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Shimadzu MOC-120H, Инструкция по эксплуатации

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42

 Preparatory measuring mode

In preparatory measuring mode, predicted measurements are displayed while measuring is in
progress and measuring is halted under the same conditions as when operating in automatic
operation mode. The difference between the measured values of automatic operation mode and
pedictive measuring mode is displayed as the necessary bias.
In order to obtain accurate predicted measurements, it is recommended to perform at least 5
preparatory measurements and take the average to determine the bias.
You should also take care in terms of the amount of the sample and the way the sample material
is placed onto the sample pan. They must be the same every time and laid out as evenly as
possible.

 Predictive measuring mode

Prior to predictive measurements, specify the same drying temperature, predicted value conver-
gence range, and bias as calculated from preparatory measurements.
Note that measuring is halted if no predicted measurement has been calculated after 30 minutes
have elapsed after starting the measurement.

 

SALES & TECHNICAL SUPPORT 

QAQC LAB www.qclabequipment.com TEL (804) 318-3686

Содержание MOC-120H

Страница 1: ...ON MANUAL ELECTRONIC MOISTURE BALANCE MOC 120H 321 56738 21F DEC 2008 READ AND UNDERSTAND THIS MANUAL BEFORE OPERATION SAVE THIS MANUAL SALES TECHNICAL SUPPORT QAQC LAB www qclabequipment com TEL 804...

Страница 2: ...SALES TECHNICAL SUPPORT QAQC LAB www qclabequipment com TEL 804 318 3686...

Страница 3: ...mission of the company are strictly prohibited Microsoft Windows Windows Vista and Excel are registered trademarks of Microsoft Corporation of the U S A in the United States and other countries All ot...

Страница 4: ...and laboratory use Part 1 General requirements The last two digits of the year in which CE marking was affixed for Low Voltage Directive 2006 95 EC are 03 Note 1 This declaration becomes invalid if t...

Страница 5: ...essional use only Contact Shimadzu service representative when the equipment has reached the end of its life They will advise you regarding the equipment take back With your co operation we are aiming...

Страница 6: ...xic gas Do not place flammable materials near the electronic moisture balance Some parts of the electronic moisture balance become extremely hot during operation and could lead to fire if flammable ma...

Страница 7: ...e the parts marked with circles when operating Do not measure hazardous samples Use the Electronic Moisture Balance only for measuring the moisture content in a sample by moisture evaporation through...

Страница 8: ...f and disconnect power cable when any emergency occurs such as abnormal smell smoke or fire Key and Power Switch Operation Do not turn the power on while pressing any keys Do not operate any keys exce...

Страница 9: ...vices specified by Shimadzu to the moisture balance s connector If you do the balance may stop working normally In order to avoid trouble always connect peripheral devices in accordance with the direc...

Страница 10: ...SALES TECHNICAL SUPPORT QAQC LAB www qclabequipment com TEL 804 318 3686...

Страница 11: ...Display Mode 15 8 2 Types of Settings 16 8 3 Descriptions of Individual Measuring Condition Settings 16 8 3 1 Selecting the CONDITIONS Measuring conditions storage area 17 8 3 2 Selecting the MODE Mea...

Страница 12: ...ature Calibration Option required 47 14 Printing Output to a Printer Option 49 14 1 Printer Output Sample 49 14 2 Outputting Stored Measurement Data 52 15 Computer Interface 53 15 1 RS 232C Interface...

Страница 13: ...omputer without installing software This and other various functions can be used to meet the operator s objectives In order to make full use of the functions and performance provided in the MOC 120H p...

Страница 14: ...logen lamps A wide selection of measuring modes The MOC 120H provides a wide selection of measuring modes automatic operation mode timed operation mode high speed drying mode low speed drying mode ste...

Страница 15: ...tput RS 232C interface Communications Allows for data output using WindowsDirect function Storage of measurement conditions Allows for storage of 10 sets of measurement conditions Data memory Allows f...

Страница 16: ...ndle Observation window Temperature sensor Display Level Heater Wind shield Sample pan Sample pan handler Control panel Power conversion switch Power switch Power inlet Fuse holder RS 232C port Height...

Страница 17: ...andler 2 Wind shield Sample pan supporter Spoon and spatula 1 each Spare 8A fuses 2 Aluminum foil sheets 20 Power cord Three prong plug adapter Instruction manual Protection Cover SALES TECHNICAL SUPP...

Страница 18: ...ntly selected measuring mode Displays the conditions for convergence of measured values when operating in predictive or comparative mode When operating in high speed drying mode used to display the co...

Страница 19: ...on of measurement Used to confirm currently selected settings during menu selection When further settings must be specified pressing the ENTER key causes the next specifiable item choice to be display...

Страница 20: ...heet attached to pan supporter column Not level Level Bubble Height adjustment legs Level is located to the left of the control panel 4 Ensuring that the unit is level Turn the two height adjustment l...

Страница 21: ...round holes in the wind shield fit over the stays Place the wind shield firmly into position so that it does not come into contact with the black pan supporter column located at the center of the wei...

Страница 22: ...separately provided DPU 414 Printer User s Manual Some parts must be oriented in a fixed direction for assembly Note that placing parts in the wrong direction may prevent heater from closing or in err...

Страница 23: ...y first CHE5 and then a string of hyphens i e At the bottom left of the display will be displayed the currently specified power voltage If the power conversion switch is set to 100 120V pressing the S...

Страница 24: ...g is displayed and then a tone will sound again and the display will change to weight reading display mode Note It is recommended that you always turn on about half an hour before use in order to obta...

Страница 25: ...ke sure that the stability indicator is being displayed and then press the START STOP key The display will switch from a display of the weight i e grams to a percentage display and the measuring time...

Страница 26: ...lay of the results of the measurement i e moisture content to disappear and be replaced by a display of the weight of the sample after drying Note that a reset cannot be performed until the completion...

Страница 27: ...mode The temperature detected by the thermistor near the heater is used for setting and displaying temperatures How to select temperature display mode Key s used Display Operating instructions From t...

Страница 28: ...measuring mode This parameter may be used to specify the drying temperature The temperature may be set anywhere within a range of from from 30 C to 200 C in 1 degree increments 30 C to 180 C in TT mo...

Страница 29: ...that the password should be entered Use the key key and ENTER key to enter the password Follow the instructions under step 7 in 9 2 7 Specifying a password to set or delete a password The CONDITIONS d...

Страница 30: ...specified the message PASS will be displayed to indicate that the password should be entered Use the key key and ENTER key to enter the password Follow the instructions under step 7 in 9 2 7 Specifyin...

Страница 31: ...ashing press the ENTER key This will cause control to shift to measuring mode selection and for the currently specified measuring mode to begin flashing Press the SELECT key repeatedly until TIM begin...

Страница 32: ...uring is to be ended Display Key s used Operating instructions With the display of the weight in grams press the CONDITION key If a password has been specified the message PASS will be displayed to in...

Страница 33: ...ENTER key The rapid drying temperature that was previously specified will begin to flash Default setting is 180 C for TT mode 200 C for ST mode Press the key or key to set the desired rapid drying te...

Страница 34: ...is already flashing then proceed directly on to the next step When SLW flashes press the ENTER key Control will then shift to specification of low speed drying mode settings where the ending conditio...

Страница 35: ...ing mode selection and for the currently specified measuring mode to begin flashing Press the SELECT key repeatedly until STP begins to flash If STP is already flashing then proceed directly on to the...

Страница 36: ...e a drying time of 12 hours cannot be specified in this mode The maximum drying time for each step is 240 minutes When the desired ending condition begin to flash press the ENTER key This will cause t...

Страница 37: ...and you will next be required to specify the predicted value convergence range settings see Predicted value convergence range section 12 The current setting for the predicted value convergence range w...

Страница 38: ...ng mode selection and for the currently specified measuring mode to begin flashing Press the SELECT key repeatedly until PRD begins to flash If PRD is already flashing then proceed directly on to the...

Страница 39: ...accurate measurements Display Key s used Operating instructions With the display of the weight in grams press the CONDITION key If a password has been specified the message PASS will be displayed to i...

Страница 40: ...For information on how to specify the bias when operating in predictive measurement mode see 12 2 1 Calculating the bias to be specified when operating in predictive measurement mode Display Key s use...

Страница 41: ...Used to calibrate the balance For further information see 9 2 5 CAL Balance calibration Menu display Menu items Step 1 Step 2 minimum display MW Wet base 0 01 MD Dry base SOL Solid 0 1 Step 1 Step 2...

Страница 42: ...base MW has been selected When the desired measurement base flashes press the ENTER key The currently selected display begins to flash Press the SELECT key until the desired display is displayed The...

Страница 43: ...ted so that only the final results are output FIN should never be selected when graph output has been selected when operating in preparatory measuring mode as that would result in no predicted measure...

Страница 44: ...the SELECT key until the desired output interval is displayed Pressing the SELECT key here causes the menu item lit up to change from 30S A 1M A 2M A 5M A 10M A FIN and back to 30S in sequence each ti...

Страница 45: ...use the upper limit of the range of data output begin to flash Press the key or key until the desired upper limit is displayed Note that here a value of 20 has been selected When the desired upper lim...

Страница 46: ...U key Press the SELECT key until the CODE menu item is displayed Press the ENTER key Control will then shift to the specification of the sample code and the first character of the currently selected s...

Страница 47: ...2 digit value flashes Press the key or key to display the correct 2 digit year Pressing the ENTER key causes the year to be set and control to shift to the specification current month Press the key or...

Страница 48: ...sor or heater If you wish to abort a calibration already in progress press the TARE RESET key An Abort message will be displayed and the display will return to the weight in grams Scale calibration pr...

Страница 49: ...from 0 to 9 a letter from A to Z or a hyphen Note that here the letter A has been selected When the desired character is displayed press the ENTER key The first character will be specified and the sec...

Страница 50: ...been selected When the desired character is displayed press the ENTER key The first character will be set and the second character will flash Repeat steps 3 and 4 until the fourth character has been s...

Страница 51: ...ht of 120 grams or smaller Press the TARE RESET key to make the error message disappear This error is displayed when a sample is added during measurement Press the TARE RESET key to make the error mes...

Страница 52: ...disposable aluminum foil sheets are included with the unit Quantity and placement of powdered particulate and viscous sample materials Samples cannot be heated properly if they are not placed flatly P...

Страница 53: ...variation becomes smaller as time elapses The range of variation in moisture content specified in order to confirm a predicted value as the final is referred to as the predicted value convergence rang...

Страница 54: ...paratory measurements and take the average to determine the bias You should also take care in terms of the amount of the sample and the way the sample material is placed onto the sample pan They must...

Страница 55: ...ons Specify the desired predicted value convergence range In the example shown here a range of 0 5 is specified Note that the predicted value convergence range specified affects the amount of time req...

Страница 56: ...calculate the average bias The average bias may then be used to specify the bias to be used in predictive measuring mode If the bias varies greatly from one time to the next when performing repeated m...

Страница 57: ...ement when bias is 0 Note that the specified bias 0 60 does not affect the bias displayed here Automatic operation mode measurement Predicted measurement adjusted using specified bias of 0 60 15 50 i...

Страница 58: ...tory measuring mode subsections 12 2 1 and 12 2 2 Example Predicted value convergence range 0 5 Drying temperature 120 C Set the bias obtained through the procedures described in 12 2 1 and 12 2 2 sho...

Страница 59: ...calibration kit refer to its instruction manual Installation of Temperature Calibration Kit Option 1 Assembling temperature calibration kit Insert the sensor probe into the brackets on the holder as...

Страница 60: ...80 C can be selected Note that the set temperature here is the heater temperature Verify heater cover is completely closed Then press the START key It heats it up to the temperature that the heater se...

Страница 61: ...rd Dry base Measurement mode Timed operation mode Drying temperature 110 C Measurement time 10 mins Sample code Time of measurement Measurement graph Maker SHIMADZU CORP Model MOC 120H Serial number D...

Страница 62: ...ying temperature 110 C Automatic ending conditions 0 05 Predicted value convergence range 0 5 Elapsed measuring time Changes in drying temperature Changes in weight Measured value Predicted measuremen...

Страница 63: ...hen ST mode is selected Measurement mode Preparatory measuring mode Drying temperature 110 C Automatic ending conditions 0 05 Predicted value convergence range 0 5 Wet Mass 5 6892g Elapsed measuring t...

Страница 64: ...e output in order beginning from the most recently measured data To stop printing while printing is still in progress press the START STOP key Maker SHIMADZU CORP Model MOC 120H Serial number D2073000...

Страница 65: ...ethod Asynchronous communication Baud rate 2400 bps Data bits 8 bits Parity None Stop bits 1 bit Connector Female D SUB9 pins Pin assignment 5 4 3 2 1 9 8 7 6 Pin number Direction Description 1 Not us...

Страница 66: ...e and format of output on p 31 for instructions 15 2 3 Setting Up the Computer leave the balance unplugged 1 Turn ON the power to the computer and start Windows 2 Click Start choose Settings and Contr...

Страница 67: ...55 8 Select a Baud rate of 300 9 Click OK 10 Click Apply and wait 11 Click OK SALES TECHNICAL SUPPORT QAQC LAB www qclabequipment com TEL 804 318 3686...

Страница 68: ...to be used to read in data For instructions on how to use your computer operating system Microsoft Windows or software being used see the user manuals provided with them The Microsoft Windows name an...

Страница 69: ...3 byte temperature setting delimiter _Auto Stop Cond _ _ X XX 4 byte automatic ending conditions setting delimiter Timed operation format _Mode_ _Time _Setting_Temp _ _ XXX 3 byte temperature setting...

Страница 70: ...ormat _Mode_ _Predict _Setting Temp _ _ XXX 3 byte temperature setting delimiter _Auto Stop Cond _ _ X XX 4 byte automatic halting conditions setting delimiter Measurement output format tab Time min t...

Страница 71: ...difficult to remove If you find it particularly difficult to remove dirt or soiling wet a cloth in water or in water with a small amount of neutral detergent wring the cloth thoroughly and wipe Next r...

Страница 72: ...ses from the fuse holder and check if any are burned out 4 If there are no burned out fuses return the fuse holder to its original position Re place burned out fuse s with spare fuse s 8A 5 Return the...

Страница 73: ...Description AC Adapter should be separately Electronic Printer W O AC Adapter 321 64125 ordered Connection cable and Thermal Printer Paper 1 roll are included AC Adapter 120V 321 63306 05 For Electron...

Страница 74: ...232C Cable P N 321 63308 1 2 3 4 5 6 7 8 9 1 3 2 4 5 6 7 8 9 Printer Side SIGNAL G N D D sub9P Plug MOC 120H Side D sub9P Plug 1 2 3 4 5 6 7 8 9 1 2 3 6 5 4 8 7 9 PC Side SIGNAL G N D D sub9P Socket M...

Страница 75: ...SALES TECHNICAL SUPPORT QAQC LAB www qclabequipment com TEL 804 318 3686...

Страница 76: ...SALES TECHNICAL SUPPORT QAQC LAB www qclabequipment com TEL 804 318 3686...

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