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AMI Hydrazine

Safety Instructions

A-96.250.501 / 280915

1.3.

Restrictions for use

Alcalizing

Reagent

Correct the pH of the sample with Diisopropylamine only, however,

Diisopropylamine is not included in delivery. Please buy it from your

local supplier: E.g. VWR 6x 1l: 8.03646.1000, or SIGMA 38290-1L-F.

Sample

Require-

ments

No sand (or other polishing material) or oil are allowed in the sam-

ple.

The instrument is specified for a max. pressure of 2 bar (28 psi). If

the sample pressure exceeds 2 bar, please mount a pressure re-

duction in front of the instrument inlet.

Phosphates may interfere with the hydrazine measurement.
The pH value of the sample must be equal or higher than pH 7.

Flow

Interruption

High concentrations of Diisopropylamine reagent may attack the

acrylic material of the flow cell. This can cause cracks and render

the flow cell completely unusable. This will not happen during nor-

mal operation. However, if the sample flow is stopped, undiluted di-

isoproylamine will diffuse through the diffusion tube and can cause

damage. Therefore, the following rules should be observed if the

sample flow is stopped for more than one day:
Remove diisopropylamine bottle and close it. Keep it in a safe

place for further use.

WARNING

Diisopropylamine is corrosive.



Read the Safety Data Sheets (SDS) first.



Wear suitable protective clothing, gloves and eye/face protec-

tion.



Avoid inhalation of DIPA vapor.



In case of contact with eyes, rinse immediately with plenty of

water eyelid wide open for at least 10 min, summon medical

advice. In case of accident or if you feel unwell, summon

medical advice immediately (show the label where possible).



Screw an empty reagent bottle on the holder.



Let the sample flow for another 30 minutes to rinse out the Di-

isopropylamine dissolved in the diffusion tubing material.



Stop sample flow.

Содержание AMI Hydrazine

Страница 1: ...AMI Hydrazine Version 5 40 and higher A 96 250 501 280915 Operator s Manual ...

Страница 2: ...alists around the world For any technical question contact your nearest SWAN representative or the manufacturer SWAN ANALYTISCHE INSTRUMENTE AG Studbachstrasse 13 8340 Hinwil Switzerland Internet www swan ch E mail support swan ch Document Status Title Monitor AMI Hydrazine Operator s Manual ID A 96 250 501 Revision Issue 00 June 2007 First Edition 01 April 2015 Update to Rev 5 40 main board V2 4 ...

Страница 3: ...the Reference Electrode 16 3 5 Install the Temperature Sensor 17 3 6 Electrical Connections 18 3 6 1 Connection Diagram 20 3 6 2 Power Supply 21 3 7 Relay Contacts 22 3 7 1 Input 22 3 7 2 Alarm Relay 22 3 7 3 Relay Contacts 1 and 2 23 3 8 Signal Outputs 25 3 8 1 Signal Output 1 and 2 current outputs 25 3 9 Interface Options 25 3 9 1 Signal Output 3 26 3 9 2 Hyperterminal Interface 26 3 9 3 Profibu...

Страница 4: ... Bottle 44 6 8 Changing the Diffusion Tube 45 6 9 Calibration of Hydrazine Sensor 46 6 9 1 Calibration Procedure 46 6 9 2 Zero Hydrazine 46 6 9 3 Process Hydrazine 47 6 10 Replacing Fuses 49 6 11 Longer Stop of Operation 50 7 Troubleshooting 51 7 1 Error List 53 8 Program Overview 56 8 1 Messages Main Menu 1 56 8 2 Diagnostics Main Menu 2 57 8 3 Maintenance Main Menu 3 58 8 4 Operation Main Menu 4...

Страница 5: ... instructions are given throughout this manual at the respective locations where observation is most important Strictly follow all safety instructions in this publication Target audience Operator Qualified person who uses the equipment for its intended purpose Instrument operation requires thorough knowledge of applications instrument functions and software program as well as all applicable safety...

Страница 6: ...w the prevention instructions carefully WARNING Severe injuries or damage to the equipment can occur if such warnings are ignored Follow the prevention instructions carefully CAUTION Damage to the equipment minor injury malfunctions or incor rect process can be the consequence if such warnings are ig nored Follow the prevention instructions carefully Mandatory Signs The importance of the mandatory...

Страница 7: ...razine Safety Instructions A 96 250 501 280915 5 Warning Signs The importance of the warning signs in this manual Electrical shock hazard Corrosive Harmful to health Flammable Warning general Attention general ...

Страница 8: ...bility for any claim resulting from unauthorized modification or alter ation WARNING Electrical Shock Hazard If proper operation is no longer possible the instrument must be disconnected from all power lines and measures must be taken to prevent inadvertent operation To prevent from electrical shock always make sure that the ground wire is connected Service shall be performed by authorized personn...

Страница 9: ...se cracks and render the flow cell completely unusable This will not happen during nor mal operation However if the sample flow is stopped undiluted di isoproylamine will diffuse through the diffusion tube and can cause damage Therefore the following rules should be observed if the sample flow is stopped for more than one day Remove diisopropylamine bottle and close it Keep it in a safe place for ...

Страница 10: ...fications as option Only possible if no communication interface is used Relays Two potential free contacts programmable as limit switches for measuring values controllers or timer for system cleaning with au tomatic hold function Both contacts can be used as normally open or normally closed Maximum load 1 A 250 VAC Alarm Relay One potential free contact Alternatively Open during normal operation c...

Страница 11: ...e a flow Alarm is triggered The signal of amperometric systems depends on flow rate The constant head guarantees a constant flow if the sample always overflows into the longer constant head tube Temperature compensation is done automatically Fluidics The measurement of hydrazine requires a high pH of the sample The AMI Hydrazine buffers the pH to pH 10 5 by adding diisopro pylamine The diisopropyl...

Страница 12: ... D E F Constant head Overflow tube to waste long Overflow tube to sensor short Flow regulating valve Sample inlet Hydrazine sensor G H I J K L Filter vessel Sample outlet Garb sample outlet Grab sample valve Diisopropylamine Diffusions tube A B C D F E G H I J K L ...

Страница 13: ... Range Accuracy Stability Response time 0 1 600 ppb 5 of reading up to 200 ppb 15 up to 600 ppb or 2 ppb whichever is greater 5 of reading per month or 2ppb per month 90 of change in 60 sec after the sample entered the flow cell Measuring range temperature Measuring range Resolution up to 60 C 0 1 C Sample requirements Flow rate Temperature Sample inlet pressure Sample outlet pressure pH value app...

Страница 14: ...MI Hydrazine Product Description Dimensions Panel Mounting hole distance Screws Weight 280x850x180 mm stainless steel 254x824 8 mm diameter 12 0 kg AMI Hydrazine 850 mm 33 13 mm 4 x dia 8 mm 254 mm 10 280 mm 11 824 mm 32 7 16 ...

Страница 15: ...ffusion tube Reference electrode Grab sample valve Grab sample outlet Flow regulating valve Hydrazine sensor K L M N O P Q R S T Filter vessel Sample outlet Sample inlet Hall sensor not visible Flow cell block Constant head Overflow tube to sensor short Overflow tube to waste long Constant head cover Temperature sensor A B C D E F G H I J K L M N O P Q R S T ...

Страница 16: ...rence Electrode p 16 Install the Temperature Sensor p 17 Diisopropyl amine Install the Diisopropylamine Bottle p 28 Electrical wir ing Note Do not switch on the Instrument until all electrical connections are made Connect all external devices like limit switches current loops and pumps see Connection Diagram p 20 Connect the power cord see Power Supply p 21 Power up Establish Sample Flow p 29 Swit...

Страница 17: ...ation material is available 4 Screws 8x60 mm 4 Dowels 4 Washers 8 4 24 mm Mounting re quirements The instrument is only intended for indoor installation Instrument Specification p 11 3 3 Connecting Sample and Waste Sample inlet Slide the knurled nut C and the compression ferrule B over the 4x6 plastic tube E Push it into the serto fitting A and tighten the knurled nut Waste Connect the 1 2 tube F ...

Страница 18: ...nd PCB in the AMI transmitter To install the reference electrode proceed as follows 1 Loosen the union nut D 2 Remove the protective cap B from the reference electrode C 3 Push the reference electrode through the union nut D into the bore of the flow cell block E as far as it will go 4 Tighten the union nut 5 Remove the connector A from the panel and screw it onto the reference electrode A B C Con...

Страница 19: ... already connected to the front end PCB in the AMI transmitter To install the temperature sensor proceed as follows 1 Remove the temperature sensor A from the panel 2 Put the temperature sensor in the designated hole of the con stant head cover B 3 Push it into the hole as far as it will go A B C Temperature sensor Constant head cover Constant head A B C ...

Страница 20: ...operate the instrument from an power outlet which has a ground connection Make sure the power specification of the instrument corre sponds to the power on site Cable thicknesses In order to comply with IP66 use the following cable thicknesses Note Protect unused cable glands Wire For Power and Relays Use max 1 5 mm2 AWG 14 stranded wire with end sleeves For Signal Outputs and Input Use 0 25 mm2 AW...

Страница 21: ...ted to the following con tacts are disconnected from the power before resuming in stallation relay 1 relay 2 alarm relay WARNING To prevent from electrical shock do not connect the instrument to the power unless the groundwire PE is connected Do not connect unless specifically instructed to do so WARNING The mains of the AMI Transmitter must be secured by a main switch and appropriate fuse or circ...

Страница 22: ...tallation 3 6 1 Connection Diagram CAUTION Use only the terminals shown in this diagram and only for the mentioned purpose Use of any other terminals will cause short circuits with possible corresponding consequences to material and personnel ...

Страница 23: ...arts must be per formed by professionals Note The protective earth wire Ground has to be connected to the grounding terminal Installation requirements The installation must meet the following requirements Mains fuse 1 6 AT Mains cable to comply with standards IEC 60227 or IEC 60245 flammable rating FV1 Mains equipped with an external switch or circuit breaker near the instrument easily accessible ...

Страница 24: ...d 1 AT 250 VAC Alarm output for system errors Error codes see Troubleshooting p 51 Programming see menu 5 3 1 p 69 NOTICE With certain alarms and certain settings of the AMI transmitter the alarm relay does not switch The error however is shown on the display 1 usual use Terminals Description Relay connection NC1 Normally Closed 10 11 Active opened during normal operation Inactive closed on error ...

Страница 25: ...the status of the relays described below For programming see Menu Installation 5 3 2 and 5 3 3 p 71 Relay config Terminals Jumper pos Description Relay configuration Normally Open 6 7 Relay 1 8 9 Relay 2 Inactive opened dur ing normal operation and loss of power Active closed when a programmed function is executed Normally Closed 6 7 Relay 1 8 9 Relay 2 Inactive closed during normal operation and ...

Страница 26: ...cuit in par allel to the load A snubber is not necessary if an AMI relaybox is used Resistive load Resistive loads max 1A and control signals for PLC impulse pumps and so on can be connected without further measures Actuators Actuators like motor valves are using both relays One relay con tact is used for opening the other for closing the valve i e with the 2 relay contacts available only one moto...

Страница 27: ... Terminals 14 and 13 Signal output 2 Terminals 15 and 13 For programming see Chapter 9 5 2 Signal Outputs p 65 Menu Installation 3 9 Interface Options The slot for interfaces can be used to expand the functionality of the AMI instrument with either an additional signal output a Profbus or Modbus interface a Hyperterminal interface an USB Interface A B C D AMI Transmitter Slot for interfaces Fronte...

Страница 28: ...B Note Max burden 510 Terminal 38 and 37 3 9 2 Hyperterminal Interface Terminal 50 52 53 The AMI hyperterminal Interface RS232 PCB is used for Logger down load and Firmware up load For detailed information see the corresponding manual AMI RS232 Interface Hyperterminal Interface PCB A Third signal output 0 4 20 mA PCB installed on main board A ...

Страница 29: ...he PRO FIBUS MODBUS manual Use appropriate network cable Note The switch must be ON if only one instrument is installed or on the last instrument in the bus Profibus Modbus Interface PCB RS 485 3 9 4 USB Interface The USB Interface is used to store Logger data and for Firmware up load For detailed information see the corresponding installation instruction USB Interface A On OFF switch PB DPV1 V5 5...

Страница 30: ...83 591 010 WARNING Diisopropylamine is corrosive Read the Safety Data Sheets SDS first Wear suitable protective clothing gloves and eye face pro tection Avoid inhalation of DIPA vapor To prevent formation of re agent vapors close the reagent bottle firmly check the EPDM seal regularly In case of contact with eyes rinse immediately with plenty of water eyelid wide open for at least 10 min summon me...

Страница 31: ...ottle as shown in the picture above 7 Tighten the screw cover well 4 2 Establish Sample Flow 1 Make sure that the grab sample valve is closed 2 Open the flow regulating valve 3 Wait until the flow cell is completely filled 4 Switch on power 4 3 Programming Program all parameters for external devices interface recorders etc Program all parameters for instrument operation limits alarms See Program O...

Страница 32: ... has to be known Hydrazine reacts with dimethylaminobenzal dehyde in an acid solution and forms a yellow color The color intensity can be measured by a photometer Refer to an appropri ate standard method e g DIN 38413 The manual sample must be taken from the grab sample outlet of the flow cell Let the sample flow out for roughly 1 minute before grabbing the sample for the manual analysis See Calib...

Страница 33: ...ges to move back to the previous menu level B to move DOWN in a menu list and to decrease digits C to move UP in a menu list and to increase digits D to open a selected sub menu to accept an entry Exit Enter B C D A 25 4 C RUN 9 l h 14 10 45 R1 0 45 ppm R2 1 Installation Operation Diagnostics Messages Maintenance Main Menu Enter Exit ...

Страница 34: ...ERROR Error Fatal Error C Keys locked transmitter control via Profibus D Time E Process values F Sample temperature G Sample flow H Relay status upper lower limit not yet reached upper lower limit reached control upw downw no action control upw downw active dark bar indicates control intensity motor valve closed motor valve open dark bar indicates approx position timer timer timing active hand rot...

Страница 35: ...nt parameters that might need to be modified during daily routine Normally password protected and used by the process operator Subset of menu 5 Installation but process related Menu Installation 5 For initial instrument set up by SWAN authorized person to set all instrument parameters Can be protected by means of password 1 Messages Operation Maintenance Diagnostics Main Menu Installation 1 1 Pend...

Страница 36: ...w parameter is set 5 1 2 Sensors Sensor type FOME Temperature NT5K Standards Disinf Free chlorine 4 4 1 Logger Log interval 30 min Clear logger no 4 1 3 Logger Clear logger no Log interval 30min 1 Hour Interval 5 min 30 min 10 min 4 1 3 Logger Log interval 10 min Clear logger no 4 1 3 Logger Log interval Clear logger no No Save Yes 1 Select the value you want to change 2 Press Enter 3 Set required...

Страница 37: ... a process calibration see Process Hydrazine p 47 Monthly Exchange Diisopropylamine bottle if there is less than 150 ml half of the diffusion tube has to be covered with Diisopropylamine see Changing Diisopropylamine Bottle p 44 Half yearly Replace sealing of reagent bottle EPDM Yearly Exchange diffusion tube see Changing the Diffusion Tube p 45 ...

Страница 38: ...or In case of contact with eyes rinse immediately with plenty of water eyelid wide open for at least 10 min summon medical advice In case of accident or if you feel unwell summon medical advice immediately show the label where possible 1 Wear safety gloves and safety glasses 2 Remove the diisopropylamine bottle and close it well 3 Screw an empty bottle on the holder Let the sample run for 30 min 4...

Страница 39: ...ample main tap before the filter 3 Unscrew and remove the filter vessel C from the flow cell block 4 Unscrew and remove the filter from B the flow cell block 5 Backwash the filter under pressure of tap water Clean the out side of the filter 6 Install the filter and filter vessel again 7 Open sample supply and flow regulating valve again A B C Flow regulating valve Filter Filter vessel A B C ...

Страница 40: ...d hydrazine reading is 0 ppm 3 Shut off power of the instrument 4 Disconnect the BNC connector G from the hydrazine sensor F Prevent it from getting wet 5 Unscrew and remove one of the two knurled nuts H A B C D Flow regulating valve Threaded bolt Rotor O Ring E F G H Orifices Hydrazine sensor BNC connector Knurled nut A B C G F F E C B D H H D E ...

Страница 41: ...ing 1 Remove the rotor C from the hydrazine sensor 2 Clean the tow orifices E with a pipe cleaner or a toothpick 3 Clean the rotor with a soft tissue 4 Cautiously wipe the sensor with a soft tissue mainly the plati num parts and the whole area which is in contact with water 5 After cleaning rinse all parts well with clean water Install 1 Put rotor on the sensor 2 Install the sensor into the flow c...

Страница 42: ...rew B 3 Pull the reference electrode out 4 Wipe sensor tip cautiously with a soft tissue If necessary use alcohol to remove oily deposits Do not use any acid 5 Push the reference electrode through the union screw into the flow cell as far as it will go 6 Tighten the union screw A B Reference electrode Union screw E F Washer O Ring C D B A ...

Страница 43: ...usehold deliming agent in standard concentration A B C D E F G H I J K L M N O P Q R Temperature senor Tube from sample inlet Tube to hydrazine sensor Constant head cover Constant head tube Constant head tube fixation Overflow tube to waste Overflow tube to sensor Flow cell block Grab sample tap Fixing screw Flow regulating valve Sample Inlet Hall sensor Filter Filter vessel Hydrazine sensor Sampl...

Страница 44: ...e flow cell block I but with out however removing the flow cell block from the panel Tube from sample inlet to DIPA bottle B Tube from DIPA bottle to hydrazine sensor C Constant head cover D Constant head tube E Overflow tube to waste long G Overflow tube to sensor short H Grab sample tap J Sample inlet M and grab sample outlet not visible Filter vessel P Filter O Sample outlet R Hall Effect senso...

Страница 45: ...rings and grease them with teflon paste 3 Assemble the flow cell 4 Install all sensors 5 Open the main tap and wait until the flow cell is filled 6 Check all connection for leakage if necessary retighten leaky points 7 Switch on the instrument A B C Teflon band Hose nozzle at sample outlet Serto fitting at sample inlet and grab sample outlet C B A ...

Страница 46: ... E 6 Dip the diffusion tube into the beaker filled with high purity wa ter Rinse some seconds 7 Push the diffusion tube over the steel tubes 8 Open the new reagent bottle and add 20 ml of high purity water Note If you fill up Diisopropylamine into the almost empty bottle no high purity water needs to be added 9 Slide the reagent bottle over the diffusions tube and ensure that it lies pretzel shape...

Страница 47: ...he new diffusion tube 1 Fill roughly 750 ml high purity water into a 1 l bea ker 2 Unscrew and remove Diisopropylamine bottle from the holder 3 Close the bottle immediately 4 Remove the old diffusion tube from the steel tubes 5 Dip the new diffusion tube into the beaker filled with high purity water and rinse it some seconds 6 Push the new diffusion tube over the steel tubes 7 Open the reagent bot...

Страница 48: ...on is not necessary If your quality procedure specifies a zero point calibration please proceed as described below Note Let the instrument run continuously for at least 5 days in normal operation before doing a zero point calibration 1 Navigate to menu Maintenance Calibration Zero Hydra zine 2 Press Enter 3 Follow the instructions on the screen During a zero calibration the sample flow is turned o...

Страница 49: ...e performing the manual analysis enter the difference between the measuring values of the AMI Hydrazine Example Displayed measuring value of AMI Hydrazine during grab sample 10 ppb Displayed measuring value of AMI Hydrazine after concentration determination 15 ppb Determined hydrazine concentration 8 ppb There is a change of the measurement value of 50 during the concentration determination This m...

Страница 50: ...nt value Raw value Process value Current value and Process value are equal 3 Press Enter 4 Enter the calculated value Use the or keys to increase or decrease the Process value 5 Press Enter to save Process Hydrazine Raw value x µA Save Enter Process Value 18 80 ppm 3 1 4 1 Current Value 18 80 ppb Process Hydrazine Current Value 18 8 ppb Raw value x nA Save Enter Process Value 24 0 ppb 3 1 2 5 3 1 ...

Страница 51: ...are disconnected from the power before resuming in stallation relay 1 relay 2 alarm relay When a fuse has blown find out the cause and fix it before replac ing it with a new one Use tweezers or needle nosed pliers to remove the defective fuse Use original fuses provided by SWAN only A B C D E F 1 6 AT 250V Instrument power supply 1 0 AT 250V Relay 1 1 0 AT 250V Relay 2 1 0 AT 250V Alarm relay 1 0 ...

Страница 52: ...ter Rinse it some seconds 3 Unscrew and remove the filter vessel from the flow cell block empty and dry it then screw it onto the flow cell block again 4 Loosen the connector from the reference electrode and put the connector cap on the electrode plug Do not spill water on connector 5 Remove the reference electrode from the flow cell block fill wa ter in the protective cap and put the protective c...

Страница 53: ... sample is too low thereby the current dif ference to zero is too small Process value used for calibration should be higher Check the diagnostic value of the zero point Low sample flow resulting in no signal difference to zero Check sample inlet pressure if necessary readjust sample flow to min 170 rpm Hydrazine sensor contaminated Sensor does not provide enough current for the value measured with...

Страница 54: ...ually too little running in time Possible cause Corrective action Diisopropylamine bot tle empty Exchange Diisopropylamine bottle see Changing Diisopropylamine Bottle p 44 or Install the Diisopropylamine Bottle p 28 Insufficient immersion depth of the diffusion tube Place the diffusion Tube correct see Changing the Diffusion Tube p 45 Orifices at sensor inlet clogged Clean the senor see Cleaning o...

Страница 55: ...mple Flow low Such Errors are marked E0xx bold and orange Errors which indicate a hardware failure of the instrument Such Errors are marked E0xx bold and red Error or fatal Error Error not yet acknowledged Check Pending Errors 1 1 5 and take corrective action Press ENTER Navigate to menu Pending Errors Press ENTER Press ENTER to acknowledge the Pending Errors The Error is reset and saved in the Me...

Страница 56: ...ample Flow high check Inlet pressure readjust sample flow check programmed value 5 3 1 2 2 p 70 E010 Sample Flow low check Inlet pressure readjust sample flow clean instrument check programmed value 5 3 1 2 35 p 70 E011 Temp shorted Check wiring of temperature sensor see Connection Diagram p 20 Check sensor E012 Temp disconnected Check wiring of temperature sensor see Connection Diagram p 20 Check...

Страница 57: ...on Relay contact Relay 1 2 see 5 3 2 and 5 3 3 p 71 E024 Input active See If Fault Yes is programmed in Menu see 5 3 4 p 75 E025 IC MK41T56 call service E026 IC LM75 call service E027 IC PCF8574 call service E028 EEProm Microcon call service E029 EEProm Motherboard call service E030 EEProm Frontend call service E031 Calibration Recout call service E032 Wrong Frontend call service E033 Power on non...

Страница 58: ...3 Maintenance is for service Calibration simulation of outputs and set time date Please protect with password Menu 4 Operation is for the user allowing to set limits alarm values etc The presetting is done in the menu Installation only for the System engineer Please protect with password Menu 5 Installation Defining assignment of all inputs and outputs measuring parameters interface passwords etc ...

Страница 59: ...s Days Hours Minutes Seconds 2 1 4 1 2 1 4 Sensors Hydrazine Sensor Current Value 2 2 2 2 1 Raw value Ref voltage Cal History Number 2 2 1 5 1 2 2 1 5 Date Time Offset Slope Miscellaneous Case Temp 2 2 2 1 2 2 2 Sample Sample ID 2 3 1 2 3 Temperature C Nt5K Ohm Sample Flow Raw value I O State Alarm Relay 2 4 1 2 4 Relay 1 and 2 2 4 2 Input Signal Output 1 and 2 Interface Protocol 2 5 1 only with R...

Страница 60: ...Output 2 3 2 5 Set Time Date Time 3 3 Sensors Filter Time Const 4 1 1 Menu numbers 4 1 Hold after Cal 4 1 2 Relay Contacts Alarm Relay Alarm Alarm High 4 2 1 1 1 4 2 4 2 1 4 2 1 1 Alarm Low 4 2 1 1 26 Hysteresis 4 2 1 1 36 Delay 4 2 1 1 46 Relay 1 and 2 Setpoint 4 2 x 100 4 2 2 and 4 2 3 Hysteresis 4 2 x 200 Delay 4 2 x 30 Input Active 4 2 4 1 4 2 4 Signal Outputs 4 2 4 2 Output Control 4 2 4 3 Fa...

Страница 61: ...36 Delay 5 3 1 1 46 Sample Flow Flow Alarm 5 3 1 2 1 5 3 1 2 Alarm High 5 3 1 2 2 Alarm Low 5 3 1 2 36 Sample Temp Alarm High 5 3 1 3 1 5 3 1 3 Alarm Low 5 3 1 3 26 Case Temp high 5 3 1 4 Case Temp low 5 3 1 5 Relay 1 and 2 Function 5 3 2 1 5 3 3 1 5 3 2 5 3 3 Parameter 5 3 2 20 5 3 3 20 Setpoint 5 3 2 300 5 3 3 301 Hysteresis 5 3 2 400 5 3 3 401 Delay 5 3 2 50 5 3 3 50 Input Active 5 3 4 1 5 3 4 ...

Страница 62: ...60 A 96 250 501 280915 AMI Hydrazine Program Overview Interface Protocol 5 5 1 only with RS485 5 5 Device Address 5 5 21 RS232 or USB Baud Rate 5 5 31 interface Parity 5 5 41 ...

Страница 63: ...only be viewed not modified 2 1 Identification Desig Designation of the instrument Version Firmware of instrument e g V5 40 11 14 2 1 3 Factory Test Test date of the Instrument and Motherboard 2 1 4 Operating Time Shows the operating time in Years Days Hours Minutes and Seconds 2 2 Sensors 2 2 1 Hydrazine Sensor Current value Actual measuring value in ppb Raw value measuring value in nA Ref Voltag...

Страница 64: ...of the sample Temperature Shows temperature in C Nt5K Shows raw value of the temperature in Sample Flow Shows the sample Flow in rpm Raw value Shows the sample Flow in Hz 2 4 I O State Shows actual status of all in and outputs 2 4 1 2 5 Interface Only available if optional interface is installed Review programmed communication settings Alarm Relay Open or closed Relay 1 and 2 Open or closed Input ...

Страница 65: ...lect the alarm relay relay 1or 2 signal output 1or 2 with the or key Press the Enter key Change the value or state of the selected item with the or key Press the Enter key The value is simulated by the relay signal output At the absence of any key activities the instrument will switch back to normal mode after 20 min If you quit the menu all simulated val ues will be reset and the transmitter rebo...

Страница 66: ... logger The logger data can be downloaded to a PC by Hyperterminal or SWAN Terminal if option HyperTerminal interface is installed copied to a PC with an USB stick if option USB interface is in stalled The logger can save approx 1500 data records The Records con sists of Date time alarms measuring value measuring value un compensated case temperature flow 4 3 1 Log Interval Select a convenient log...

Страница 67: ...range and a function to each signal output 5 2 1 1 Parameter Assign one of the process values to the signal output Available values Hydrazine Temperature Sample Flow 5 2 1 2 Current Loop Select the current range of the signal output Make sure the connected device works with the same current range Available ranges 0 20 mA or 4 20 mA 5 2 1 3 Function Define if the signal output is used to transmit a...

Страница 68: ...or the bilinear scale If Parameter Hydrazine 5 2 1 40 10 Range low 0 00 1000 ppb 5 2 1 40 20 Range high 0 00 1000 ppb If Parameter Temperature 5 2 1 40 11 Range low 30 0 to 120 C 5 2 1 40 21 Range high 30 0 to 120 C If Parameter Sample flow 5 2 1 40 12 Range low 0 300 rpm 5 2 1 40 22 Range high 0 300 rpm A B linear bilinear X Measured value X Measured value logarithmic 20 0 0 0 1 0 2 0 3 0 4 0 5 1...

Страница 69: ... controller The combination of a P controller with a D controller will minimize the response time to a fast change of the process value If the derivative time is set to zero the D controller is switched off Parameters setpoint P Band derivative time PID controller The combination of a P an I and a D con troller allows a proper control of the process Parameters setpoint P Band reset time derivative...

Страница 70: ...Band Range 0 to 100 C 5 2 1 43 Control Parameters if Parameter Sample Flow 5 2 1 43 12 Setpoint Range 0 300 rpm 5 2 1 43 22 P Band Range 0 300 rpm 5 2 1 43 3 Reset time The reset time is the time till the step response of a sin gle I controller will reach the same value as it will be suddenly reached by a P controller Range 0 9 000 sec 5 2 1 43 4 Derivative time The derivative time is the time til...

Страница 71: ...ram alarm levels for the following parameters Alarm Hydrazine Sample Flow Sample Temp Case Temp high Case Temp low 5 3 1 1 Alarm Hydrazine 5 3 1 1 1 Alarm High If the measured value rises above the alarm high val ue the alarm relay is activated and E001 is displayed in the mes sage list Range 0 00 1000 ppb 5 3 1 1 25 Alarm Low If the measured value falls below the alarm low value the alarm relay i...

Страница 72: ...0 rpm 5 3 1 2 35 Alarm Low If the measuring values falls below the programmed value E010 will be issued Range 150 300 rpm 5 3 1 3 Sample Temp Define at which sample temperature an alarm should be issued 5 3 1 3 1 Alarm High If the measured value rises above the alarm high val ue the alarm relay is activated and E007 is issued Range 30 70 C 5 3 1 3 25 Alarm Low If the measured value rises above the...

Страница 73: ...When the relays are used as upper or lower limit switches program the following 5 3 2 20 Parameter select a process value 5 3 2 300 Setpoint If the measured value rises above respectively falls below the set point the relay is activated 5 3 2 400 Hysteresis within the hysteresis range the relay does not switch This prevents damage of relay contacts when the measured value fluctuates around the ala...

Страница 74: ... is controlled by the operating time 5 3 2 32 20 Cycle time duration of one control cycle on off change Range 0 600 sec 5 3 2 32 30 Response time Minimal time the metering device needs to react Range 0 240 sec 5 3 2 32 4 Control Parameters Range for each Parameter same as 5 2 1 43 p 68 Examples of metering devices that are pulse frequency driven are the classic membrane pumps with a potential free...

Страница 75: ... Mode Operating mode 5 3 2 340 Interval The interval can be programmed within a range of 1 1440 min 5 3 2 44 Run Time Enter the time the relay stays active Range 5 6000 sec 5 3 2 54 Delay during run time plus the delay time the signal and control outputs are held in the operating mode programmed below Range 0 6 000 sec 5 3 2 6 Signal Outputs Select operating mode of the signal output Actuator Moto...

Страница 76: ...l 5 3 2 6 Signal Outputs see Interval 5 3 2 7 Output Control see Interval The relay contact can be activated at one or several days of a week The daily starting time is valid for all days 5 3 2 342 Calendar 5 3 2 342 1 Start time The programmed start time is valid for each of the pro grammed days To set the start time see 5 3 2 341 p 74 Range 00 00 00 23 59 59 5 3 2 342 2 Monday Possible settings ...

Страница 77: ...4 Fault 5 3 4 5 Delay Time which the instrument waits after the input is deactivat ed before returning to normal operation Range 0 6 000 Sec 5 3 2 1 Function Fieldbus No Input is never active When closed Input is active if the input relay is closed When open Input is active if the input relay is open Continuous Signal outputs continue to issue the measured value Hold Signal outputs issue the last ...

Страница 78: ...values including communication parameters 5 4 3 Load Firmware Firmware updates should be done by instructed service personnel only 5 4 4 Password Select a password different from 0000 to prevent unau thorized access to the following menus 5 4 4 1 Messages 5 4 4 2 Maintenance 5 4 4 3 Operation 5 4 4 4 Installation Each menu may be protected by a different password If you forgot the passwords contac...

Страница 79: ... 30 ID Nr Range Analyzer Manufacturer Multivariable 5 5 40 Local operation Range Enabled Disabled 5 5 1 Protocol Modbus RTU 5 5 21 Device address Range 0 126 5 5 31 Baud Rate Range 2400 115200 Baud 5 5 41 Parity Range none even odd 5 5 1 Protocol Hyper Terminal 5 5 23 Baudrate Range 2400 115200 Baud see separate RS232 Operation Manual for Logger download 5 5 1 Protocol USB Stick Only visible if an...

Страница 80: ...0 mA Function linear Scaling Range low 0 00 ppb Scaling Range high 100ppb Signal Output 2 Parameter Temperature Current loop 4 20 mA Function linear Scaling Range low 0 0 C Scaling Range high 50 0 C Alarm Relay Alarm Hydrazine Alarm high 1000ppb Alarm low 0 00 ppb Hysteresis 10ppb Delay 5 Sec Sample Flow Flow Alarm yes Sample Flow Alarm high 300 rpm Sample Flow Alarm low 150 rpm Sample Temp Alarm ...

Страница 81: ...ttings Pulse Frequency 120 min Settings Control Parameters Setpoint 300 rpm Settings Control Parameters P band 10 rpm Common Settings Settings Control Parameters Reset time 0 Sec Settings Control Parameters Derivative Time 0 Sec Settings Control Parameters Control Timeout 0 Min Settings Actuator Time proportional Cycle time 60 s Response time 10 s Settings Actuator Motor valve Run time 60 s Neutra...

Страница 82: ...501 280915 AMI Hydrazine Default Values Output Control off Fault no Delay 10 Sec Miscellaneous Language English Set default no Load firmware no Password for all modes 0000 Sample ID Interface Protocol Hyperterminal ...

Страница 83: ... 41 Fluidics 9 Function Control upwards downwards 72 Limit upper lower 71 Timer 73 I Input 8 22 75 Instrument Overview 13 Interface 8 Interface RS232 26 Interface RS485 27 Interface USB 27 L Logger 64 Longer Stop of Operation 50 M Mounting requirements 15 O On site requirements 11 P Power Supply 11 21 R Relay Contacts 1 and 2 23 Relays 8 S Safety Features 9 Sample Flow 70 Sample flow establish 29 ...

Страница 84: ...82 A 96 250 501 280915 AMI Hydrazine Notes 12 Notes ...

Страница 85: ...AMI Hydrazine Notes A 96 250 501 280915 83 ...

Страница 86: ...ry companies and distributors cooperates with independent representatives all over the world SWAN Products Analytical Instruments for High Purity Water Feedwater Steam and Condensate Potable Water Pool and Sanitary Water Cooling Water Waste Water and Effluents Made in Switzerland ...

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