoint C is the control temperature of the condenser The water default setpoint V below this voltage the water defect alarm is generated This menu can also contain according to the requested op...

Page 41: ...NUAL Page 41 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization SECTION 2 INSTALLATION MANUAL 9 1 LOCATION 9 2 FASTENING 9 3 ELECTRICAL CONN...

Page 42: ...he device tank sewer etc on the left A power supply of 110V or 230V 50 60Hz An inlet for the sample to be analysed at a max pressure of 3 bar minimum 0 5bar 50 l h 100 to 500l h if a sampling treatmen...

Page 43: ...e reproduced without authorization The power supply to the analyzer must be connected downstream of a secured electrical installation in accordance with local standards For a 110V supply a special set...

Page 44: ...ructions No 10844 This document is the property of SERES and cannot be reproduced without authorization 9 3 2 Communication Figure 9 Input output board terminal drawing 1 channel For more information...

Page 45: ...UTION USER MAINTENANCE MANUAL Page 45 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization Figure 10 Input output board terminal drawing Multi...

Page 46: ...y the device and can be retrieved at any time this table is therefore specific to the configuration of the analyzer Go to the Tools tab Copy log files menu For the two different communication modes RS...

Page 47: ...he device The connection is made via the Ethernet connector available on the right side of the analyzer on the outside Simply mount the Ethernet cable in the connector and plug the connector For this...

Page 48: ...atmosphere on the left side of the analyser at 3 points 9 4 2 Standard for calibrating the analyser The standard inlet required for calibrating the device will be implemented via the other channel of...

Page 49: ...TOC EVOLUTION USER MAINTENANCE MANUAL Page 49 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization SECTION 3 USER MANUAL...

Page 50: ...and at the height of the device at room temperature A tray can be provided optional for setting them down To implement the reagent containers wear appropriate protection gloves goggles and protective...

Page 51: ...s the Electrical test menu Access the Solenoid Valve SV tab o Enable the draining solenoid valve Access the Pumps tab o Press ON to enable each reagent pump Check that the reagents are injected correc...

Page 52: ...hout authorization The Measurement window appears Press on the value of the threshold to modify them 10 6 Setting the parameters of the 4 20 mA range From the main screen Press of the relevant channel...

Page 53: ...and measuring This time is called in the Option menu Timing of sample purging line 10 8 Launch of the continuous cycles In order to start the continuous analysis press button in the main window 10 9...

Page 54: ...o do so Launch 1 measuring cycle with demineralised water instead of the sample Press button when the reactor is filled Enable the draining solenoid valve Purge the reagent pumps with demineralised wa...

Page 55: ...TOC EVOLUTION USER MAINTENANCE MANUAL Page 55 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization SECTION 4 MAINTENANCE MANUAL...

Page 56: ...his occasion we will check the cleanliness of the reactor Replacing the pipes of the peristaltic pumps every 3 months Complete disassembly of all sub assemblies on a yearly basis in order to clean and...

Page 57: ...ients The maximum deviation between the calculated coefficient and the current coefficient is of 50 of the current coefficient For example if the current coefficient is equal to 1 the calculated ratio...

Page 58: ...re the chemical method requires some measurements before giving a significant result One or several manual steps are then carried out before a calibration to obtain a correct calibration coefficient F...

Page 59: ...ogress from the main screen press Enter the authorised user code Access the Tools tab Push on Maintenance Start the ZERO measure by pressing At the end of the cycle a window displays the zero mass and...

Page 60: ...ctor during the reagent priming phase Stop the cycle in progress by pressing Stop Access the Tools tab Enter the authorised user code Access the Electrical test menu Press ON to run the pumps and OFF...

Page 61: ...SERES and cannot be reproduced without authorization o Switch off the analyser Unscrew the three screws on the front panel Remove the front panel of the pump body Remove the pipe from its compartment...

Page 62: ...pipes Perform a new calibration Replacing a pipe of the supply pump for the sample and water The pump pipes are to be changed every three months Important before replacing the pump pipes o Before chan...

Page 63: ...sure gauge MAN014 indicates less than 0 2 bars There is no air flow into the solenoid valve In such a case remove and clean up the device The soda lime granules have a fully violet coloring CO2 satura...

Page 64: ...occurs a second cartridge can be installed to upsized the TOC Once the reloading is done it is mandatory to fix the air circuit pressure to 3 bars 11 2 8 Copper cartridge depend upon application Copp...

Page 65: ...of the air and water network solenoid valves every 3 months replace the membrane if necessary 11 2 10 Compressor and Desiccant cartridge The compressor does not require any specific maintenance The re...

Page 66: ...crew this board replace and reconnect the cables 11 3 4 Replacing a pump Tooling Open ended wrenches Flathead screwdriver Hex wrench Before changing a pump it is recommended to empty it and or rinse i...

Page 67: ...ged systematically and provided with the new lamp WARNING Use anti UV protective glasses if an operation must be carried out on the entire system which is protected by the protective cover on which ar...

Page 68: ...easuring cell this action is quite simple Repeat the operations of section 11 3 6 1 to remove the cover Unscrew the two screws of the black part that supports the receiver Replace with the new receive...

Page 69: ...against the radiator and place the condenser system on top After adjusting the position screw the 4 fastening screws of the part The Peltier is maintained Insert the cables through the hole on the cas...

Page 70: ...leeves Replace with the new heating unit Connect the 2 sleeves Reconnect the 2 electrical components 11 3 9 Replacing the mass controller Switch the analyser OFF before performing the maintenance oper...

Page 71: ...side of the controller Unscrew the Earth braid The controller is removed To reassemble proceed by going back through the steps 11 3 10 Replacing the Air filter Switch the analyser OFF before performi...

Page 72: ...nd pressure at the sampling point The filling solenoid valve does not operate correctly Check that the filling solenoid valve is connected properly and that the LED lights up One or more hydraulic pip...

Page 73: ...if there is one operates correctly otherwise it may be necessary to install one The sewer system is blocked Check the condition of the pipes The zero of the device is calibrated incorrectly Check the...

Page 74: ...TOC EVOLUTION USER MAINTENANCE MANUAL Page 74 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization 13 Annexs NF EN ISO 9001 2015...

Page 75: ...TOC EVOLUTION USER MAINTENANCE MANUAL Page 75 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization DECLARATION CE UKCA OF CONFORMITY...

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