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29 

5. Handling Precautions 

Precautions during operation 

 

(1)

 

Be sure to connect the earth wire when connecting power supply. 

(2)

 

Securely connect with ADL311S or GB210A. 

(3)

 

Using the blower at a low air amount may cause a malfunction. Set it at least 0.2m

3

/min or 

more. 

(4)

 

Flow  meter  for  the  oxygen  sensor  (small)  and  a  flow  meter  for  introducing  N2  (large)  are 
located inside the left side door. Adjust the flow meter for the oxygen sensor to 0.2L/min at 

AIR IN during preparations and adjust the flow meter for introducing N

2

 to 35

40L/min when 

performing N2 IN. 

(5)

 

When  this  unit  is  connected  to  ADL311S  or  GB210A,  the  blower  of  ADL311S  or  GB210A 
cannot be used. Use the dial of GAS410 for setting an air amount. 

(6)

 

Make sure that the glass chamber is fixed at the specified position without any play. 
Check the connecting assembly when oxygen concentration will not decrease properly or its 
increase speed has risen. 
When  a  defect  at  a  connection  of  pipes  or  at  a  packing  is  suspected,  repair  or  replace  the 
relevant part. 

(7)

 

Do not heat up the temperature around outlet over 100 Celsius degree, for the material of the 
suction/exhaust  hose,  material  of  the  filter,  and  performance  of  the  blower  may  be 
deteriorated.. 

(8)

 

Check the glass chambers are fixed to the specified position with no gap, and then turn on the 
switches of blower and heater. 

(9)

 

The unit is not explosion proof. You cannot use this unit in an atmosphere where a flammable 
gas exists or at a place where a flammable gas may be produced. 

(10)

 

If the leakage is existed between container for product and bracket at lower of the cyclone, 
the  dried  powder  may  be  stocked  onto  the  lower  of  the  cyclone  without  falling  into  the 
container  for  product.    Therefore,  pay  special  attention  to  the  unit  with  the  container  for 
product be mounted. 

(11)

 

When  the  heater  is  ON,  do  not  expose  the  cap  and  bayonet  of  the  spray  nozzle  to  the 
non-guard status, and do supply the air to the heater part for at least 0.1 to 0.2m

3

/min. 

(12)

 

If the sample is not fed from the feeding pump, the following causes may be considered; the 
sample tube is crushed at the roller of the pump, the inner wall of the tube is adhered tightly 
without restoration, or the inner of the nozzle is blocked.    Remove the cause, and reset to the 
normal status. 

(13)

 

Do  not  perform  unattended  operation  during  activating  the  unit.  Since  the  unit  is  in  idling 
status and the nozzle is blocked of after the operation using sample, the temperature around 
outlet is increased and the remaining sample is flown from the sample tube disconnected from 
the unit, and these failures may cause the indeterminism accident. 

(14)

 

There are to types of specimen tubes, those made of silicone and those made of Viton. Take 
care they might be corroded, swell and break with some solvents during operation. 

(15)

 

When the high temperature is set to the temperature around inlet for the operation, supplying 
too excessive airflow of the blower to the unit may not reach the temperature to the setting 
one caused by not keeping balance with the heater capacity.    To resolve this error, turn down 
the airflow of the blower, increase the setting temperature, and operate this unit. To avoid a 
malfunction of the blower, set the air amount below the red zone on the dial scale. When you 
operate the unit at a higher set temperature, the setting and the actual inlet temperature will 
not match. 
The  heater  will  stop  automatically  when  the  inlet  temperature  exceeds  230

,  or  when  the 

outlet temperature exceeds 110

Summary of Contents for GAS410

Page 1: ...Ltd To use this unit properly read this Instruction Manual thoroughly before using this unit Keep this instruction manual around this unit for referring at anytime WARNING Carefully read and thorough...

Page 2: ...About applicable organic solvents 24 Corrosion resistance table 26 Piping system diagram 27 List of materials 28 Precautions during operation 29 6 Maintenance Method 31 Daily Inspection and Maintenanc...

Page 3: ...equire hospitalization or outpatient visits for a long time Note 2 Minor injury means a wound or an electrical shock that does not require hospitalization or outpatient visits for a long time Note 3 P...

Page 4: ...Hazard of explosion Caution General cautions Electrical shock Burning Caution for no liquid heating Caution for water leak For water only Poisonous material Prohibitions General bans Fire ban Do not d...

Page 5: ...rn off the power switch of the main unit immediately and turn off the original power source and finally contact to either the dealer you purchased this unit or our sales office Leaving the failure may...

Page 6: ...is flown from the sample tube disconnected from the unit and this failure may cause the indeterminism accident Any people other than the qualified personnel shall never attempt to operate the unit Ta...

Page 7: ...nt of the user 2 Pay attention to the color of each core wire when connecting the power cord Be sure to check that the breaker on the power source equipment side is turned OFF when connecting power co...

Page 8: ...may result Refer to page 47 13 List of Dangerous Substances 5 Do not use explosive or flammable substances Take extreme care for use of an explosive or a flammable solvent Such a solvent may cause an...

Page 9: ...s uses the same power line of this unit If the phenomena might be found change the power line of this unit to the other power line For connecting of the device to the power source ask the dealer that...

Page 10: ...eter N2 flow meter Circulation path filter Gas selector switch N2 bombe connection port Duct connection outlet Cooling fan ELB with over current protector Duct connection port Collecting flask door Fo...

Page 11: ...Filter for oxygen sensor Pump for oxygen sensor For condensing solvent in condenser path Temperature sensor Ball valve Clamp 2L collecting flask Freezer Compressor Filter case Flow meter for introduci...

Page 12: ...pressure between the inlet and outlet of the filter to check the filter status Air amount meter monitor installation port Air amount meter and monitor are optional This port is used for installing opt...

Page 13: ...g process will discharge organic solvents hot air and fine particles at the exhaust port out of the pipe path Connect the supplied discharge duct to the discharge port and discharge to external using...

Page 14: ...ol an option for exclusive use of ADL311 in an operation position lowering by all means and can put height together when I am connected to GAS410 The footstool an option for exclusive use of ADL311 be...

Page 15: ...into the connecting tube to the duct connecting inlet port of GAS410 Put an O ring and securely fix using a clamp for installation C Connect a Fluororubber tube milky white and fix it using a wire cl...

Page 16: ...upper position of the connecting port and remove a set of filter installation parts from the lower position of the connecting port 2 Connect the supplied connecting tube using M4 10 truss screws Conne...

Page 17: ...n O ring and securely fix using a clamp for installation C Connect a Fluororubber tube milky white and fix it using a wire clamp D Connect a tetrone braided hose and fix it using a wire clamp E Connec...

Page 18: ...y moves to the next one after calibration or press NEXT key Any key operation will be invalid until the timer counts becomes 0s When connected to GAS410 the blower of ADL311S or GB210A will not be use...

Page 19: ...in N2 gas concentration control by this solenoid valve Open Close Set the liquid tube as shown in the left diagram Push the pump rod CCW to open the pump head put the liquid sending tube in it and the...

Page 20: ...open the ball vale above the collecting flask to start recovering solvent 8 Readjust dry air amount spray pressure and liquid sending speed so that the inlet and the outlet temperature will be stable...

Page 21: ...ontinue operation for a while to completely recover solvent When solvent contains water content the cooling trap may be frosted and the amount of solvent recovered may decrease If amount of solvent re...

Page 22: ...GAS410 OFF 17 Remove the container holding band and take out the product collecting container When taking out the container take care the powder attached on the back side of the cyclone cover 18 Hold...

Page 23: ...is in operation When the lamp is on the liquid sending pump is operating in the normal direction When the lamp is on the liquid sending pump is operating in the reverse direction When this lamp is on...

Page 24: ...t Blower dial value 50 100 150 0 4 44 73 97 4 5 44 75 98 5 5 45 76 100 7 45 76 101 8 5 46 78 102 10 47 79 103 The table below shows the relationship between dial values of the blower and average circu...

Page 25: ...breaker and the main power Immediately contact a service technician for inspection If this procedure is not followed fire or electrical shock may result Never perform repair work yourself since it is...

Page 26: ...educing the air amount and amount of liquid to send for solvents with a low boiling point such as methylene chloride Example Environmental temperature 25 Amount of liquid to send 1170mL H methylene ch...

Page 27: ...anol Acetic ether Hexane Methanol Chloroform Acetone Methylene chloride o 144 m 139 3 p 138 5 82 3 80 1 78 4 77 1 67 7 64 6 61 2 56 2 40 o 25 m 47 4 p 13 2 88 5 5 114 3 83 6 95 3 97 4 63 5 94 6 97 7 o...

Page 28: ...meter Bond to glass O ring Solenoid valve seal Liquid sending tube Hoses Packing for installing the oxygen concentration measurement sensor Filter bottom packing Oxygen concentration meter pump valve...

Page 29: ...27 5 Handling precautions Piping system diagram...

Page 30: ...onnecting hose Teflon G Cap Silicone Compressor Cover case PP Connecting hose Teflon H Pressure meter Solenoid valve for N2 control Seal assembly Teflon I Needle valve Seal assembly Teflon Viton Flow...

Page 31: ...f the cyclone without falling into the container for product Therefore pay special attention to the unit with the container for product be mounted 11 When the heater is ON do not expose the cap and ba...

Page 32: ...electricity such as attaching included earth clips at three positions on the clamp at the connection of the cyclone or attaching an antistatic brush to the body of the cyclone 18 Depending on the samp...

Page 33: ...normal one Do not disassemble this unit Caution Use a well drained soft cloth to wipe dirt on this unit Do not use benzene thinner or cleanser for wiping Do not scrub this unit Deformation deteriorati...

Page 34: ...filter element and remove dusts attached inside the filter case or on the bottom by suctioning with an electric cleaner or by wiping out with a cloth During this work take care so that dusts will not...

Page 35: ...three months thereafter Remove the blind plates on the right side plate and at the lower right of the rear side Stop the blower remove the oil drain plug and allow all old oil to discharge Replace th...

Page 36: ...sassemble this unit as possible and recycle the reusable parts considering to the environmental protection The feature components of this unit and materials used are listed below Component Name Materi...

Page 37: ...p temperature becomes 40 or more Imperfect connection or disconnection of the temperature sensor Malfunction of the display monitor temperature controller Malfunction of the freezer or the inverter Po...

Page 38: ...ly voltage Repair or replace Lower ambient temperature or cleaning the plug to ensure a well ventilated Repair or replace Supply voltage too high or too low Motor mechanical failure Ambient temperatur...

Page 39: ...onfirmation and language select for the manual You can select English or Chinese with the language select function for the manual Confirmation and language select for the manual Pressing ESC key will...

Page 40: ...and language select for the manual You can select English or Chinese with the language select function for error display and comments Language selection for error display Language selection for commen...

Page 41: ...efective Wait for five minutes and check whether the freezer operates or not Replace the heater Replace the touch panel or the sequencer Repair the defective points or replace the temperature controll...

Page 42: ...connect the test port of oxygen concentration meter to atmosphere directly See P 40 picture Replace the flowmeter Replace Replace the filter Replace Replace Thermo regulator failure Defective display...

Page 43: ...arbon filter absorption operate as per the following pictures Adjust the gas pipe switching valve to connect to atmosphere External gas wait for several minutes and check if the oxygen concentration d...

Page 44: ...nd other information and send it to our customer service center by Facsimile 03 3231 6523 Then store it securely Warranty period is one full year from the date of purchase Repair service for free is a...

Page 45: ...ntration Compressor For pushing the spray nozzle Safety device Oxygen concentration meter flammable gas alarm Power supply AC200V AC240V Single phase 5A External dimensions 1 W D H 700 950 1500 Weight...

Page 46: ...44 11 Wiring diagram...

Page 47: ...N2 YSJ A040403013 Solenoid valve CKD AB41 02 5 F AC100V for controlling N2 YSJ A040403004 Linear compressor AC0910 YSC B030200001 Differential pressure meter DG87 641 1C 0 1kPa YSC B042300001 Filter...

Page 48: ...Temperature controller TTM214 Q RI RUV for trap display YSC B020101027 Relay HF13F A1002Z1D YSJ A011002005 Transformer AD21 200A2 YSC B010701011 Oxygen sensor module GPR 2500 GPR11 32 RST YSJ B9901002...

Page 49: ...chlorate ammonium perchlorate and other perchlorates Potassium peroxide sodium peroxide barium peroxide and other inorganic peroxides Potassium nitrate sodium nitrate ammonium nitrate and other nitrat...

Page 50: ...s Unexpected accidents or breakdown may result in Note The contents of this document may be changed in future without notice Any books with missing pages or disorderly binding may be replaced Instruct...

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