Endress+Hauser Analytik Jena multi N/C, Руководство по эксплуатации, Страница: 3 / 106

multi N/C pharma UV Contents
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Contents
1 Basic Information ....................................................................................................... 7
1.1 User manual notes ............................................................................................................ 7
1.2 Intended Use ..................................................................................................................... 8
1.3 Warranty and liability ....................................................................................................... 8
2 Safety instructions ...................................................................................................... 9
2.1 Safety markings on the analyzer ..................................................................................... 9
2.2 Technical condition .......................................................................................................... 9
2.3 Requirements for the operating personnel ................................................................... 10
2.4 Safety instructions, transport and installation ............................................................. 11
2.5 Safety instructions - operation ...................................................................................... 11
2.5.1 General ............................................................................................................................ 11
2.5.2 Safety instructions - Protection against explosion and fire ......................................... 12
2.5.3 Safety instructions - electrical equipment ..................................................................... 12
2.5.4 Safety instructions for compressed gas containers and systems ................................. 12
2.5.5 Safety notes on UV radiation ......................................................................................... 13
2.5.6 Handling of auxiliary and operating materials ............................................................. 13
2.5.7 Safety instructions - service and repair ......................................................................... 14
2.6 Behavior during emergencies ........................................................................................ 14
3 Function and setup ................................................................................................... 15
3.1 System design ................................................................................................................. 15
3.1.1 UV reactor with control gear .......................................................................................... 16
3.1.2 Components for sample preparation ............................................................................. 16
3.1.3 Hose system .................................................................................................................... 17
3.1.4 Components for gas drying and cleaning ...................................................................... 20
3.1.5 NDIR detector ................................................................................................................. 22
3.1.6 Indicator and control elements, connectors .................................................................. 23
3.1.7 Reagent accessories ....................................................................................................... 24
3.1.8 Autosampler for the analyzer ........................................................................................ 24
3.2 Principle of operation ..................................................................................................... 24
3.3 Measuring method ......................................................................................................... 26
3.3.1 TC analysis ...................................................................................................................... 26
3.3.2 TOC analysis .................................................................................................................... 26
3.3.3 TIC analysis ..................................................................................................................... 27
3.3.4 NPOC analysis ................................................................................................................. 27
3.3.5 NPOC analysis according to the NPOC plus method ..................................................... 27
3.4 Calibration ....................................................................................................................... 28
3.4.1 Calibration strategies ..................................................................................................... 28
3.4.2 Day factor ........................................................................................................................ 28
3.4.3 Calibration method in multiWin .................................................................................... 29
3.4.4 Method characteristics ................................................................................................... 30
3.4.5 Other calculations ........................................................................................................... 31
3.5 Blank Values .................................................................................................................... 32
3.5.1 Blank water values ......................................................................................................... 32
3.5.2 Reagent blank value ....................................................................................................... 33
3.5.3 Eluate blank value .......................................................................................................... 34
3.6 System Suitability Test (SST) ......................................................................................... 34
4 First commissioning ................................................................................................. 36
4.1 Site requirements ........................................................................................................... 36
4.1.1 Installation conditions .................................................................................................... 36
4.1.2 Space requirement.......................................................................................................... 36
4.1.3 Energy supply .................................................................................................................. 37
4.1.4 Gas supply ....................................................................................................................... 37
4.2 Unpacking and placing the analyzer.............................................................................. 37
5 Connecting add-on devices ...................................................................................... 38