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1260 SFC Binary Pump

37

Using the Pump

3

Leak and Waste Handling

Leak and Waste Handling

For details on correct installation, see separate installation documentation.

WA R N I N G

Toxic, flammable and hazardous solvents, samples and reagents

The handling of solvents, samples and reagents can hold health and safety risks.

➔

When working with these substances observe appropriate safety procedures (for
example by wearing goggles, safety gloves and protective clothing) as described in
the material handling and safety data sheet supplied by the vendor, and follow
good laboratory practice.

➔

Do not use solvents with an auto-ignition temperature below 200 °C (392 °F). Do
not use solvents with a boiling point below 56 °C (133 °F).

➔

Avoid high vapor concentrations. Always keep the temperature in the sample
compartment at least 25 K below the boiling point of the solvent used.

➔

Do not operate the instrument in an explosive atmosphere.

➔

Reduce the volume of substances to the minimum required for the analysis.

➔

Never exceed the maximum permissible volume of solvents (8 L) in the solvent
cabinet. Do not use bottles that exceed the maximum permissible volume as
specified in the usage guideline for solvent cabinet.

➔

Ground the waste container.

➔

Regularly check the filling level of the waste container. The residual free volume in
the waste container must be large enough to collect the waste liquid.

➔

To achieve maximal safety, regularly check the tubing for correct installation.

N O T E

For details, see the usage guideline for the solvent cabinet. A printed copy of the guideline
has been shipped with the solvent cabinet, electronic copies are available in the Agilent
Information Center or via the Internet.

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Содержание G4782A

Страница 1: ...Agilent Technologies Agilent InfinityLab LC Series 1260 Infinity II SFC Binary Pump User Manual...

Страница 2: ...are furnished under a license and may be used or copied only in accordance with the terms of such license Restricted Rights Legend If software is for use in the performance of a U S Government prime...

Страница 3: ...meters of the Binary Pump 4 Optimizing Performance This chapter gives information on how to optimize the performance of the Binary Pump under special operational conditions 5 Troubleshooting and Diagn...

Страница 4: ...s This chapter provides information on cables used with the Agilent InfinityLab LC Series modules 11 Hardware Information This chapter provides detailed technical information about your binary pump 12...

Страница 5: ...7 Hints for Successful Use of the Binary Pump 39 Setting up the Pump with the G4208A Instant Pilot 40 Setting up the Pump with the Instrument Control Interface 41 Solvent Information 46 Algae Growth i...

Страница 6: ...e Valve 102 Remove the Pump Head Assembly 105 Maintenance of a Pump Head without Seal Wash 107 Maintenance of a Pump Head with Seal Wash 110 Reinstall the Pump Head Assembly 114 Seal Wear in Procedure...

Страница 7: ...onnections 157 Interfaces 159 Setting the 6 bit Configuration Switch 166 Early Maintenance Feedback 170 Instrument Layout 171 12 LAN Configuration 173 What You Have to Do First 174 TCP IP parameter co...

Страница 8: ...8 1260 SFC Binary Pump Contents...

Страница 9: ...ment and Operation 10 Introduction to the Pump 10 Principle of Operation 11 Product Description 12 Features 12 Overview of the Hydraulic Path 13 Leak and Waste Handling 17 Waste Concept 21 This chapte...

Страница 10: ...ser is available for applications that require best flow stability especially at low flow rates for maximum detector sensitivity The pump is capable of delivering flow in the range of 0 1 5 mL min aga...

Страница 11: ...p to 600 bar Each channel comprises a pump assembly including pump drive pump head and outlet valve The two channels are fed into cross connector which is connected to a damping unit and a mixer A pre...

Страница 12: ...tegrated solvent selection 2 channel degasser and built in active seal wash on channel A for increased uptime Figure 2 Overview of the pump Features Fast and precise gradients the pump is the perfect...

Страница 13: ...he pump through an active inlet valve Each side of the binary pump comprises two substantially identical pump units Both pump units comprise a ball screw drive and a pump head with two sapphire piston...

Страница 14: ...itialization the pump starts operation with the set parameters for the two pump channels The inlet valve is opened and the down moving piston draws solvent into the first pump head At the same time th...

Страница 15: ...how compressibility compensation works Piston 1 draws solvent at ambient pressure The movement direction is reversed and piston 1 now compresses the solvent until the operating pressure of the HPLC sy...

Страница 16: ...ity compensation for the solvent in use Small stroke volumes generate less pressure pulsation than larger stroke volumes at the same flow rate In addition the frequency of the pressure pulsation will...

Страница 17: ...rnet All leak plane outlets are situated in a consistent position so that all Infinity and Infinity II modules can be stacked on top of each other Waste tubes are guided through a channel on the right...

Страница 18: ...18 1260 SFC Binary Pump 1 Introduction Leak and Waste Handling Figure 4 Infinity II Leak Waste Concept flexible rack installation...

Страница 19: ...1260 SFC Binary Pump 19 Introduction 1 Leak and Waste Handling Figure 5 Infinity II Single Stack Leak Waste Concept bench installation...

Страница 20: ...duction Leak and Waste Handling Figure 6 Infinity II Two Stack Leak Waste Concept bench installation The waste tube connected to the leak pan outlet on each of the bottom instruments guides the solven...

Страница 21: ...ng Waste Concept 1 Agilent recommends using the 6 L waste can with 1 Stay Safe cap GL45 with 4 ports 5043 1221 for optimal and safe waste disposal If you decide to use your own waste solution make sur...

Страница 22: ...22 1260 SFC Binary Pump 1 Introduction Leak and Waste Handling...

Страница 23: ...nt Technologies 2 Site Requirements and Specifications Site Requirements 24 Physical Specifications 27 Performance Specifications 28 This chapter provides information about site requirements and speci...

Страница 24: ...use automatic electronic fuses are implemented in the power supply WARNING Hazard of electrical shock or damage of your instrumentation can result if the devices are connected to a line voltage higher...

Страница 25: ...er connector of the instrument can be easily reached and unplugged Provide sufficient space behind the power socket of the instrument to unplug the cable WARNING Absence of ground connection The absen...

Страница 26: ...G Power cords Solvents may damage electrical cables Prevent electrical cables from getting in contact with solvents Exchange electrical cables after contact with solvents NOTE Agilent recommends that...

Страница 27: ...10 Wide ranging capability Line frequency 50 or 60 Hz 5 Power consumption 90 VA 74 W Ambient operating temperature 4 55 C 39 131 F Ambient non operating temperature 40 70 C 40 158 F Humidity 95 r h a...

Страница 28: ...eater Based on retention time at constant temperature Pressure operating range Up to 60 MPa 600 bar 8702 psi up to 5 mL min Compressibility compensation Pre defined based on mobile phase compressibili...

Страница 29: ...ea Network LAN Safety and maintenance Extensive diagnostics error detection and display through Agilent LabAdvisor leak detection safe leak handling leak output signal for shutdown of the pumping syst...

Страница 30: ...30 1260 SFC Binary Pump 2 Site Requirements and Specifications Performance Specifications...

Страница 31: ...the Pump with the G4208A Instant Pilot 40 Setting up the Pump with the Instrument Control Interface 41 Overview 41 Setup of Basic Pump Parameters 41 Pump Control 42 Auxiliary Pump Parameters 43 Data C...

Страница 32: ...32 1260 SFC Binary Pump 3 Using the Pump Magnets Magnets 1 This stack exemplarily shows the magnets positions in the modules...

Страница 33: ...1260 SFC Binary Pump 33 Using the Pump 3 Turn on off Turn on off 1 Plug in power cord 2 Power switch 1 On 2 Off 3 Plug off the module...

Страница 34: ...e 2 Run mode 3 Not ready Waiting for a specific pre run condition to be reached or completed 4 Error mode interrupts the analysis and requires attention for example a leak or defective internal compon...

Страница 35: ...fer applications were used Inspect solvent filters for dirt or blockages Clean or exchange if no flow is coming out of the solvent line when removed from the degasser inlet Power up Shut down the pump...

Страница 36: ...volatile additives How to deal with solvents Use clean bottles only Exchange water based solvents daily Select solvent volume to be used up within 1 2 days Use only HPLC grade solvents and water filte...

Страница 37: ...ons Always keep the temperature in the sample compartment at least 25 K below the boiling point of the solvent used Do not operate the instrument in an explosive atmosphere Reduce the volume of substa...

Страница 38: ...ing Waste Concept 1 Agilent recommends using the 6 L waste can with 1 Stay Safe cap GL45 with 4 ports 5043 1221 for optimal and safe waste disposal If you decide to use your own waste solution make su...

Страница 39: ...Check purge valve frit and column frit in regular time intervals A blocked purge valve frit can be identified by black yellow or greenish layers on its surface or by a pressure greater than 10 bar in...

Страница 40: ...ith the G4208A Instant Pilot Generic operation of the G4208A Instant Pilot is covered in the Agilent Instant Pilot G4208A User s Guide G4208 90006 Details about setting up module specific parameters c...

Страница 41: ...run manually useful for method development Post Time off 99999 min Time between the end of a run and the start of the next Used for column equilibration after a gradient Pressure Limits Max 0 600 bar...

Страница 42: ...n will show up in method printouts etc Timetable max number of lines depends on free space in pump memory Use the timetable to build solvent gradients flow gradients or combinations of both Gradients...

Страница 43: ...scription Maximum Flow Gradient 0 1 100 mL min default 100 mL min With this parameter flow rate changes can be ramped up and down slowly to avoid pressure shocks to the column The default value is 100...

Страница 44: ...sure data curve is generated from the pressure sensor readings while A B and flow are calculated from the method settings of the pump CAUTION The bottle filling feature fails if multiple solvent inlet...

Страница 45: ...volume in liter which considers the position of the solvent inlet and size shape of the solvent bottle such that no air is drawn if the actual volume gets close to this limit Turn pump off default unc...

Страница 46: ...ions for the pH range given for different materials like flow cells valve materials etc and recommendations in subsequent sections Materials in Flow Path Following materials are used in the flow path...

Страница 47: ...f UHPLC systems solvents solvent mixtures and samples Information can also not be generalized due to catalytic effects of impurities like metal ions complexing agents oxygen etc Apart from pure chemic...

Страница 48: ...compatibility of PEEK Polyimide Agilent uses semi crystalline polyimide for rotor seals in valves and needle seats in autosamplers One supplier of polyimide is DuPont which brands polyimide as Vespel...

Страница 49: ...if your chromatography method allows by phosphoric acid or phosphate buffer which are less corrosive against stainless steel Halogenated solvents or mixtures which form radicals and or acids for exam...

Страница 50: ...with ammonia 10 Diamond Like Carbon DLC Diamond Like Carbon is inert to almost all common acids bases and solvents There are no documented incompatibilities for HPLC applications Fused silica and Quar...

Страница 51: ...ts like halogenated hydrocarbons TFE PDD copolymer tubings which are used in all Agilent degassers except 1322A are not compatible with fluorinated solvents like Freon Fluorinert or Vertrel They have...

Страница 52: ...adient problems or a complete failure of the pump Small pore high pressure solvent filters usually placed before the injector to plug resulting in high system pressure PTFE frits blockage leading to i...

Страница 53: ...e solvent Place a layer of argon on top of your solvent Avoid exposure of the solvent bottle to direct sunlight Checking the Solvent Filters The solvent filters are located on the low pressure side of...

Страница 54: ...apillary columns can be damaged by nitric acid Replace the filter WARNING When opening capillary or tube fittings solvents may leak out The handling of toxic and hazardous solvents and reagents can ca...

Страница 55: ...for valve balls which is a conductive ceramic and replaces non conductive ruby balls The balls do not charge up electrostatically and show good performance in normal phase The valves are marked with N...

Страница 56: ...ls have a limited life time when used with normal phase solvents and sapphire pistons Agilent recommends a maximum pressure of 200 bar for this combination which shall also be applied for pressure tes...

Страница 57: ...al Hints for the Vacuum Degasser 58 When to Use the Active Seal Wash Option 59 How to Optimize the Compressibility Compensation Setting 60 Optimization of Legacy Compressibility Settings 60 This chapt...

Страница 58: ...is used with maximum sensitivity in the low UV wavelength range Your application requires highest injection precision Your application requires highest retention time reproducibility flow rates below...

Страница 59: ...ash option comprises a peristaltic pump secondary seals gaskets seal holders and tubing for both pump heads A bottle of premixed water isopropanol 90 10 vol is placed in the solvent cabinet and connec...

Страница 60: ...ue for the actual pump pressure Compressibility data for the most common solvents is readily available in the pump firmware The compensation algorithm is so powerful that the damper and mixer can be r...

Страница 61: ...table Use degassed solvent only Check the tightness of the system with the pressure test see 3 Your pump must be connected to an Agilent data system or Instant Pilot the pressure and ripple can be mon...

Страница 62: ...Binary Pump 4 Optimizing Performance How to Optimize the Compressibility Compensation Setting Methanol 120 1 Propanol 100 Toluene 87 Water 46 Table 8 Solvent Compressibility Solvent pure Compressibili...

Страница 63: ...Binary Pump Agilent Technologies 5 Troubleshooting and Diagnostics Overview of the Module s Indicators and Test Functions 64 Agilent Lab Advisor Software 65 Overview of the troubleshooting and diagnos...

Страница 64: ...check of the operation of the module Error Messages In the event of an electronic mechanical or hydraulic failure the module generates an error message in the user interface For each message a short...

Страница 65: ...finity Series and Agilent InfinityLab LC Series instrument The Lab Advisor Advanced features can be unlocked by purchasing a license key and include real time monitoring of instrument actuals all vari...

Страница 66: ...66 1260 SFC Binary Pump 5 Troubleshooting and Diagnostics Agilent Lab Advisor Software...

Страница 67: ...nsor Open 74 Compensation Sensor Short 74 Fan Failed 75 Open Cover 76 Module Error Messages 77 Solvent Zero Counter 77 Pressure Above Upper Limit 77 Pressure Below Lower Limit 78 Pressure Signal Missi...

Страница 68: ...Pump Head Missing 86 Index Limit 86 Index Adjustment 87 Index Missing 87 Stroke Length 88 Initialization Failed 88 This chapter describes the meaning of error messages and provides information on pro...

Страница 69: ...LEDs get red and the run will be stopped Depending on the module type this stop is implemented differently For example for a pump the flow will be stopped for safety reasons For a detector the lamp wi...

Страница 70: ...as present during a sequence or multiple injection run for a period longer than the timeout threshold Check the logbook for the occurrence and source of a not ready condition Restart the analysis wher...

Страница 71: ...f one or more of the modules is no longer recognized as being connected to the system the error message is generated Probable cause Suggested actions 1 Not ready condition in one of the instruments co...

Страница 72: ...k sensor is cooled by the solvent This changes the resistance of the leak sensor which is sensed by the leak sensor circuit on the main board Probable cause Suggested actions 1 Loose fittings Ensure a...

Страница 73: ...ent to change within defined limits If the current increases above the upper limit the error message is generated Probable cause Suggested actions 1 Leak sensor not connected to the Power Switch board...

Страница 74: ...error message is generated Compensation Sensor Short Error ID 0080 The ambient compensation sensor NTC on the main board in the module has failed open circuit The resistance across the temperature co...

Страница 75: ...time the error message is generated This limit is given by 2 revolutions second for longer than 5 seconds Depending on the module assemblies e g the lamp in the detector are turned off to assure that...

Страница 76: ...message is generated Probable cause Suggested actions 1 The top foam was removed during operation Please contact your Agilent service representative 2 Foam not activating the sensor Please contact yo...

Страница 77: ...matches the actual bottle filling and set the shutoff limit to a reasonable value e g 100 mL for 1 L bottles Probable cause Suggested actions 1 Upper pressure limit set too low Ensure the upper pressu...

Страница 78: ...lower pressure limit is set to a value suitable for the analysis 2 Air bubbles in the mobile phase Make sure that the degasser is in flow path and works correctly Purge the module Ensure solvent inle...

Страница 79: ...efore and after each switching cycle If the voltages are outside expected limits the error message is generated Probable cause Suggested actions 1 Solvent selection valve disconnected Please contact y...

Страница 80: ...mp configuration The binary pump is assigned its configuration at the factory If the active inlet valve and pump encoder of channel B are disconnected and the binary pump is rebooted the error message...

Страница 81: ...lectronic fuse to open Probable cause Suggested actions 1 Defective solvent selection valve Restart the pump If the error message appears again exchange the solvent selection valve 2 Defective connect...

Страница 82: ...continually monitors the temperature of the drive circuits on the main board If excessive current is being drawn for long periods the temperature of the circuits increases If the temperature exceeds...

Страница 83: ...hes the maximum limit the module is switched off and the error message is generated Probable cause Suggested actions 1 Flow path blockage in front of the damper Ensure the capillaries and frits betwee...

Страница 84: ...n the module is missing or defective The processor checks the presence of the pump encoder connector every 2 s If the connector is not detected by the processor the error message is generated Probable...

Страница 85: ...e to take control of the phase sequencing with the commutator If the rotor is unable to move or if the C position cannot be reached the error message is generated Probable cause Suggested actions 1 Me...

Страница 86: ...hort pump During initialization the first piston is moved to the mechanical stop After reaching the mechanical stop the piston reverses direction until the encoder index position is reached If the ind...

Страница 87: ...dule was not found during initialization During initialization the first piston is moved to the mechanical stop After reaching the mechanical stop the piston reverses direction until the encoder index...

Страница 88: ...rated Initialization Failed Error ID 2207 2217 Initialization Failed Pump channel A B Initialization Failed Pump channel B The module failed to initialize successfully within the maximum time window A...

Страница 89: ...89 1260 SFC Binary Pump Agilent Technologies 7 Test Functions and Calibration Pump Leak Rate Test 90 This chapter explains all test functions that are available for the binary pump...

Страница 90: ...7 Test Functions and Calibration Pump Leak Rate Test Pump Leak Rate Test Introduction The Pump Leak Rate Test is used for verifying the internal tightness of the pump and helps identifying parts which...

Страница 91: ...O Ring on the Purge Valve 102 Remove the Pump Head Assembly 105 Maintenance of a Pump Head without Seal Wash 107 Maintenance of a Pump Head with Seal Wash 110 Reinstall the Pump Head Assembly 114 Seal...

Страница 92: ...enance Introduction to Maintenance The pump is designed for easy maintenance The most frequent maintenance procedures such as piston seal replacement and purge valve frit exchange can be done from the...

Страница 93: ...p edged parts of the equipment may cause injuries To prevent personal injury be careful when getting in contact with sharp metal areas WARNING Toxic flammable and hazardous solvents samples and reagen...

Страница 94: ...e board by the edges and do not touch the electrical components Always use ESD protection for example an ESD wrist strap when handling electronic boards and components CAUTION Safety standards for ext...

Страница 95: ...cloth slightly dampened with water or a solution of water and mild detergent WARNING Liquid dripping into the electronic compartment of your module can cause shock hazard and damage the module Do not...

Страница 96: ...and can be accessed from the front simple repairs Replacement of valve or filters don t require to remove the pump from the system stack Figure 7 Overview of Maintenance and Simple Repairs 1 2 3 4 5...

Страница 97: ...ly on page 105 During yearly maintenance Necessary to get access to pump seals and pistons Maintenance of a Pump Head without Seal Wash on page 107 Yearly or if pump performance indicates seal wear Le...

Страница 98: ...ed p n Description 5067 5746 Door Assembly Infinity 180 Right 5067 5745 Door Assembly Infinity 180 Left NOTE The figures shown in this procedure exemplarily show the Infinity II Multisampler module Th...

Страница 99: ...Remove and Install Doors 1 Press the release buttons and pull the front door out 2 For the Installation of the front door Insert the hinges into their guides and move the door in until the release bu...

Страница 100: ...required p n Description 8710 0510 Wrench open 1 4 5 16 inch 8710 1924 Wrench open 14 mm Pair of tweezers OR Toothpick Parts required p n Description Frits Purge Valve 5067 4728 Seal cap Preparations...

Страница 101: ...oothpick remove the frit 4 Place a new frit into the purge valve with the orientation of the frit as shown below slit in frit points to the front Reinstall the seal cap including the gold seal 5 Inser...

Страница 102: ...Toothpick Parts required p n Description 1 5067 6595 1260 PV O ring FKM 5 pack 1 01018 22707 PTFE frits pack of 5 OPTIONAL 1 5067 4728 Seal cap OPTIONAL Preparations Switch off pump at the main power...

Страница 103: ...e Purge Valve Body 6 Place the mounting ring on the screw and push down the o ring 7 Place a new frit into the purge valve with the orientation of the frit as shown below slit in frit points to the fr...

Страница 104: ...lace the O Ring on the Purge Valve 8 Push the screw up and guide the o ring into the gap 9 Install the purge valve to the pump make sure that you do not turn the Purge Valve Body when the screw is fix...

Страница 105: ...0240 Hex driver slitted Preparations Switch off the pump at the main power switch CAUTION Damage of the pump drive Starting the pump when the pump head is removed may damage the pump drive Never start...

Страница 106: ...nce Remove the Pump Head Assembly 1 Open the doors 2 Disconnect the capillaries Beware of leaking solvents 3 Using a 4 mm hexagonal key stepwise loosen and remove the two pump head screws 4 Remove the...

Страница 107: ...l PTFE carbon filled black pack of 2 default OR 1 0905 1420 PE seals pack of 2 1 5067 4695 Sapphire piston Preparations Switch off the pump at the main power switch Open the doors of the module Use an...

Страница 108: ...carefully pull the pump housing away from the piston housing 3 Remove the support rings from the piston housing 4 Lift the housing away from the pistons 5 Check the piston surface and remove any depos...

Страница 109: ...sert tool insert new seals into the pump head 8 Place the support rings on the piston housing Note the correct position of the pins on the support ring 9 Place the pump housing onto the piston housing...

Страница 110: ...1718 Wash seal PTFE 5062 2484 Gasket seal wash pack of 6 5067 4695 Sapphire piston 0905 1719 PE Seal Preparations Switch off the pump at the main power switch Open the doors of the module Use an opti...

Страница 111: ...t ring assembly 5 Lift the housing away from the pistons 6 Check the piston surface and remove any deposits or layers clean the piston surface with abrasive paper and rinse with 2 propanol Replace pis...

Страница 112: ...w wash seal spring pointing upwards into the recess of the support ring 11 Place a seal wash gasket in the recess of the support ring Use a matching orientation of gasket and support ring Put the seal...

Страница 113: ...1260 SFC Binary Pump 113 Maintenance 8 Maintenance of a Pump Head with Seal Wash 15 Tighten the lock screw 16 Install the pump head see...

Страница 114: ...d Assembly When When reassembling the pump Tools required 3 mm hexagonal key 4 mm hexagonal key 1 Slide the pump head assembly onto the pump drive 2 Using a 4 mm hexagonal key tighten the pump head sc...

Страница 115: ...m for 5 min with isopropanol at a flow rate of 2 mL min 5 Close the purge valve set the flow to a value that gives a pressure of 350 bar Pump 15 min at this pressure to wear the seals in The pressure...

Страница 116: ...n Description 5065 4445 Peristaltic pump with Pharmed tubing Preparations Switch off pump at the main power switch Open the doors 1 Remove the wash solvent tubings from the support ring outlet and fr...

Страница 117: ...eal Wash Cartridge 3 Put the new peristaltic pump cartridge onto the rod of the pump motor and push the plastic clips into the module housing 4 Connect the peristaltic pump tubes to the support rings...

Страница 118: ...ubing assembly i d 6 mm o d 9 mm 1 2 m to waste approximately 85 mm required 1 Open the doors 2 Press the Leak Adapter down and remove it together with the tubing 3 Install the Leak Adapter by pressin...

Страница 119: ...ive inlet valve G4302 60066 Inlet Valve SFC Preparations Switch off the pump at the main power switch 1 Disconnect the solvent inlet tube at the inlet valve beware of leaking solvents 2 Using a 14 mm...

Страница 120: ...mm Parts required p n Description 1 G1312 60167 Outlet valve Channel A 2 G1312 60067 Outlet valve Channel B Preparations Switch off the pump at the main power switch 1 Using a inch wrench disconnect...

Страница 121: ...1260 SFC Binary Pump 121 Maintenance 8 Exchange the Outlet Valve 3 Reinstall the outlet valve and tighten it using a torque wrench approx 12 Nm 4 Reconnect the capillary approx 12 Nm...

Страница 122: ...on Valve Upgrade Kit Preparations Switch off the pump at the main power switch 1 Lift solvent bottles out of the solvent cabinet and place them on the table Disconnect the solvent tubes from the solve...

Страница 123: ...election valve 6 Tighten the screws of the valve holder 7 Reconnect all tubings to the solvent selection valve NOTE After an exchange of the valve it may be required to pump several mL of solvent befo...

Страница 124: ...or this module When The installation of newer firmware might be necessary if a newer version solves problems of older versions or to keep all systems on the same validated revision The installation of...

Страница 125: ...Pump Head Assembly Channel B 128 Pump Head Assembly Channel A 130 Outlet Valve 132 Purge Valve Assembly 133 HPLC System Tool Kit 134 Active Seal Wash Option 135 Solvent Cabinet 136 Bottle Head Assembl...

Страница 126: ...egasser to Channel B 6 1 G1312 87305 Capillary SSL 0 17 x 150 mm pressure sensor to damper 7 13 1 G1316 87300 Capillary ST 0 17 mm x 90 mm S S 8 1 G1312 87300 Absorber capillary 9 1 G7111 60061 Purge...

Страница 127: ...1260 SFC Binary Pump 127 Parts and Materials for Maintenance 9 Hydraulic Path with Solvent Selection Valve Figure 8 Hydraulic Path with Solvent Selection Valve 1 2 3 4 5 6 7 8 9 10 11 12 13...

Страница 128: ...20 60015 Support ring including backup ring 5 1 0905 1503 Pump seals PTFE PumpHead B 6 1 G1312 25260 Pump housing 7 1 G1312 60066 Passive inlet valve 8 1 G7111 60061 Purge valve 9 1 0515 2118 Pump hea...

Страница 129: ...1260 SFC Binary Pump 129 Parts and Materials for Maintenance 9 Pump Head Assembly Channel B Figure 9 Pump Head Assembly Without Seal Wash 1 2 3 4 5 6 7 8 9 10 11 12 13...

Страница 130: ...G4220 60016 Seal holder including backup ring 7 0905 1719 PE Seal 8 G1312 25260 Pump housing 9 G4302 60066 Inlet Valve SFC 10 0515 2118 Pump head screw M5 60 mm 11 G1312 60001 Adapter 12 5042 1303 Lo...

Страница 131: ...1260 SFC Binary Pump 131 Parts and Materials for Maintenance 9 Pump Head Assembly Channel A Figure 10 Pump Head Assembly with Seal Wash Option 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15...

Страница 132: ...60 SFC Binary Pump 9 Parts and Materials for Maintenance Outlet Valve Outlet Valve Figure 11 Outlet valve p n Description G1312 60067 Outlet valve 1220 1260 G1312 60167 1260 Infinity Outlet Valve Type...

Страница 133: ...Parts and Materials for Maintenance 9 Purge Valve Assembly Purge Valve Assembly Item p n Description 1 G7111 60061 Purge valve 2 01018 22707 PTFE frits pack of 5 3 5067 4728 Seal cap 5067 6595 1260 PV...

Страница 134: ...24 Wrench open 14 mm 01018 23702 Insert tool 0100 1681 Syringe adapter luer barb 8710 2394 Hex key 9 64 inch 15 cm long T handle 8710 1534 Wrench 4 mm both ends open end 8710 2409 Wrench open end 5 16...

Страница 135: ...rt ring seal wash 2 0515 1508 Screws for Seal Wash Pump Motor 1 5065 9978 Tubing 1 mm i d 3 mm o d silicone 5 m 4 0905 1175 Wash seal PTFE 1 5063 6589 Piston seal PTFE carbon filled black pack of 2 de...

Страница 136: ...0 SFC Binary Pump 9 Parts and Materials for Maintenance Solvent Cabinet Solvent Cabinet For details refer to Usage Guideline for the Solvent Cabinet 01200 90150 p n Description 5067 5760 Solvent Cabin...

Страница 137: ...embly Bottle Head Assembly p n Description G7120 60007 Bottle Head Assembly 5063 6598 Ferrules with lock ring 10 Pk 5063 6599 Tube screw 10 Pk Wire marker 5062 2483 Tube PTFE 1 5 mm x 5 m 3 mm od 5062...

Страница 138: ...s Figure 12 Cover Parts Item p n Description 1 5067 5746 Door Assembly Infinity 180 Right 2 5067 5745 Door Assembly Infinity 180 Left 3 5043 1354 Name Plate 1290 Infinity 2 4 G7104 68713 Cabinet Kit 1...

Страница 139: ...5181 1519 CAN cable Agilent module to module 1 m 1 5500 1246 Capillary ST 0 17 mm x 500 mm SI SI 1 5500 1217 Capillary ST 0 17 mm x 900 mm SI SX ps ps 3 5063 6527 Tubing assembly i d 6 mm o d 9 mm 1 2...

Страница 140: ...140 1260 SFC Binary Pump 9 Parts and Materials for Maintenance Accessory Kit...

Страница 141: ...0 Identifying Cables Cable Overview 142 Analog Cables 144 Remote Cables 146 CAN LAN Cables 150 RS 232 Cable Kit 151 Agilent 1200 Module to Printer 152 This chapter provides information on cables used...

Страница 142: ...ription 35900 60750 Agilent 35900A A D converter 01046 60105 Analog cable BNC to general purpose spade lugs p n Description 5188 8029 ERI to general purpose 5188 8044 Remote Cable ERI ERI 5188 8045 Re...

Страница 143: ...int to point connection p n Description RS232 61601 RS 232 cable 2 5 m Instrument to PC 9 to 9 pin female This cable has special pin out and is not compatible with connecting printers and plotters It...

Страница 144: ...these cables provides a BNC connector to be connected to Agilent modules The other end depends on the instrument to which connection is being made Agilent Module to 35900 A D converters p n 35900 6075...

Страница 145: ...es Agilent Module to BNC Connector Agilent Module to General Purpose p n 8120 1840 Pin BNC Pin Agilent module Signal Name Shield Shield Analog Center Center Analog p n 01046 60105 Pin Pin Agilent modu...

Страница 146: ...Color code Enhanced Remote Classic Remote Active TTL 1 white IO1 START REQUEST Low 2 brown IO2 STOP Low 3 green IO3 READY High 4 yellow IO4 POWER ON High 5 grey IO5 NOT USED 6 pink IO6 SHUT DOWN Low...

Страница 147: ...RI Signal Pin ERI Active TTL 10 GND 10 1 Start Request 1 Low 2 Stop 2 Low 3 Ready 3 High 5 Power on 5 High 4 Future 4 6 Shut Down 6 Low 7 Start 7 Low 8 Prepare 8 Low Ground Cable Shielding NC p n 5188...

Страница 148: ...chnologies APG Analytical Products Group remote connector to be connected to Agilent modules The other end depends on the instrument to be connected to Table 11 5188 8057 ERI to APG and RJ45 p n 5188...

Страница 149: ...are run Low 3 Gray 3 Gray Start Low 4 Blue 4 Blue Shut down Low 5 Pink 5 Pink Not connected 6 Yellow 6 Yellow Power on High 7 Red 7 Red Ready High 8 Green 8 Green Stop Low 9 Black 9 Black Start reques...

Страница 150: ...lent modules CAN or LAN connectors CAN Cables LAN Cables p n Description 5181 1516 CAN cable Agilent module to module 0 5 m 5181 1519 CAN cable Agilent module to module 1 m p n Description 5023 0203 C...

Страница 151: ...601 RS 232 cable 2 5 m Instrument to PC 9 to 9 pin female This cable has special pin out and is not compatible with connecting printers and plotters It s also called Null Modem Cable with full handsha...

Страница 152: ...nt 1200 Module to Printer Agilent 1200 Module to Printer To connect a USB Flash Drive use a USB OTG cable with Mini B plug and A socket p n Description 5188 8050 USB A M USB Mini B 3 m PC Module 5188...

Страница 153: ...ormation ALL 158 Rear view of the module 158 Interfaces 159 Overview Interfaces 160 ERI Enhanced Remote Interface 162 USB Universal Serial Bus 165 Setting the 6 bit Configuration Switch 166 Special Se...

Страница 154: ...RS 232C memory management ability to update the firmware of the main system Main System Its properties are the complete communication capabilities CAN LAN USB and RS 232C memory management ability to...

Страница 155: ...for example 1315B for the G1315B DAD R the firmware revision for example A for G1315B or B for the G1315C DAD VVV is the revision number for example 650 is revision 6 50 XXX is the build number of the...

Страница 156: ...revision For example a G1315C DAD SL cannot be downgraded below firmware revision B 01 02 or to a A xx xx Some modules can be re branded e g G1314C to G1314B to allow operation in specific control so...

Страница 157: ...used to control the module from a computer through a LAN connection This connector is activated and can be configured with the configuration switch With the appropriate software the USB connector may...

Страница 158: ...e module Figure 14 Rear view of the pump electrical connections and label CCXZZ00000 Format CC Country of manufacturing DE Germany JP Japan CN China X Alphabetic character A Z used by manufacturing ZZ...

Страница 159: ...Pump 2 Yes Yes No No E G7112B Binary Pump 2 Yes Yes No No E G7120A High Speed Pump 2 No Yes Yes 1 A Samplers G7129A B Vialsampler 2 Yes Yes No No E G7167A B Multisampler 2 Yes Yes No No E Detectors G7...

Страница 160: ...369B C LAN Interface or they have an on board LAN interface e g detectors G1315C D DAD and G1365C D MWD This interface allows the control of the module system via a PC with the appropriate control sof...

Страница 161: ...r technique To provide maximum safety within a distributed analysis system one line is dedicated to SHUT DOWN the system s critical parts in case any module detects a serious problem To detect whether...

Страница 162: ...injection cycle for example by start key on any module Receiver is the autosampler 2 STOP L Request to reach system ready state as soon as possible for example stop run abort or finish and stop injec...

Страница 163: ...ns eight individual programmable input output pins In addition it provides 24 V power and 5 V power and a serial data line to detect and recognize further add ons that could be connected to this inter...

Страница 164: ...ure Use This serial line can be used to read out an EPROM or write into an EPROM of a connected ERI device The firmware can detect the connected type of device automatically and update information in...

Страница 165: ...ware command defined turn on off For devices that need higher power Class 0 0 5 A maximum 12 W Class 1 1 0 A maximum 24 W Class 2 2 0 A maximum 48 W Class depends on hosting module s internal power ov...

Страница 166: ...ngs provide configuration parameters for LAN and instrument specific initialization procedures All modules with FUSION electronics Default is ALL switches DOWN best settings Default IP address for LAN...

Страница 167: ...en from non volatile memory 0 n a 2 2 not assigned Always keep these switches on position 0 off n a LAN Init Mode n a Use Default IP Address3 3 Default IP Address is 192 168 254 11 0 0 0 0 0 Use Stor...

Страница 168: ...to bring the module into a defined mode with default parameter settings Boot Main System Revert to Default Data The instrument will boot to main mode and changes to the module s default parameter May...

Страница 169: ...15 Boot Resident Forced Coldstart SW1 SW2 SW3 SW4 SW5 SW6 Init Mode 1 0 0 0 0 0 Boot Main System Keep Data 1 1 0 0 0 0 Boot Resident System Keep Data 1 0 0 0 0 1 Boot Main System Revert to Default Dat...

Страница 170: ...the limit is exceeded Some counters can be reset to zero after the required maintenance procedure Using the EMF Counters The user settable EMF limits for the EMF Counters enable the early maintenance...

Страница 171: ...ed in a metal inner cabinet which is enclosed by a plastic external cabinet The advantages of this packaging technology are virtual elimination of fixing screws bolts or ties reducing the number of co...

Страница 172: ...172 1260 SFC Binary Pump 11 Hardware Information Instrument Layout...

Страница 173: ...rameter configuration 175 Configuration Switches 176 Initialization Mode Selection 177 Dynamic Host Configuration Protocol DHCP 179 General Information DHCP 179 Setup DHCP 180 Manual Configuration 182...

Страница 174: ...on a label at the rear of the module underneath the configuration switch see Figure 18 on page 174 Figure 17 MAC Label 2 Connect the instrument s LAN interface see Figure 18 on page 174 to the PC net...

Страница 175: ...ing the so called Dynamic Host Configuration Protocol This mode requires a LAN onboard Module or a G1369C LAN Interface card see Setup DHCP on page 180 by manually setting the parameters using Telnet...

Страница 176: ...he configuration switch can be accessed at the rear of the module Figure 19 Location of Configuration switch example shows a G7114A B VWD The module is shipped with all switches set to OFF as shown ab...

Страница 177: ...is selected the parameters are taken from the non volatile memory of the module The TCP IP connection will be established using these parameters The parameters were configured previously by one of th...

Страница 178: ...he session select the initialization mode Using Stored power on again and establish the TCP IP connection using the new parameters When the module is wired to the PC directly e g using a cross over ca...

Страница 179: ...ome the active parameters immediately They are not stored to the non volatile memory of the card Besides requesting the network parameters the card also submits its hostname to the DHCP Server The hos...

Страница 180: ...firmware B 06 40 or above or modules with D firmware All modules should use latest firmware from the same set 1 Note the MAC address of the LAN interface provided with G1369C LAN Interface Card or Ma...

Страница 181: ...mStation Edition Lab Advisor Firmware Update Tool and use MAC address as host name e g 0030d3177321 The LC system should become visible in the control software see Note in section General Information...

Страница 182: ...mandatory to make the stored parameters become the active parameters given that the initialization mode selection switches are allowing it Figure 24 Manual Configuration Principle With Telnet Whenever...

Страница 183: ...e Figure 25 Telnet Starting a session where IP address may be the assigned address from a Bootp cycle a configuration session with the Handheld Controller or the default IP address see Configuration S...

Страница 184: ...configuration parameter you are defining and value refers to the definitions you are assigning to that parameter Each parameter entry is followed by a carriage return 5 Use the and press Enter to lis...

Страница 185: ...AC address initialization mode Initialization mode is Using Stored active TCP IP settings TCP IP status here ready connected to PC with controller software e g Agilent ChemStation here not connected F...

Страница 186: ...ration parameters type exit and press Enter to exit with storing parameters Figure 30 Closing the Telnet Session NOTE If the Initialization Mode Switch is changed now to Using Stored mode the instrume...

Страница 187: ...nstrument 189 Do Not Operate in an Explosive Atmosphere 190 Do Not Remove the Instrument Cover 190 Do Not Modify the Instrument 190 In Case of Damage 190 Solvents 191 Safety Symbols 192 Waste Electric...

Страница 188: ...y for the customer s failure to comply with these requirements Safety Standards This is a Safety Class I instrument provided with terminal for protective earthing and has been manufactured and tested...

Страница 189: ...ty or EMC regulations Make all connections to the unit before applying power NOTE Note the instrument s external markings described under Safety Symbols on page 192 WARNING Missing electrical ground E...

Страница 190: ...mable gases or fumes Explosion hazard Do not operate the instrument in the presence of flammable gases or fumes WARNING Instrument covers removed Electrical shock Do Not Remove the Instrument Cover On...

Страница 191: ...compartment at least 25 K below the boiling point of the solvent used Do not operate the instrument in an explosive atmosphere Reduce the volume of substances to the minimum required for the analysis...

Страница 192: ...pecifications of refrigerant charge capacity carbon dioxide equivalent CDE and global warming potential GWP see instrument label Confirms that a manufactured product complies with all applicable Europ...

Страница 193: ...jects that could be damaged by strong magnetic fields Indicates a pinching or crushing hazard Indicates a piercing or cutting hazard Table 21 Symbols WARNING A WARNING alerts you to situations that co...

Страница 194: ...arting with 13 August 2005 NOTE This product complies with the WEEE Directive 2002 96 EC marking requirements The affixed label indicates that you must not discard this electrical electronic product i...

Страница 195: ...protection against radio interference All cables are in compliance with safety or EMC regulations Test and Measurement If test and measurement equipment is operated with unscreened cables or used for...

Страница 196: ...tatement is provided to comply with the requirements of the German Sound Emission Directive of 18 January 1991 This product has a sound pressure emission at the operator position 70 dB Sound Pressure...

Страница 197: ...Pump 197 Appendix 13 Agilent Technologies on the Internet Agilent Technologies on the Internet For the latest information on products and services visit our worldwide web site on the Internet at http...

Страница 198: ...dimensions 27 doors install 98 remove 98 dual piston in series design 11 E electrical connections descriptions of 157 electronic fuse of SSV open 81 electronic waste 194 electrostatic discharge ESD 9...

Страница 199: ...figuration with telnet 182 manual configuration 182 TCP IP parameter configuration 175 using default 178 using stored 177 what you have to do first 174 174 leak sensor open 73 leak sensor short 73 lea...

Страница 200: ...16 seal wash wash solvent 59 when to use 59 seals 39 serial number information 158 servo restart failed 85 shutdown 70 sieve 97 120 site requirements 23 power cords 25 solvent cabinet 39 136 solvent f...

Страница 201: ...1260 SFC Binary Pump 201 Index W wash solvent 59 waste electrical and electronic equipment 194 WEEE directive 194 weight 27 wrong pump configuration 80...

Страница 202: ...In This Book This manual contains The manual describes the following Introduction Site Requirements and Specifications Using the Pump Optimizing Performance Troubleshooting and Diagnostics Error Info...

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