78
7.2 pH Calibration
7.2.1 Description
New sensors must be calibrated before use. Regular recalibration is also necessary. Use auto calibration instead of manual
calibration. Auto calibration avoids common pitfalls and reduces errors. The analyzer recognizes the buffers and uses
temperature-corrected pH values in the calibration. Once the Model 1056 successfully completes the calibration, it calcu-
lates and displays the calibration slope and offset. The slope is reported as the slope at 25°C.
THIS SECTION DESCRIBES HOW TO CALIBRATE THE MODEL 1056 WITH A pH SENSOR. THE FOLLOWING
CALIBRATION ROUTINES ARE COVERED.
Measure Sec.
Menu function: default
Description
pH
7.2.2
Auto Calibration -
pH 2 point buffer calibration with auto buffer recognition
7.2.3
Manual Calibration -
pH 2 point buffer calibration with manual buffer value entry
7.2.4
Entering A Known Slope Value - pH
Slope calibration with manual entry of known slope value
7.2.5
Standardization - pH
1 point buffer calibration with manual buffer value entry
A detailed flow diagram is provided at the end of Sec. 7 to guide you through the calibration routines.
TABLE 7-1
pH Calibration Routines
To calibrate pH:
1. Press the
MENU
button
2. Select Calibrate. Press
ENTER
.
3. Select
Sensor 1
or
Sensor 2
corresponding to
pH. Press ENTER.
4. Select
pH
. Press ENTER.
The following screen will appear. To calibrate pH or
Temperature scroll to the desired item and press
ENTER.
S1: 1.234µS/cm 25.0ºC
S2: 12.34pH 25.0ºC
S
N
Calibrate?
pH
Temperature
7.2.2 Auto Calibration — pH
This screen appears after selecting
pH calibration
.
Note that pH auto calibration criteria can be changed.
The following criteria can be adjusted:
Stabilization time (default 10 sec.)
Stabilization pH value (default 0.02 pH)
Type of Buffer used for AUTO CALIBRATION
(default is Standard, non-commercial buffers).
The following commercial buffer tables are recognized
by the analyzer:
Standard (NIST plus pH7)
DIN 19267
Ingold
Merck
The following screen will appear to allow adjustment of
these criteria:
S1: 1.234µS/cm 25.0ºC
S2: 12.34pH 25.0ºC
S
N
pH Cal
Buffer Cal
Standardize
Slope: 59.16mV/pH
Offset: 600 mV
S1: 1.234µS/cm 25.0ºC
S2: 12.34pH 25.0ºC
S
N
Setup
Stable Time: 10 sec
Stable Delta: 0.02 pH
Buffer: Standard
The following sub-sections show the initial display screen that appears for each calibration routine. Use the
flow
diagram for pH calibration
at the end of Sec. 7 and the live screen prompts to complete calibration.
Instruction Manual
LIQ-MAN-1056
Section 7.0: Calibration
April 2017
Содержание Rosemount 1056
Страница 1: ...Instruction Manual LIQ MAN 1056 Rev K April 2017 Rosemount 1056 Dual Input Intelligent Analyzer ...
Страница 4: ...Quick Start Guide Figure A Quick Start Guide ...
Страница 5: ...Quick Reference Guide Figure B Model 1056 Menu Tree ...
Страница 28: ...20 Instruction Manual LIQ MAN 1056 Section 2 0 Installation April 2017 ...
Страница 50: ...42 Instruction Manual LIQ MAN 1056 Section 6 0 Programming the Measurements April 2017 ...
Страница 84: ...76 Instruction Manual LIQ MAN 1056 Section 6 0 Programming the Measurements April 2017 ...
Страница 113: ...105 FIGURE 7 1 Calibrate pH Instruction Manual LIQ MAN 1056 Section 7 0 Calibration April 2017 ...
Страница 114: ...106 FIGURE 7 2 Calibrate ORP Instruction Manual LIQ MAN 1056 Section 7 0 Calibration April 2017 ...
Страница 117: ...109 FIGURE 7 5 Calibrate Oxygen Instruction Manual LIQ MAN 1056 Section 7 0 Calibration April 2017 ...
Страница 118: ...110 FIGURE 7 6 Calibrate Ozone Instruction Manual LIQ MAN 1056 Section 7 0 Calibration April 2017 ...
Страница 119: ...111 FIGURE 7 7 Calibrate Temperature Instruction Manual LIQ MAN 1056 Section 7 0 Calibration April 2017 ...
Страница 120: ...112 FIGURE 7 8 Calibrate Turbidity Instruction Manual LIQ MAN 1056 Section 7 0 Calibration April 2017 ...
Страница 121: ...113 FIGURE 7 9 Calibrate Flow Instruction Manual LIQ MAN 1056 Section 7 0 Calibration April 2017 ...
Страница 122: ...114 Instruction Manual LIQ MAN 1056 Section 7 0 Calibration April 2017 ...
Страница 124: ...116 Instruction Manual LIQ MAN 1056 Section 8 0 Return of Material April 2017 ...