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Thermo Scientific 43i, Instruction Manual

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Contents 

Where to Get Help 

xiv

     Model 43

i

 Trace Level-Enhanced Instruction Manual 

Thermo Fisher Scientific 

 

Servicing .............................................................................................................7-1

 

Safety Precautions ............................................................................... 7-1

 

Firmware Updates ............................................................................... 7-2

 

Accessing the Service Mode................................................................. 7-2

 

Replacement Parts List ........................................................................ 7-3

 

Cable List............................................................................................ 7-4

 

External Device Connection Components .......................................... 7-5

 

Removing the Measurement Bench and Lowering the Partition Panel 7-6

 

Fuse Replacement ............................................................................... 7-8

 

Pump Replacement ............................................................................. 7-8

 

Fan Replacement............................................................................... 7-10

 

Optical Bench Replacement .............................................................. 7-11

 

Cleaning the Mirrors......................................................................... 7-12

 

Flash Lamp Replacement .................................................................. 7-12

 

Flash Lamp Voltage Adjustment ....................................................... 7-14

 

Flash Trigger Assembly Replacement ................................................ 7-14

 

Flash Intensity Assembly Replacement .............................................. 7-15

 

Photomultiplier Tube Replacement .................................................. 7-16

 

PMT High Voltage Power Supply Replacement................................ 7-17

 

PMT Voltage Adjustment ................................................................. 7-19

 

DC Power Supply Replacement ........................................................ 7-20

 

Analog Output Testing ..................................................................... 7-21

 

Analog Output Calibration ............................................................... 7-23

 

Analog Input Calibration .................................................................. 7-24

 

Calibrating the Input Channels to Zero Volts ................................ 7-24

 

Calibrating the Input Channels to Full Scale.................................. 7-25

 

Pressure Transducer Assembly Replacement...................................... 7-26

 

Pressure Transducer Calibration........................................................ 7-27

 

Flow Transducer Replacement .......................................................... 7-29

 

Flow Transducer Calibration............................................................. 7-30

 

Heater Assembly Replacement .......................................................... 7-32

 

Kicker Replacement .......................................................................... 7-33

 

Thermistor Replacement................................................................... 7-34

 

Ambient Temperature Calibration .................................................... 7-35

 

Input Board Replacement ................................................................. 7-36

 

I/O Expansion Board (Optional) Replacement ................................. 7-37

 

Digital Output Board Replacement................................................... 7-39

 

Motherboard Replacement................................................................ 7-40

 

Measurement Interface Board Replacement ...................................... 7-41

 

Front Panel Board Replacement........................................................ 7-42

 

LCD Module Replacement ............................................................... 7-43

 

Service Locations............................................................................... 7-44

 

 
 

Chapter 7

 

Summary of Contents for 43i

Page 1: ...Model 43i Trace Level Enhanced Instruction Manual Pulsed Fluorescence SO2 Analyzer Part Number 102780 00 14Jan2008 ...

Page 2: ...ons terms and pricing are subject to change Not all products are available in all countries Please consult your local sales representative for details Thermo Fisher Scientific Air Quality Instruments 27 Forge Parkway Franklin MA 02038 1 508 520 0430 www thermo com aqi ...

Page 3: ...ientific has contracted with one or more recycling disposal companies in each EU Member State and this product should be disposed of or recycled through them Further information on Thermo Fisher Scientific s compliance with these Directives the recyclers in your country and information on Thermo Fisher Scientific products which may assist the detection of substances subject to the RoHS Directive a...

Page 4: ......

Page 5: ...Preventive Maintenance provides maintenance procedures to ensure reliable and consistent instrument operation Chapter 6 Troubleshooting presents guidelines for diagnosing analyzer failures isolating faults and includes recommended actions for restoring proper operation Chapter 7 Servicing presents safety alerts for technicians working on the analyzer step by step instructions for repairing and rep...

Page 6: ...the warning is ignored WARNING A hazard is present or an unsafe practice can result in serious personal injury if the warning is ignored CAUTION The hazard or unsafe practice could result in minor to moderate personal injury if the warning is ignored Equipment Damage The hazard or unsafe practice could result in property damage if the warning is ignored Safety and Equipment Damage Alerts in this M...

Page 7: ...e the equipment Note This equipment has been tested and found to comply with the limits for a Class A digital device pursuant to Part 15 of the FCC Rules These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment This equipment generates uses and can radiate radio frequency energy and if not installed and used ...

Page 8: ...o Fisher Scientific Service is available from exclusive distributors worldwide Contact one of the phone numbers below for product support and technical information or visit us on the web at www thermo com aqi 1 866 282 0430 Toll Free 1 508 520 0430 International Where to Get Help ...

Page 9: ...erminal Board 2 8 Startup 2 9 Operation 3 1 Display 3 2 Pushbuttons 3 3 Soft Keys 3 4 Software Overview 3 4 Power Up Screen 3 6 Run Screen 3 6 Main Menu 3 6 Range Menu 3 7 Single Range Mode 3 8 Dual Range Mode 3 9 Autorange Mode 3 10 Gas Units 3 12 SO2 Range 3 13 Set Custom Ranges 3 14 Custom Ranges 3 14 Averaging Time 3 15 Calibration Factors Menu 3 15 SO2 Background 3 16 SO2 Span Coefficient 3 1...

Page 10: ...6 Concentrations 3 26 Other Measurements 3 27 Analog Inputs 3 27 Commit Content 3 28 Reset to Default Content 3 28 Configure Datalogging 3 29 Logging Period Min 3 29 Memory Allocation Percent 3 29 Data Treatment 3 30 Communication Settings 3 30 Baud Rate 3 31 Instrument ID 3 31 Communication Protocol 3 31 Streaming Data Configuration 3 32 Streaming Data Interval 3 32 Choose Item Signal 3 33 Concen...

Page 11: ... Compensation 3 47 Pressure Compensation 3 48 Screen Contrast 3 48 Service Mode 3 49 Date Time 3 49 Diagnostics Menu 3 50 Program Versions 3 50 Voltages 3 50 Motherboard Voltages 3 51 Interface Board Voltages 3 51 I O Board Voltages 3 52 Temperatures 3 52 Pressure 3 52 Sample Flow 3 53 Lamp Intensity 3 53 Optical Span Test 3 53 Analog Input Readings 3 54 Analog Input Voltages 3 54 Digital Inputs 3...

Page 12: ...ode Select 3 67 Pressure Calibration 3 67 Calibrate Pressure Zero 3 68 Calibrate Pressure Span 3 68 Restore Default Pressure Calibration 3 69 Flow Calibration 3 69 Calibrate Flow Zero 3 69 Calibrate Flow Span 3 70 Restore Default Flow Calibration 3 70 Input Board Test 3 71 Temperature Calibration 3 71 Analog Output Calibration 3 71 Analog Output Calibrate Zero 3 72 Analog Output Calibrate Full Sca...

Page 13: ...tems 4 3 Permeation Tube System 4 3 Commercial Permeation Systems 4 4 Multi Point Calibration 4 5 Multipoint Calibration in Dual Auto Range Mode 4 7 Zero Span Check 4 10 Preventive Maintenance 5 1 Safety Precautions 5 1 Replacement Parts 5 2 Cleaning the Outside Case 5 2 Visual Inspection and Cleaning 5 2 Cleaning the Mirrors 5 2 Capillary Inspection and Replacement 5 3 Fan Filter Inspection and C...

Page 14: ... PMT High Voltage Power Supply Replacement 7 17 PMT Voltage Adjustment 7 19 DC Power Supply Replacement 7 20 Analog Output Testing 7 21 Analog Output Calibration 7 23 Analog Input Calibration 7 24 Calibrating the Input Channels to Zero Volts 7 24 Calibrating the Input Channels to Full Scale 7 25 Pressure Transducer Assembly Replacement 7 26 Pressure Transducer Calibration 7 27 Flow Transducer Repl...

Page 15: ...4 Instrument Control 8 4 Monitoring Signals 8 5 Measurement Calculations 8 5 Output Communication 8 5 Electronics 8 6 Motherboard 8 6 External Connectors 8 6 Internal Connectors 8 7 Measurement Interface Board 8 7 Measurement Interface Board Connectors 8 7 Flow Sensor Assembly 8 7 Pressure Sensor Assembly 8 8 Bench Heater 8 8 PMT Power Supply Assembly 8 8 Diagnostic LED 8 8 Input Board 8 8 Digital...

Page 16: ...Temperature with Water Bath 9 6 Setting Temperature with Known Resistance 9 7 Determining Permeation Rate by Weight Loss 9 7 Determining Release Rate by Transfer Standard 9 8 Teflon Particulate Filter 9 9 I O Expansion Board Assembly 9 9 25 Pin Terminal Board Assembly 9 9 Terminal Block and Cable Kits 9 9 Cables 9 10 Mounting Options 9 11 Warranty A 1 C Link Protocol Commands B 1 Instrument Identi...

Page 17: ...3 Data C 3 Error Check C 3 Function Codes C 3 0x01 0x02 Read Coils Read Inputs C 3 0x03 0x04 Read Holding Registers Read Input Registers C 5 0x03 0x04 Read Holding Registers Read Input Registers C 5 0x05 Force Write Single Coil C 7 MODBUS Commands Supported C 8 Geysitech Bayern Hessen Protocol D 1 Serial Communication Parameters D 1 TCP Communication Parameters D 2 Instrument Address D 2 Abbreviat...

Page 18: ...Contents Where to Get Help xviii Model 43i Trace Level Enhanced Instruction Manual Thermo Fisher Scientific ...

Page 19: ...s Dilution System 4 3 Figure 4 2 Permeation Tube System 4 4 Figure 5 1 Inspecting and Replacing the Capillary 5 3 Figure 5 1 Inspecting and Cleaning the Fan 5 5 Figure 5 2 Rebuilding the Pump 5 7 Figure 6 1 Board Level Connection Diagram Common Electronics 6 10 Figure 6 2 Board Level Connection Diagram Measurement System 6 11 Figure 7 1 Properly Grounded Antistatic Wrist Strap 7 2 Figure 7 2 Model...

Page 20: ...38 Figure 7 21 Rear Panel Board Connectors 7 39 Figure 7 22 Replacing the Measurement Interface Board 7 42 Figure 7 23 Replacing the Front Panel Board and the LCD Module 7 43 Figure 8 1 Hardware Components 8 2 Figure 9 1 Internal Permeation Span Source Flow Diagram 9 2 Figure 9 2 Cal Oven Therm Resistor Screen 9 5 Figure 9 3 Cal Gas Therm Bath Screen 9 6 Figure 9 4 Cal Gas Therm Resistor Screen 9 ...

Page 21: ...es 6 5 Table 6 4 Troubleshooting Alarm Messages 6 8 Table 6 5 Motherboard Connector Pin Descriptions 6 12 Table 6 6 Measurement Interface Board Connector Pin Descriptions 6 16 Table 6 7 Front Panel Board Connector Pin Diagram 6 19 Table 6 8 I O Expansion Board Optional Connector Pin Descriptions 6 21 Table 6 9 Digital Output Board Connector Pin Descriptions 6 22 Table 6 10 Input Board Connector Pi...

Page 22: ...ontrast Level B 32 Table B 9 Reply Termination Formats B 37 Table B 10 Analog Current Output Range Values B 39 Table B 11 Analog Voltage Output Range Values B 40 Table B 12 Default Output Assignment B 41 Table C 1 Read Registers for 43i Trace Level Enhanced C 8 Table C 2 Write Coils for 43i Trace Level Enhanced C 9 Table C 3 Read Coils for 43i Trace Level Enhanced C 10 Table D 1 Operating Status f...

Page 23: ...nsitivity Fast response time Linearity through all ranges Internal sample pump Totally self contained Insensitive to changes in flow and ambient temperature User selectable digital input output capabilities Standard communications features include RS232 485 and Ethernet C Link MODBUS Geysitech Bayern Hessen and streaming data protocols For details of the analyzer s principle of operation and produ...

Page 24: ... chamber where pulsating UV light excites the SO2 molecules The condensing lens focuses the pulsating UV light into the mirror assembly The mirror assembly contains eight selective mirrors that reflect only the wavelengths which excite SO2 molecules As the excited SO2 molecules decay to lower energy states they emit UV light that is proportional to the SO2 concentration The bandpass filter allows ...

Page 25: ...0 100 200 500 and 1000 ppb 0 20 50 100 200 500 1000 and 2000 μg m3 Custom ranges 0 10 to 1000 ppb 0 20 to 2000 μg m3 Zero noise 0 14 ppb RMS 10 second averaging time 0 06 ppb RMS 60 second averaging time 0 025 ppb RMS 300 second averaging time Lower detectable limit 0 208 ppb 10 second averaging time 0 12 ppb 60 second averaging time 0 05 ppb 300 second averaging time Zero drift 24 hour 0 2 ppb Sp...

Page 26: ... 220 240 VAC 50 60 Hz 165 watts Physical dimensions 16 75 W X 8 62 H X 23 D Weight Approximately 48 lbs Analog outputs 6 voltage outputs 0 100 mV 1 5 10 V user selectable 5 of full scale over under range 12 bit resolution user selectable for measurement input Digital outputs 1 power fail relay Form C 10 digital relays Form A user selectable alarm output relay logic 100 mA 200 VDC Digital inputs 16...

Page 27: ...t 45 C Temperature stability 0 1 C Warm up time 1 hour permeation device can take 24 to 48 hours to stabilize Carrier gas flow 70 scc min Chamber size Accepts permeation tubes up to 9 cm in total length 1 cm in diameter Temperature range 20 30 C Physical dimensions Contained inside the Model 43i Trace Level Enhanced Power requirements 120 VAC 50 60 Hz 50 watts in addition to the standard Model 43i...

Page 28: ...Introduction Specifications 1 6 Model 43i Trace Level Enhanced Instruction Manual Thermo Fisher Scientific ...

Page 29: ...9 When lifting the instrument use a procedure appropriate to lifting a heavy object such as bending at the knees while keeping your back straight and upright Grasp the instrument at the bottom in the front and at the rear of the unit Although one person can lift the unit it is desirable to have two persons lifting one by grasping the bottom in the front and the other by grasping the bottom in the ...

Page 30: ...allows easy access to both the front and rear 2 Remove the cover to expose the internal components 3 Remove the packing material Figure 2 1 Figure 2 1 Remove the Packing Material 4 Remove the three shipping screws from the pump Figure 2 2 Figure 2 2 Removing the Shipping Screws Shipping Screws 3 Units without Optional I O Board Remove Packing 2 pieces Units with Optional I O Board Remove Packing 2...

Page 31: ...rticulate Filter on page 9 9 If the sample may contain particulates larger than 5 microns it should be filtered before introducing it to the instrument Use a filter such as Teflon that does not interact with SO2 in the sample If a sample filter is used all calibrations and span checks must be performed through the filter The filter element should be replaced regularly to prevent the absorption of ...

Page 32: ...9 9 Instrument Controls Menu on page 3 22 For detailed information about troubleshooting a connection refer to Analog Output Testing on page 7 21 4 Plug the instrument into an outlet of the appropriate voltage and frequency WARNING The Model 43i Trace Level Enhanced is supplied with a three wire grounding cord Under no circumstances should this grounding system be defeated Figure 2 3 Rear Panel ...

Page 33: ...llowing terminal board PCB assemblies are available for iSeries instruments I O terminal board PCB assembly 37 pin standard D O terminal board PCB assembly 37 pin standard 25 pin terminal board PCB assembly included with optional I O Expansion Board Figure 2 5 shows the recommended method for attaching the cable to the terminal board using the included tie down and spacer Table 2 1 identifies the ...

Page 34: ...iption 1 Analog1 13 Power_Fail_NC 2 Analog ground 14 Power_Fail_COM 3 Analog2 15 Power_Fail_NO 4 Analog ground 16 TTL_Input1 5 Analog3 17 TTL_Input2 6 Analog ground 18 TTL_Input3 7 Analog4 19 TTL_Input4 8 Analog ground 20 Digital ground 9 Analog5 21 TTL_Input5 10 Analog ground 22 TTL_Input6 11 Analog6 23 TTL_Input7 12 Analog ground 24 Digital ground Component Side Viewed from Top of Board Detail A...

Page 35: ...tions Pin Signal Description Pin Signal Description 1 Relay1_ContactA 13 Relay7_ContactA 2 Relay1_ContactB 14 Relay7_ContactB 3 Relay2_ContactA 15 Relay8_ContactA 4 Relay2_ContactB 16 Relay8_ContactB 5 Relay3_ContactA 17 Relay9_ContactA 6 Relay3_ContactB 18 Relay9_ContactB 7 Relay4_ContactA 19 Relay10_ContactA 8 Relay4_ContactB 20 Relay10_ContactB 9 Relay5_ContactA 21 Not Used 10 Relay5_ContactB 2...

Page 36: ...al Board Pin Descriptions Pin Signal Description Pin Signal Description 1 IOut1 13 Analog_In1 2 Isolated ground 14 Analog_In2 3 IOut2 15 Analog_In3 4 Isolated ground 16 GNDD 5 IOut3 17 Analog_In4 6 Isolated ground 18 Analog_In5 7 IOut4 19 Analog_In6 8 Isolated ground 20 GNDD 9 IOut5 21 Analog_In7 10 Isolated ground 22 Analog_In8 11 IOut6 23 GNDD 12 Isolated ground 24 GNDD 25 Pin Terminal Board Com...

Page 37: ... Turn the power ON 2 Allow 30 minutes for the instrument to stabilize 3 Set instrument parameters such as operating ranges and averaging times to appropriate settings For more information about instrument parameters see the Operation chapter 4 Before beginning actual monitoring perform a multipoint calibration as described in the Calibration chapter Startup ...

Page 38: ...Installation Startup 2 10 Model 43i Trace Level Enhanced Instruction Manual Thermo Fisher Scientific ...

Page 39: ...ribes the gas units SO2 range and custom ranges Averaging Time on page 3 15 describes the averaging period applied to SO2 measurements Calibration Factors Menu on page 3 15 describes the calibration factors used to correct SO2 measurement readings Calibration Menu on page 3 18 describes manual and automatic calibration of zero and span Instrument Controls Menu on page 3 22 describes the instrument...

Page 40: ...ument controls help and error messages Some menus contain more items than can be displayed at one time For these menus use and to move the cursor up and down to each item Figure 3 1 Front Panel Display CAUTION If the LCD panel breaks do not to let the liquid crystal contact your skin or clothes If the liquid crystal contacts your skin or clothes wash it off immediately using soap and water Display...

Page 41: ...he is used to display the Main Menu when in the Run screen or back up one level in the menu system For more information about the Main Menu see Main Menu later in this chapter Help The is context sensitive that is it provides additional information about the screen that is being displayed Press for a brief explanation about the current screen or menu Help messages are displayed using lower case le...

Page 42: ...item cannot be assigned the key assignment screen will not come up upon entering right arrow soft key combinations All items under the Service menu including the menu itself cannot be assigned soft keys EDIT SOFT KEY PROMPT CURRENTLY RANGE RANGE ABCDEFGHIJKLMN BKSP OPQRSTUVWXYZ PAGE 0123456789 SAVE RANGE AVG DIAGS ALARM The Model 43i Trace Level Enhanced utilizes the menu driven software as illust...

Page 43: ...iagnostics Program Version Voltages Temps Pressure Flow Lamp Intensity Optical Span Test Analog Input Readings Analog Input Voltages Digital Inputs Relay States Test Analog Outputs Instrument Config Contact Info Alarms Alarms Detected Internal Temp Chamber Temp Perm Gas Temp Pressure Sample Flow Lamp Intensity Lamp Voltage Zero Check Span Check Zero Autocal Span Autocal SO Conc MB Status Int Bd St...

Page 44: ...mation about the optional solenoid valves see Chapter 9 Optional Equipment When operating in dual or auto range mode two sets of coefficients are used to calculate the CO High and Low concentrations Also two averaging times are used one for each range The title bar indicates which range concentrations are displayed The words LOW RANGE CONCENTRATION on the top of the display indicates that the low ...

Page 45: ...FACTORS CALIBRATION INSTRUMENT CONTROLS DIAGNOSTICS ALARMS ª RANGE AVG DIAGS ALARM SERVICE PASSWORD The Range menu allows the operator to select the gas units SO2 ranges and to set the custom ranges The screens that follow show the range menu in single mode and dual autorange modes The only difference between the screens are the words HI and LO to indicate which range is displayed For more informa...

Page 46: ...e selected from the Range Mode Select in the Service Menu later in this chapter Figure 3 4 Pinout of Rear Panel Connector in Single Range Mode Table 3 2 Default Analog Outputs in Single Range Mode Channel Connector Pin I O Terminal Pin Description 1 14 1 SO2 Analog Output 2 33 3 SO2 Analog Output 3 15 5 None 4 34 7 None 5 17 9 None 6 36 11 None Ground 16 18 19 35 37 2 4 6 8 10 12 Signal Ground Not...

Page 47: ...ach SO2 analog output has a span coefficient There are two span coefficients so that each range can be calibrated separately This is necessary if the two ranges are not close to one another For example the low SO2 range is set to 0 10 ppb and the high SO2 range is set to 0 1000 ppb By default in the dual range mode the analog outputs are arranged on the rear panel connector as shown in Figure 3 5 ...

Page 48: ...et to 50 ppb and the high range is set to 100 ppb Figure 3 6 Sample concentrations below 50 ppb are output based on low range selection and sample concentrations above 50 ppb are output based on high range selection When the low range is active the status output is at 0 volts When the high range is active the status output is at half of full scale When the high range is active the concentration mu...

Page 49: ...torange Mode By default in the autorange mode the analog outputs are arranged on the rear panel connector as shown in Figure 3 7 See Table 3 4 for channels and pin connections Autorange mode may be selected from Range Mode Select in the Service Menu later in this chapter Figure 3 7 Pin Out of Rear Panel Connector in Auto Range Mode ...

Page 50: ...ngs are expressed Gas units of parts per billion ppb or micrograms per cubic meter μg m3 are available The μg m3 gas concentration is calculated using a standard pressure of 760 mmHg and a standard temperature of 20 C When switching the selected units from ppb or μg m3 the analog ranges all default to the highest range in that mode For example when switching from μg m3 to ppb all the ranges defaul...

Page 51: ...is used to change the range The range screen is similar for the single dual and autorange modes The only difference between the screens are the words High or Low displayed to indicate which range is displayed The example that follows shows the SO2 range screen in single mode For more information about the dual and autorange modes see Single Range Mode Dual Range Mode and Autorange Mode earlier in ...

Page 52: ...d as a range In the Main Menu choose Range Set Custom Ranges CUSTOM RANGES CUSTOM RANGE 1 55 6 CUSTOM RANGE 2 75 0 CUSTOM RANGE 3 85 0 RANGE AVG DIAGS ALARM The Custom Ranges screen is used to define the custom ranges The display shows the current custom range The next line of the display is used to set the range To use the custom full scale range be sure to select it Custom range 1 2 or 3 in the ...

Page 53: ...u is displayed before the averaging time screen This additional menu is needed because the dual and autorange modes have two averaging times high and low The averaging time screen functions the same way in the single dual and autorange modes The following averaging times are available 1 2 5 10 20 30 60 90 120 180 240 and 300 seconds In the Main Menu choose Averaging Time AVERAGING TIME CURRENTLY 3...

Page 54: ...ubtracted from the SO2 reading In the example that follows the analyzer is reading 1 49 ppb of SO2 while sampling zero air The SO2 background correction is 0 0 ppb That is the analyzer is not applying a zero background correction The question mark is used as a prompt to change the background correction In this case the background correction must be increased to 1 49 ppb in order for the SO2 readin...

Page 55: ...and is being used to correct the SO2 concentration Notice that as the span coefficient value is changed the current SO2 concentration reading on the above line also changes However no real changes are made to the value stored in memory until is pressed Only proposed changes as indicated by a question mark prompt are displayed until is pressed In dual or autorange modes HIGH or LOW is displayed to ...

Page 56: ...tion In the Main Menu choose Calibration The Calibrate SO2 Background screen is used to adjust the SO2 background or perform a zero calibration Before performing a zero calibration ensure the analyzer samples zero air for at least 5 minutes It is important to note the averaging time when calibrating The longer the averaging time the more accurate the calibration will be To be most accurate use the...

Page 57: ...ibration see Chapter 4 Calibration In dual or auto range modes HIGH or LOW is displayed to indicate the calibration of the high or low coefficient In the Main Menu choose Calibration Cal SO2 Coefficient CALIBRATE SO2 SO2 813 SPAN CONC 00000800 MOVE CURSOR ª CHANGE VALUE SAVE RANGE AVG DIAGS ALARM The Zero Span Check menu is available with the zero span valve option It is used to program the instru...

Page 58: ...nd of the next zero span check is calculated and displayed In the Main Menu choose Calibration Zero Span Check Next Time The Zero Span Period Hours screen defines the period or interval between zero span checks Periods between 0 and 999 hours are acceptable To turn the zero span check off set the period to 0 In the Main Menu choose Calibration Zero Span Check Period Hours ZERO SPAN PERIOD CURRENTL...

Page 59: ...T TO 31 MIN MOVE CURSOR ª CHANGE VALUE SAVE RANGE AVG DIAGS ALARM The Zero Span Averaging Time screen allows the user to adjust the zero span averaging time The zero span averaging time is used by the analyzer only when performing an automatic zero or span check or calibration The analyzer s averaging time is used for all other functions The following averaging times are available 1 2 5 10 20 30 6...

Page 60: ...choose Instrument Controls INSTRUMENT CONTROLS FLASH LAMP DATALOGGING SETTINGS COMMUNICATION SETTINGS I O CONFIGURATION TEMPERATURE COMPENSATION PRESSURE COMPENSATION SCREEN CONTRAST ª RANGE AVG DIAGS ALARM SERVICE MODE DATE TIME The Flash Lamp screen is used to turn the flash lamp on or off The flash lamp must be off when using the optical span test LED For more information about the optical span...

Page 61: ...ct SREC LREC is used to select short record or long record format for other operations in this menu In the Main Menu choose Instrument Controls Datalogging Settings Select SREC LREC SEL LOG TYPE CURRENTLY SREC SET TO LREC TOGGLE VALUE RANGE AVG DIAGS ALARM The View Logged Data screen is used to select the start point to view the logged data by number or records or date and time In the Main Menu ch...

Page 62: ... records time date flags 10 01 06 20 05 FC0088900 10 02 06 20 05 FC0088900 10 03 06 20 05 FC0088900 10 04 06 20 05 FC0088900 ª PGUP DN PAN L R RANGE AVG DIAGS ALARM The Date and Time screen is used to set a start date and time for which to view logged data For example if 20 JUN 2005 10 00 is entered then the first logged data record that is displayed is the first record after this time If set to o...

Page 63: ... displays a list of 32 record fields to use and a submenu list of the analog output signal group choices to choose from Choices are Concentrations Other Measurements and Analog Inputs if the I O expansion board is installed This is a temporary list of items for the selected record type that must be committed via the datalogging menu before the changes will apply Note that committing any changes to...

Page 64: ... 1 32 DATA IN SREC FIELD 1 CONCENTRATIONS OTHER MEASUREMENTS ANALOG INPUTS RANGE AVG DIAGS ALARM Note The ANALOG INPUTS item is only displayed if the I O Expansion Board option is installed The Concentrations screen allows the user to select the output signal that is tied to the selected field item The selected item is shown by after it Note that at this point pressing indicates that these are pro...

Page 65: ...mit Content that follows In the Main Menu choose Instrument Controls Datalogging Settings Select Content Select Field Other Measurements OTHER MEASUREMENTS NONE INT TEMP CHAMBER TEMP PERM OVN GAS PERM OVN HTR CHAMBER PRES SAMPLE FLOW ª RANGE AVG DIAGS ALARM The Analog Inputs screen allows the user to select the output signal none or analog inputs 1 8 that is tied to the selected field item The sel...

Page 66: ...oices see Commit Content in this chapter In the Main Menu choose Instrument Controls Datalogging Settings Select Content The Reset to Default Content screen is used to reset all of the datalogging field items to default values For more information about selecting the analog output signal group choices see Select Content in this chapter In the Main Menu choose Instrument Controls Datalogging Settin...

Page 67: ... 5 15 30 and 60 minutes default In the Main Menu choose Instrument Controls Datalogging Settings Configure Datalogging Logging Period Min SET PERIOD FOR SREC CURRENTLY OFF MIN SET TO 60 MIN ª CHANGE VALUE SAVE RANGE AVG DIAGS ALARM The Memory Allocation Percent screen is used to select the percentage of each record type for both srecs and lrecs Percentages between 0 and 100 are available in increm...

Page 68: ...nt value last value measured Data treatment doesn t apply to all data just to the concentration measurement All other data points log the current value at the end of the interval In the Main Menu choose Instrument Controls Datalogging Settings Configure Datalogging Data Treatment SET LREC DATA TYPE CURRENTLY AVG SET TO CUR ª CHANGE VALUE SAVE RANGE AVG DIAGS ALARM The communication Settings menu i...

Page 69: ...trol the instrument or collect data It may be necessary to edit the ID number if two or more of the same instruments are connected to one computer Valid Instrument ID numbers are from 0 to 127 The Model 43i Trace Level Enhanced has a default Instrument ID of 43 For more information about the Instrument ID see Appendix B C Link Protocol Commands or Appendix C MODBUS Protocol In the Main Menu choose...

Page 70: ...if the I O expansion board option is installed Note Add Labels and Prepend Timestamp are toggle items that change between yes or no when selected In the Main Menu choose Instrument Controls Communication Settings Streaming Data Config STREAMING DATA CONFIG INTERVAL 10 SEC ADD LABELS NO PREPEND TIMESTAMP YES ITEM 1 SO2 ITEM 2 INTT ITEM 3 RCTT ITEM 4 PRES ª RANGE AVG DIAGS ALARM ITEM 5 SMPLFL ITEM 6...

Page 71: ...DIAGS ALARM The Concentrations screen allows the user to select the output signal that is tied to the selected streaming data item The selected item is shown by after it In dual or auto range mode HI or LO is displayed to indicate high or low concentrations Range Status is also visible in auto range mode In the Main Menu choose Instrument Controls Communication Settings Streaming Data Config Selec...

Page 72: ... input signal none or analog inputs 1 8 that is tied to the selected streaming data item The selected item is shown by after it In the Main Menu choose Instrument Controls Communication Settings Streaming Data Config Select Item Analog Inputs ANALOG INPUTS NONE INPUT 1 INPUT 2 INPUT 3 INPUT 4 INPUT 5 INPUT 6 ª RANGE AVG DIAGS ALARM INPUT 7 INPUT 8 The RS 232 RS 485 Selection screen allows the user...

Page 73: ...ntrols Communication Settings TCP IP Settings TCP IP SETTINGS USE DHCP OFF IP ADDRESS 192 168 1 200 NETMASK 255 255 255 0 GATEWAY 192 168 1 1 HOST NAME iSeries RANGE AVG DIAGS ALARM The Use DHCP screen is used to specify whether to use DHCP or not When DHCP is enabled the network dynamically provides an IP address for the instrument The instrument s power must be cycled for a change to this parame...

Page 74: ...for which the instrument can directly communicate to other devices on The netmask can only be changed when DHCP is OFF For more information on DHCP see Use DHCP in this chapter In the Main Menu choose Instrument Controls Communication Settings TCP IP Settings Netmask NETMASK CURRENT 255 255 255 0 SET TO 255 255 255 000 MOVE CURSOR ª CHANGE VALUE SAVE RANGE AVG DIAGS ALARM The Default Gateway scree...

Page 75: ...ABCDEFGHIJKLMN BKSP OPQRSTUVWXYZ PAGE 0123456789 SAVE RANGE AVG DIAGS ALARM The I O Configuration menu deals with configuration of the analyzer s I O system The analog input configuration is displayed only if the I O expansion board option is installed Note The digital outputs may take up to one second after the assigned state occurs to show up on the outputs Note Analog Input Config is only displ...

Page 76: ...NOP NONE 6 NOP NONE 7 NOP SO2 MODE ª RANGE AVG DIAGS ALARM 8 NOP NONE 9 NOP NONE 10 NOP NONE The Logic State screen is used to change the I O relay to either normally open or normally closed Press to toggle and set the logic state between open and closed OUTPUT RELAY SETUP LOGIC STATE OPEN INSTRUMENT STATE RANGE AVG DIAGS ALARM The Instrument State submenu allows the user to select the instrument ...

Page 77: ...TATUS alarm is only present if the I O expansion board is installed ZERO CHK CAL and SPAN CHK CAL are only present if autozero span check is enabled ALARM STATUS ITEMS NONE GEN ALARM SO2 CONC MAX SO2 CONC MIN INT TEMP CHAMB TEMP PRESSURE ª RANGE AVG DIAGS ALARM SAMPLE FLOW FLASH REF FLASH VOLTS MB STATUS MIB STATUS I O BD STATUS CONC ALARM ZERO CHK CAL SPAN CHK CAL The Non Alarm status screen allo...

Page 78: ...o select the instrument parameter or logic state to change for the relay selected Note The digital inputs must be asserted for at least one second for the action to be activated In the Main Menu choose Instrument Controls I O Configuration Digital Input Settings DIGITAL INPUT SETTINGS 1 NOP SET BACKGROUND 2 NOP CAL TO LO SPAN 3 NOP AOUTS TO ZERO 4 NOP AOUTS TO FS 5 NOP CAL TO HI SPAN 6 NOP NONE 7 ...

Page 79: ...NGE AVG DIAGS ALARM The Instrument Action screen allows the user to select the instrument state that is tied to the selected digital input In the Main Menu choose Instrument Controls I O Configuration Digital Input Settings Select Relay Instrument State CHOOSE ACTION NONE ZERO MODE SPAN MODE SET BACKGROUND CAL TO LO SPAN AOUTS TO ZERO ª RANGE AVG DIAGS ALARM AOUTS TO FS CAL TO HI SPAN The Analog O...

Page 80: ...RM The Minimum Value screen is used to edit the zero 0 to full scale 100 value in percentages for the selected analog output channel See Table 3 7 for a list of choices In dual or auto range mode HI or LO is displayed to indicate high or low concentrations Range Status is visible only in auto range mode The minimum and maximum output value screens function the same way The example that follows sho...

Page 81: ...rm max value Perm Oven Heater Temp Perm Oven Heater alarm min value Perm Oven Heater alarm max value Pressure User set alarm min value User set alarm max value Sample Flow User set alarm min value User set alarm max value PMT Volts 700 volts 1100 volts Flash Voltage User set alarm min value User set alarm max value Flash Reference User set alarm min value User set alarm max value Everything Else 0...

Page 82: ...ations Other Measurements Analog Inputs None None None SO2 single auto range only Internal Temperature Analog Input 1 I O Expansion Board installed LO SO2 dual range only Chamber Temperature Analog Input 2 I O Expansion Board installed HI SO2 dual auto range only Perm Oven Gas Analog Input 3 I O Expansion Board installed Range Status auto range only Perm Oven Heater Analog Input 4 I O Expansion Bo...

Page 83: ... characters in length and defaults to IN1to IN8 user input channel number In the Main Menu choose Instrument Controls I O Configuration Analog Input Config Select Channel Descriptor ANALOG INPUT DESCRIPTOR ASS ABCDEFGHIJKLMN BKSP OPQRSTUVWXYZ PAGE 0123456789 SAVE RANGE AVG DIAGS ALARM The Units screen allows the user to enter the units for the selected analog input channel The units are displayed ...

Page 84: ...aces DECIMAL PLACES CURRENTLY 2 SET TO 3 ª INC DEC SAVE VALUE RANGE AVG DIAGS ALARM The Number of Table Points screen allows the user to select how many points are used in the conversion table The points range from 2 to 10 with a default of 2 In the Main Menu choose Instrument Controls I O Configuration Analog Input Config Select Channel Table Points NUMBER OF TABLE POINTS CURRENTLY 2 SET TO 10 ª ...

Page 85: ... CURSOR SAVE VALUE RANGE AVG DIAGS ALARM The User Value screen allows the user to set the output value for the corresponding input voltage for the selected table point in the conversion table from 9999999 to 99999999 The default table is a two point table with point 1 0 00 V 000 0 U and point 2 10 00 V 10 0 U In the Main Menu choose Instrument Controls I O Configuration Analog Input Config Select ...

Page 86: ...ALUE RANGE AVG DIAGS ALARM Pressure compensation provides compensation for any changes to the instrument s output signal due to reaction chamber pressure variations The effects of reaction chamber pressure changes on the analyzer s subsystems and output have been empirically determined This empirical data is used to compensate for any change in reaction chamber pressure When pressure compensation ...

Page 87: ...ation about the service mode see Service Menu later in this chapter Note The service mode should be turned off when finished as it prevents remote operation In the Main Menu choose Instrument Controls Service Mode SERVICE MODE CURRENTLY OFF SET TO ON TOGGLE VALUE RANGE AVG DIAGS ALARM The Date Time screen and allows the user to view and change the system date and time 24 hour format The internal c...

Page 88: ...S DIGITAL INPUTS RELAY STATES TEST ANALOG OUTPUTS INSTRUMENT CONFIGURATION CONTACT INFORMATION The Program Versions screen read only shows the version numbers of the programs installed Prior to contacting the factory with any questions regarding the instrument please note the product model program version numbers In the Main Menu choose Diagnostics Program Versions PROGRAM VERSIONS PRODUCT MODEL 4...

Page 89: ...tages Motherboard Voltages MOTHERBOARD VOLTAGES 3 3 SUPPLY 3 3 V 5 0 SUPPLY 5 0 V 15 0 SUPPLY 15 0 V 24 0 SUPPLY 24 0 V 3 3 SUPPLY 3 3 V RANGE AVG DIAGS ALARM The Interface Board screen read only is used to display the current voltage readings on the interface board In the Main Menu choose Diagnostics Voltages Interface Board Voltages INTERFACE BOARD VOLTAGES PMT SUPPLY 612 5 V FLASH SUPPLY 1000 0...

Page 90: ...The Temperatures screen read only displays the current internal instrument temperature and chamber temperature The internal temperature is the air temperature measured by a sensor located on the interface board In the Main Menu choose Diagnostics Temperatures TEMPERATURES INTERNAL 34 6 o C CHAMBER 49 7 o C PERM OVEN GAS 45 0 o C PERM OVEN HTR 45 0 o C RANGE AVG DIAGS ALARM The Pressure screen read...

Page 91: ...ime as the lamp degrades In the Main Menu choose Diagnostics Lamp Intensity LAMP INTENSITY 90 RANGE AVG DIAGS ALARM The Optical Span Test screen is used to turn the optical span test LED on or off and displays the SO2 concentration reading Within the fluorescence chamber is a light emitting diode LED which may be used to simulate a particular concentration of SO2 It is designed to provide a quick ...

Page 92: ... Vª RANGE AVG DIAGS ALARM IO8 0 0 V The Analog Input Voltages screen read only displays the 8 raw analog voltage readings if the I O expansion board option is installed In the Main Menu choose Diagnostics Analog Input Voltages ANALOG INPUT VOLTAGES ANALOG IN 1 6 24 V ANALOG IN 2 4 28 V ANALOG IN 3 0 00 V ANALOG IN 4 0 00 V ANALOG IN 5 0 00 V ANALOG IN 6 0 00 V ANALOG IN 7 0 00 Vª RANGE AVG DIAGS A...

Page 93: ... The relays are restored to their original states upon exiting this screen In the Main Menu choose Diagnostics Relay States Press to toggle the relay state open and closed RELAY STATE OUTPUT 1 1 OUTPUT 2 0 OUTPUT 3 0 OUTPUT 4 1 OUTPUT 5 0 OUTPUT 6 0 OUTPUT 7 0ª RANGE AVG DIAGS ALARM OUTPUT 8 0 OUTPUT 9 0 OUTPUT 10 0 The Test Analog Outputs menu contains a number of digital to analog converter DAC ...

Page 94: ...alog outputs to 0 volts and normal operation The example that follows shows the selected output state ALL is set to full scale In the Main Menu choose Diagnostics Test Analog Outputs ALL Voltage Channel 1 6 or Current Channel 1 6 TEST ANALOG OUTPUTS SETTING ALL OUTPUT SET TO FULL SCALE SET TO FULL SCALE ª SET TO ZERO RESET TO NORMAL RANGE AVG DIAGS ALARM The Instrument Configuration screen display...

Page 95: ...l go from OK to either LOW or HIGH respectively If the alarm is not a level alarm the status will go from OK to FAIL The number of alarms detected is displayed to indicate how many alarms have occurred If no alarms are detected the number zero is displayed To see the actual reading of an item and its minimum and maximum limits move the cursor to the item and press Items displayed are determined by...

Page 96: ...e minimum and maximum alarm limits Acceptable alarm limits range from 8 to 47 C If the internal temperature reading goes beyond either the minimum or maximum alarm limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu In the Main Menu choose Alarms Internal Temp INTERNAL TEMPERATURE ACTUAL 30 1 o C MIN 8 0 o C MAX 47 0 o C RANGE AVG DIAGS ALARM The Minimum Inter...

Page 97: ... in the Main Menu In the Main Menu choose Alarms Chamber Temp CHAMBER TEMPERATURE ACTUAL 45 4 o C MIN 43 0 o C MAX 47 0 o C RANGE AVG DIAGS ALARM The Minimum Chamber Temperature alarm limit screen is used to change the minimum chamber temperature alarm limit The minimum and maximum internal temperature screens function the same way In the Main Menu choose Alarms Chamber Temp Min or Max CHAMBER TEM...

Page 98: ...re screens function the same way In the Main Menu choose Alarms Pressure Min or Max PRESSURE ACTUAL MIN 400 0 mmHg SET MIN TO 500 0 mmHg ª INC DEC SAVE VALUE RANGE AVG DIAGS ALARM The Sample Flow screen displays the current sample flow reading and sets the minimum and maximum alarm limits Acceptable alarm limits range from 0 to 2 5 LPM If the sample flow reading goes beyond either the minimum or m...

Page 99: ... limits Acceptable alarm limits range from 20 to 100 percent If the lamp intensity reading goes beyond either the minimum or maximum limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu In the Main Menu choose Alarms Lamp Intensity LAMP INTENSITY ACTUAL 90 MIN 40 MAX 100 RANGE AVG DIAGS ALARM The Minimum Lamp Intensity alarm limit screen is used to change the m...

Page 100: ...200 V RANGE AVG DIAGS ALARM The Minimum Lamp Voltage alarm limit screen is used to change the minimum lamp voltage alarm limit The minimum and maximum lamp voltage screens function the same way In the Main Menu choose Alarms Lamp Voltage Min or Max LAMP VOLTAGE ACTUAL MIN 750 V SET MIN TO 700 V ª INC DEC SAVE VALUE RANGE AVG DIAGS ALARM The Zero Span Check screen allows the user to view the status...

Page 101: ...ecent auto background calibration The zero and span auto calibration screens are visible only if the auto calibration option is enabled and function the same way In the Main Menu choose Alarms Zero or Span Autocal ZERO AUTO CALIBRATION ALARM OK RESPONSE 1 2 RANGE AVG DIAGS ALARM The SO2 Concentration screen displays the current SO2 concentration and sets the maximum alarm limit Acceptable alarm li...

Page 102: ...ion the same way In the Main Menu choose Alarms SO2 Concentration Min or Max SO2 CONCENTRATION ACTUAL MIN 100 0 SET MIN TO 000400 0 MOVE CURSOR ª INC DEC SAVE VALUE RANGE AVG DIAGS ALARM The Minimum Trigger screen allows the user to view and set the SO2 concentration alarm trigger type to either floor or ceiling The minimum alarm may be programmed as a floor trigger alarm is triggered when the con...

Page 103: ...ose Service SERVICE FLASH VOLTAGE ADJUSTMENT INITIAL FLASH REFERENCE PMT SUPPLY SETTINGS RANGE MODE SELECT PRESSURE CALIBRATION FLOW CALIBRATION INPUT BOARD TEST ª RANGE AVG DIAGS ALARM TEMPERATURE CALIBRATION ANALOG OUT CALIBRATION ANALOG INPUT CALIBRATION PERM OVEN SETTINGS DILUTION RATIO DISPLAY PIXEL TEST RESTORE USER DEFAULTS The Flash Voltage Adjustment screen allows the user to manually adj...

Page 104: ...This adjustment should only be performed by an instrument service technician In the Main Menu choose Service Initial Flash Reference SET INITIAL FLASH REF CURRENT REF 1 50 V SAVE CURRENT REF VOLTS AS INITIAL RANGE AVG DIAGS ALARM The PMT Voltage Adjustment screen is used to manually adjust the PMT supply voltage The PMT voltage adjustment is visible only when the instrument is in service mode For ...

Page 105: ...GE AVG DIAGS ALARM The Pressure Calibration menu is used to calibrate the pressure sensor to zero span or restore factory default values The pressure calibration is visible only when the instrument is in service mode For more information on the service mode see Service Mode earlier in this chapter The pressure sensor s zero counts and span slope are displayed on the menu Note This adjustment shoul...

Page 106: ...RE RANGE AVG DIAGS ALARM The Calibrate Pressure Span screen allows the user to view and set the pressure sensor calibration span point Note The plumbing going to the pressure sensor should be disconnected so the sensor is reading ambient pressure before performing the span calibration The operator should use an independent barometer to measure the ambient pressure and enter the value on this scree...

Page 107: ...vice mode For more information on the service mode see Service Mode earlier in the chapter Note This adjustment should only be performed by an instrument service technician In the Main Menu choose Service Flow Calibration FLOW SENSOR CAL ZERO 200 SPAN 1 0000 SET DEFAULTS RANGE AVG DIAGS ALARM The Calibrate Flow Zero screen calibrates the flow sensor at zero flow Note The pump must be disconnected ...

Page 108: ...flow then the operator enters the flow value on this screen to perform the calibration In the Main Menu choose Service Flow Calibration Span CALIBRATE FLOW SPAN CURRENTLY 0 508 LPM SET TO 0 808 LPM MOVE CURSOR ª CHANGE VALUE SAVE RANGE AVG DIAGS ALARM The Restore Default Flow Calibration screen allows the user to reset the configuration values to factory defaults In the Main Menu choose Service Fl...

Page 109: ...e user to view and set the ambient temperature sensor calibration The temperature calibration is visible only when the instrument is in service mode For more information on the service mode see Service Mode earlier in the chapter Note This adjustment should only be performed by an instrument service technician In the Main Menu choose Service Temperature Calibration CALIBRATE AMBIENT TEMP CURRENTLY...

Page 110: ... state of the selected analog output The operator must connect a meter to the output and adjust the output until it reads 0 0 V on the meter In the Main Menu choose Service Analog Output Calibration Selected Channel Calibrate Zero ANALOG OUTPUT CAL ZERO CONNECT METER TO OUTPUT SELECTED OUTPUT V1 SET TO 200 SAVE VALUE ª INC DEC SET OUTPUT TO 0 0 V RANGE AVG DIAGS ALARM Analog Output Calibrate Zero ...

Page 111: ...T SELECTED OUTPUT V1 SET TO 3697 SAVE VALUE ª INC DEC SET OUTPUT TO 10 V RANGE AVG DIAGS ALARM The Analog Input Calibration menu is a selection of analog input to calibrate and allows the user to select the calibration action zero or span The analog input calibration is visible only when the instrument is in service mode For more information on the service mode see Service Mode earlier in the chap...

Page 112: ... Calibration Full Scale screen allows the user to calibrate the full scale state of the selected analog input In the Main Menu choose Service Analog Input Calibration Select Channel Calibrate Full Scale Hook up a voltage source of 10 V to the analog input channel ANALOG INPUT CAL SPAN PROVIDE VOLTAGE TO INPUT SELECTED INPUT INPUT 1 CURRENTLY 9 80 V SET TO 10 00 V CALIBRATE TO VALUE RANGE AVG DIAGS...

Page 113: ...ervice Perm Oven Settings PERM OVEN SETTINGS CAL GAS THERMISTOR CAL OVEN THERMISTOR PERM OVEN SELECTION FACTORY CAL GAS THERM FACTORY CAL OVEN THERM RANGE AVG DIAGS ALARM The Calibrate Gas Thermistor submenu is used for calibrating the permeation oven gas thermistor using a water bath or known resistance In the Main Menu choose Service Perm Oven Settings Cal Gas Thermistor Water Bath or Known Resi...

Page 114: ...OR ª CHANGE VALUE SAVE RANGE AVG DIAGS ALARM The Calibrate Oven Thermistor menu is used to view and set the permeation oven thermistor resistance to a known resistor value In the Main Menu choose Service Perm Oven Settings Cal Oven Thermistor CAL OVEN THERM RESISTOR CURRENTLY 3850 Ohms SET TO 04000 Ohms MOVE CURSOR ª CHANGE VALUE SAVE RANGE AVG DIAGS ALARM The Permeation Oven Setpoint screen is us...

Page 115: ... HIGH POINT SET DEFAULTS RANGE AVE DIAGS ALARM The Calibrate Gas Thermistor Low Point screen allows the user to view and set the permeation oven thermistor resistance The low and high point screens function the same way In the Main Menu choose Service Perm Oven Settings Factory Cal Gas Therm Low Point CAL GAS THERM LOW POINT CURRENTLY 3850 Ohms SET TO 04000 Ohms MOVE CURSOR ª CHANGE VALUE SAVE RAN...

Page 116: ...ults In the Main Menu choose Service Perm Oven Settings Factory Cal Oven Therm FACTORY CAL OVEN THERM LOW POINT HIGH POINT SET DEFAULTS RANGE AVE DIAGS ALARM The Calibrate Oven Thermistor Low Point screen allows the user to view and set the permeation oven thermistor resistance The low and high point screens function the same way In the Main Menu choose Service Perm Oven Settings Factory Cal Oven ...

Page 117: ... the dilution ratio Acceptable values are 1 500 1 The default is 1 1 When this value is set the dilution ratio is applied to all concentration measurements This screen is only accessible if the dilution ratio option is installed In the Main Menu choose Service Dilution Ratio DILUTION RATIO CURRENTLY 001 0 1 SET TO 002 0 1 MOVE CURSOR ª CHANGE VALUE SAVE The Display Pixel Test is used to test the L...

Page 118: ...enu allows the user to configure password protection If the instrument is locked none of the settings may be changed via the front panel user interface The items visible under the password menu are determined by the instrument s password status In the Main Menu choose PasswordSet PASSWORD MENU SET PASSWORD LOCK INSTRUMENT CHANGE PASSWORD REMOVE PASSWORD UNLOCK INSTRUMENT RANGE AVG DIAGS ALARM The ...

Page 119: ...is shown if the instrument is unlocked and the password is set In the Main Menu choose Password Lock Instrument LOCK FRONT PANEL XXXPRESSING ENTER WILLXXXX PREVENT USER FROM CHANGING XCONFIG FROM FRONT PANELXX LOCK AND RETURN TO RUN RANGE AVG DIAGS ALARM The Change Password is used to set or change the password used to unlock the instrument s front panel The change password screen is shown if the ...

Page 120: ...e Main Menu choose Password Remove Password REMOVE PASSWORD PRESSING ENTER WILL REMOVE CURRENT PASSWORD AND DISABLE LOCKING REMOVE PASSWORD RANGE AVG DIAGS ALARM The Unlock Instrument screen is used to enter the password to unlock the front panel The unlock instrument is shown if the instrument is locked In the Main Menu choose Password Unlock Instrument ENTER NEW PASSWORD R E ABCDEFGHIJKLMN BKSP ...

Page 121: ...n or zero span check should be the same as that used during normal monitoring Third all operational adjustments to the instrument should be completed prior to calibration Fourth all parts of the gas flow system such as sample lines and particulate filters which are used in normal monitoring should also be used during calibration Finally it is recommended that the recording devices and outputs used...

Page 122: ...ard flow instruments with higher flow rates will require a higher minimum calibration system flow rate All calibration gas should be derived from local or working standards such as cylinders of compressed gas or permeation devices that are certified as traceable to an NIST primary standard A cylinder gas dilution system shown in Figure 4 1 can be constructed All connections between components in t...

Page 123: ... and 760 mm Hg Commercial precision dilution systems are available which reliably and accurately dilute a high concentration gas mixture to provide a reliable span gas A high concentration 50 ppm of SO2 in air is precisely diluted to the concentration range required The Thermo Scientific Model 146 Multigas Calibration System is one such system for precision dilution Permeation tube systems which p...

Page 124: ...rate Ensure all devices are properly calibrated and that all flows are corrected to 25 C and 1 atm Figure 4 2 Permeation Tube System The SO2 output level is calculated from F K x P SO T OUT 2 Where SO2 OUT SO2 output concentration in ppm P permeation rate in μg min FT total flow rate of gas after mixing chamber FP FD in liters minute K SO2 0 382 constant for SO2 permeant Commercial permeation syst...

Page 125: ...itching from sample to zero and from zero to span This transition time is the time required to purge the existing air Depending on the plumbing configuration and the instrument data from approximately the first minute of a zero calibration or check should be disregarded because of residual sample air Also data from approximately the first minute of a span calibration or check should be disregarded...

Page 126: ...O2 reading to zero The display flashes the message SAVING and the SO2 reading is added to the background correction Record the stable zero air reading as ZSO2 6 Press to return to the Calibration menu 7 Connect a source of calibration gas to the SAMPLE bulkhead The calibration gas concentration should be approximately 80 of the full scale range 8 To ensure that the calibration gas is being measure...

Page 127: ...oncentration after allowing time for both gas generation system and instrument to stabilize Plot a graph of instrument readings against the SO2 concentrations generated This is the instrument calibration curve All future measurements should be interpreted using this curve Regulations typically require multipoint calibration when the instrument is newly installed moved repaired interrupted for more...

Page 128: ...es which mode is active ZERO SPAN or SAMPLE 2 To ensure that the zero air is being measured at atmospheric pressure check that the zero air flow reported by the analyzer is approximately 0 5 LPM Actual zero air flow should be 0 8 LPM or more with the excess leaving out the atmospheric bypass a From the Run screen press to display the Main Menu b From the Main Menu choose Diagnostics Flow to displa...

Page 129: ... The first line of the display shows the current SO2 reading The second line of the display is where you enter the high calibration gas concentration 11 To enter the high calibration gas concentration use to move the cursor left and right Use to increment and decrement the digit Press to calibrate the instrument to the high SO2 calibration gas The display flashes the message SAVING and the correct...

Page 130: ...s the message SAVING and the corrected SO2 reading is displayed 19 Press to return to the Calibration menu 20 Generate five SO2 concentrations equally spaced between zero and the concentration above 21 Record instrument reading for each concentration after allowing time for both gas generation system and instrument to stabilize 22 Plot a graph of instrument readings against the SO2 concentrations ...

Page 131: ...r is used to activate the zero and span valves The lower left hand corner of the Run screen indicates which mode is active ZERO SPAN or SAMPLE 2 To ensure that the zero air is being measured at atmospheric pressure check that the flow reported by the analyzer is approximately 0 5 LPM Actual zero air flow should be 0 8 LPM or more with the excess flowing out the atmospheric bypass a From the Run sc...

Page 132: ...low is approximately 0 5 LPM or more with the excess flowing out the atmospheric bypass 7 Press to monitor the span gas reading and wait for the reading to stabilize 8 Record the difference between the measured SO2 value and the actual SO2 span concentration used This is the span drift since the last adjustment If the calibration has changed by more than 10 a new calibration should be performed ...

Page 133: ...on page 5 2 Cleaning the Mirrors on page 5 2 Fan Filter Inspection and Cleaning on page 5 4 Sample Particulate Filter Inspection on page 5 5 Lamp Voltage Check on page 5 5 Leak Test on page on page 5 6 Pump Rebuilding on page 5 6 Read the safety precautions before beginning any procedures in this chapter WARNING If the equipment is operated in a manner not specified by the manufacturer the protect...

Page 134: ...ittings cracked or clogged Teflon lines and excessive dust or dirt accumulation Dust and dirt can accumulate in the instrument and can cause overheating or component failure Dirt on the components prevents efficient heat dissipation and may provide conducting paths for electricity The best way to clean the inside of the instrument is to first carefully vacuum all accessible areas and then blow awa...

Page 135: ...ly ground antistatic wrist strap must be worn while handling any internal component For more information about appropriate safety precautions see the Servicing chapter Use the following procedure to inspect and replace the capillary 1 Turn the instrument OFF and unplug the power cord 2 Remove the instrument cover 3 Locate the capillary holder Figure 5 1 and unscrew the knurled cap nut Figure 5 1 I...

Page 136: ...the rear panel of the instrument should be cleaned and reconditioned at six month intervals If the instrument is operated in excessively dirty surroundings this procedure should be instituted on a more frequent schedule Use the following procedure to inspect and clean the fan filter Figure 5 1 Equipment Damage Some internal components can be damaged by small amounts of static electricity A properl...

Page 137: ...s for degradation of the flash lamp However after several years of use the lamp may have degraded to the point that is being driven with the maximum voltage that the power supply can deliver Use the following procedure to check the lamp voltage 1 Press to display the Main Menu 2 From the Main Menu select Diagnostics Voltages Interface Board and press to display the Interface Board Voltages screen ...

Page 138: ...ess to display the Sample Flow screen The flow reading should indicate zero flow 6 Press to display the Diagnostics Menu then press to move the cursor to Pressure and press to display the Pressure screen The pressure reading should be less than 180 mm Hg If not check to see that all fittings are tight and that none of the input lines are cracked or broken For detailed information about these scree...

Page 139: ...cord and remove the cover 2 Loosen the fittings and remove both lines going to the pump 3 Remove the four screws from the top plate remove top plate flapper valve and the bottom plate Figure 5 2 4 Remove the screw the securing the diaphragm to piston and remove diaphragm 5 Assemble the pump by following the previous steps in reverse make sure the Teflon white side of the diaphragm is facing up and...

Page 140: ...ce Pump Rebuilding 5 8 Model 43i Trace Level Enhanced Instruction Manual Thermo Fisher Scientific 6 Check that the flow reads approximately 0 5 LPM when power is turned ON 7 Perform a leak test as described in this chapter ...

Page 141: ...be consulted in the event of problems See Service Locations at the end of this chapter for contact information In any correspondence with the factory please note both the serial number and program number of the instrument This chapter provides the following troubleshooting information Safety Precautions on page 6 1 Troubleshooting Guides on page 6 1 Board Level Connection Diagrams on page 6 10 Con...

Page 142: ...ion Unplug the power cord disconnect the switch and check operation with a multimeter Display does not come on Pump is running DC power supply failure Check the green LED on the back edge of the power supply If the LED is off the supply has failed DC power distribution failure Check surface mount LEDs labelled 24V PWR on the motherboard and the interface board If lit power is OK Display failure If...

Page 143: ...ent flow meter to check flows at the sample inlet and exhaust bulkheads they should match Perform a leak test as described in the Preventive Maintenance chapter Span gas containing SO2 NO or a hydrocarbon is contaminating system Verify that span gases connected to the calibration system are shut off and leak tight Internal or external lines filters and other sample handling equipment are contamina...

Page 144: ...es made of vinyl or other plastics with fresh Teflon or stainless steel Replace Teflon filter membranes that look dirty Remove any filters that are not Teflon membranes Flash lamp has failed Listen for the rapid clicking of the flash lamp Check the flash lamp voltage and intensity PMT or input board has failed Check the PMT voltage and run the optical span test A good optical span test indicates t...

Page 145: ...hooting Measurement Failures Malfunction Possible Cause Action Reduced response or no response to sample gas with alarm s indicated Undefined electronic failure or pump failure Check alarm screens and the diagnostic voltage screen to localize fault Check the response to known span gas Run an optical span test Instrument is not drawing in sample as expected Check sample Flow and Pressure readings o...

Page 146: ...hen disconnect the signal cable from the input board The signal should drop from a value above 1000 to near zero PMT failure Check the PMT voltage Service menu Flash lamp assembly failure Check the lamp voltage Service menu Span calibration coefficient outside acceptable limits of 0 5 2 0 Bad span gas Verify quality of span gas System leak Perform leak test Insufficient calibrator flow Verify cali...

Page 147: ...readings on the Diagnostics screen Use an independent flow meter to check flows at the sample inlet and exhaust bulkheads they should match Perform a leak test as described in the Preventive Maintenance chapter SO2 is being absorbed and or released by dirt in the tubing or filters of the sampling system or inside the instrument Replace any lines made of vinyl or other plastics with fresh Teflon or...

Page 148: ...or leaks Check the pump for a tear in the diaphragm replace with pump repair kit if necessary Refer to the Preventive Maintenance chapter in this manual Check that capillary is properly installed and O rings are in good shape Replace if necessary Alarm Flow Flow low Check sample capillary for blockage Replace as necessary If using sample particulate filter make sure it is not blocked Disconnect sa...

Page 149: ...point be sure the min trigger is set as desired Alarm Zero Check Alarm Span Check Instrument out of calibration Recalibrate instrument Alarm Zero Autocal Alarm Span Autocal Check gas supply Perform manual calibration Alarm Motherboard Status Alarm Interface Status Alarm I O Exp Status Internal cables not connected properly Board is defective Check that all internal cables are connected properly Re...

Page 150: ...PANSION RS485 ANALOG OUTPUTS DIGITAL INPUTS P1 A P1 B RS232 RS485 J2 10 BASE T J15 J5 15 Pin 8 Pin 37 Pin 9 Pin 9 Pin RS232 RS485 J1 EXPANSION I O J2 25 Pin 37 Pin AC AC REAR PANEL AC INPUT 3 Cond AC POWER_GOOD 24VDC TRANSFO RMER 90V ACor 240V AC OPTIO NS J4 8 Pin SPARE DATA DATA TOMEA SUREMENTSY STEM Figure 6 1 and Figure 6 2 are board level connection diagrams for the common electronics and meas...

Page 151: ... Pin 3 Pin AC AC PUMP 3 Pin 4 Pin NTJ PJ5 AC AC BENCH HEATER AND 4 Pin PRESSURE 5 Pin FLOW INPUT BOARD 7 Pin HVPS PM 2 Cond 3 Pin 2 Cond Coax FJ1 MJ9 MJ10 MJ1 J1 FAN 2 Pin PJ4 2 Pin CONVERTER SOL Not 2 Pin SAMPLE SOL 2 Pin AMBIENT TEMP THERM ZERO SPAN 2 Pin PJ7 PJ8 PJ9 4 Pin 2 Pin GAS THERM HEATER 15V 1W OVEN THERM MJ1 2 Pin SPAN 2 SOL PJ10 POJ POJ PERM OVEN optional FLASH INTENSITY TRIGGER PAK 4 ...

Page 152: ...l Reference Designator Pin Signal Description INTF DATA J1 1 Ground 2 RS485 to Interface Board 3 RS485 to Interface Board 10 BASE T J2 1 Ethernet Output 2 Ethernet Output 3 Ethernet Input 4 NC 5 NC 6 Ethernet Input 7 NC 8 NC EXPANSION BD J3 1 5V 2 24V 3 24V 4 Ground 5 Ground 6 Ground 7 RS485 to Expansion Board 8 RS485 to Expansion Board SPARE DATA J4 1 5V 2 24V 3 24V 4 Ground 5 Ground 6 Ground 7 R...

Page 153: ... TTL Input 15 13 Ground 14 Analog Voltage Output 1 15 Analog Voltage Output 3 16 Ground 17 Analog Voltage Output 5 18 Ground 19 Ground 20 Power Fail Relay COM 21 Power Fail Relay N O Contact 22 Ground 23 TTL Input 3 24 TTL Input 4 25 TTL Input 6 26 Ground 27 TTL Input 9 28 TTL Input 11 29 TTL Input 12 30 TTL Input 14 31 TTL Input 16 32 Ground 33 Analog Voltage Output 2 34 Analog Voltage Output 4 3...

Page 154: ... J10 1 24V 2 Ground DIGITAL OUTPUT J14 1 5V 2 24V 3 24V 4 Ground 5 Ground 6 Ground 7 SPI Reset 8 SPI Input 9 SPI Output 10 SPI Board Select 11 SPI Clock EXT RS485 J15 1 RS485 to Rear Panel 2 RS485 to Rear Panel 3 5V 4 5V 5 5V 6 Ground 7 Ground 8 Ground 9 NC 10 NC 11 24V 12 24V 13 24V 14 24V 15 24V 24V MONITOR J17 1 24V Power Monitor 2 Ground FRONT PANEL BD J18 1 Ground 2 Ground 3 LCLK LCD Signal ...

Page 155: ... Signal 11 LD1 LCD Signal 12 LD6 LCD Signal 13 LD2 LCD Signal 14 LD7 LCD Signal 15 LD3 LCD Signal 16 LCD Bias Voltage 17 5V 18 Ground 19 Ground 20 LCD_ONOFF LCD Signal 21 Keypad Row 2 Input 22 Keypad Row 1 Input 23 Keypad Row 4 Input 24 Keypad Row 3 Input 25 Keypad Col 2 Select 26 Keypad Col 1 Select 27 Keypad Col 4 Select 28 Keypad Col 3 Select 29 Ground 30 Ground 31 Ground 32 Ground 33 24V 34 24...

Page 156: ...IN 3 Serial Port 2 TX RS485 OUT 4 NC 5 Ground 6 NC 7 Serial Port 2 RTS RS485 OUT 8 Serial Port 2 CTS RS485 IN 9 NC AC IN PJ1 1 AC HOT 2 AC NEUT 3 AC Ground AC 24VPWR PJ2 1 AC HOT 2 AC NEUT 3 AC Ground AC INTF BD PJ3 1 AC HOT 2 AC NEUT 3 AC Ground Table 6 6 Measurement Interface Board Connector Pin Descriptions Connector Label Reference Designator Pin Signal Description DATA IPJ8 1 Ground 2 RS485 f...

Page 157: ...ound 6 Measurement Frequency Output 7 Sample Hold 8 NC 9 GAIN A 10 GAIN B HVPS MJ9 1 HV Power Supply Voltage Adjust 2 Ground 3 HV Power Supply On Off 4 Ground 5 HV Power Supply Voltage Monitor 6 Ground 7 Ground PRES MJ10 1 Pressure Sensor Input 2 Ground 3 15V 4 15V FLOW MJ11 1 Flow Sensor Input 2 Ground 3 15V 4 15V 5 Ground LED MJ14 1 LED Drive 2 LED Supply AMB TEMP MJ15 1 Ambient Temperature Ther...

Page 158: ... 4 Ground 5 15V 6 15V 24V IN P1 1 24V 2 Ground AC PUMP PJ5 1 AC HOT 2 AC NEUT 3 AC Ground FAN PJ4 1 24V 2 Ground AC IN PJ3 1 AC HOT 2 AC NEUT 3 AC Ground AC CONVERTER PJ12 1 AC HOT 2 AC NEUT 3 AC Ground Z S SOL PJ7 1 24V 2 Zero Span Solenoid Control SAMPLE SOL PJ8 1 24V 2 Sample Solenoid Control CONV SOL PJ9 1 24V 2 Spare 1 Solenoid Control SPAN2 SOL PJ10 1 24V 2 Spare 2 Solenoid Control PERM OVEN...

Page 159: ...l Description MOTHER BOARD J1 1 Ground 2 Ground 3 LCLK LCD Signal 4 Ground 5 Ground 6 LLP LCD Signal 7 LFLM LCD Signal 8 LD4 LCD Signal 9 LD0 LCD Signal 10 LD5 LCD Signal 11 LD1 LCD Signal 12 LD6 LCD Signal 13 LD2 LCD Signal 14 LD7 LCD Signal 15 LD3 LCD Signal 16 LCD Bias Voltage 17 5V 18 Ground 19 Ground 20 LCD_ONOFF LCD Signal 21 Keypad Row 2 Input 22 Keypad Row 1 Input 23 Keypad Row 4 Input 24 ...

Page 160: ...5V LCD Signal 2 LD1_5V LCD Signal 3 LD2_5V LCD Signal 4 LD3_5V LCD Signal 5 LCD_ONOFF_5V LCD Signal 6 LFLM_5V LCD Signal 7 NC 8 LLP_5V LCD Signal 9 LCLK_5V LCD Signal 10 5V 11 Ground 12 25V 13 LCD Bias Voltage 14 Ground KEYBOARD J3 1 Keypad Row 1 Input 2 Keypad Row 2 Input 3 Keypad Row 3 Input 4 Keypad Row 4 Input 5 Keypad Col 1 Select 6 Keypad Col 2 Select 7 Keypad Col 3 Select 8 Keypad Col 4 Sel...

Page 161: ...4 Ground 5 Analog Voltage Input 4 6 Analog Voltage Input 5 7 Analog Voltage Input 6 8 Ground 9 Analog Voltage Input 7 10 Analog Voltage Input 8 11 Ground 12 NC 13 Current Output Return 14 Ground 15 Current Output 1 16 Current Output Return 17 Current Output 2 18 Current Output Return 19 Current Output 3 20 Current Output Return 21 Current Output 4 22 Current Output Return 23 Current Output 5 24 Cu...

Page 162: ...PI Output 10 SPI Board Select 11 SPI Clock DIGITAL OUTPUTS J2 1 Relay 1 Contact a 2 Relay 2 Contact a 3 Relay 3 Contact a 4 Relay 4 Contact a 5 Relay 5 Contact a 6 Relay 6 Contact a 7 Relay 7 Contact a 8 Relay 8 Contact a 9 Relay 9 Contact a 10 Relay 10 Contact a 11 NC 12 Solenoid Drive Output 1 13 Solenoid Drive Output 2 14 Solenoid Drive Output 3 15 Solenoid Drive Output 4 16 Solenoid Drive Outp...

Page 163: ...lay 5 Contact b 25 Relay 6 Contact b 26 Relay 7 Contact b 27 Relay 8 Contact b 28 Relay 9 Contact b 29 Relay 10 Contact b 30 24V 31 24V 32 24V 33 24V 34 24V 35 24V 36 24V 37 24V Table 6 10 Input Board Connector Pin Descriptions Connector Label Reference Designator Pin Signal Description PMT IN J1 1 PMT Input 2 Ground INTF BD J2 1 15V 2 Ground 3 15V 4 5V 5 Ground 6 Measurement Frequency Output 7 Sa...

Page 164: ...Trigger 3 Ground Table 6 12 Flash Intensity Assembly Pin Descriptions Connector Label Reference Designator Pin Signal Description FLASH INT 1 15V 2 15V 3 Ground 4 Lamp Intensity For additional assistance service is available from exclusive distributors worldwide Contact one of the phone numbers below for product support and technical information or visit us on the web at www thermo com aqi 1 866 2...

Page 165: ...s at the end of this chapter Read the safety precautions before beginning any procedures in this chapter WARNING The service procedures in this manual are restricted to qualified representatives If the equipment is operated in a manner not specified by the manufacturer the protection provided by the equipment may be impaired CAUTION Carefully observe the instructions in each procedure Equipment Da...

Page 166: ... not use alcohol acetone MEK or other Ketone based or aromatic solvents to clean the LCD module use a soft cloth moistened with a naphtha cleaning solvent Do not place the LCD module near organic solvents or corrosive gases Do not shake or jolt the LCD module Figure 7 1 Properly Grounded Antistatic Wrist Strap The firmware can be updated by the user in the field via the serial port or over the Eth...

Page 167: ...ard 100542 00 I O Expansion Board Optional 102340 00 Front Panel Connector Board 102496 00 Front Panel Display 101399 00 Transformer Step Down 220 240V Optional 101863 00 Transformer 100V Step up Transformer 100862 00 Measurement Interface Board Assembly 100883 00 Input Board Assembly 8392 Trigger Board Assembly 101023 00 Pressure Transducer Assembly 102055 00 Flow Transducer 8666 Lamp Flashtube 8...

Page 168: ...g 4119 Capillary 0 008 inch ID Perm Oven Option Table 7 2 describes the Model 43i Trace Level Enhanced cables See the Troubleshooting chapter for associated connection diagrams and board connector pin descriptions Table 7 2 Model 43i Trace Level Enhanced Cables Part Number Description 101036 00 00DC Power Supply 24V Output 101037 00 115VAC Supply to Measurement Interface Board 101048 00 RS 485 Dat...

Page 169: ...rminal Block and Cable Kit DB25 optional 101556 00 Terminal Block and Cable Kit DB37 optional 102645 00 Cable DB37M to Open End Six Feet optional 102646 00 Cable DB37F to Open End Six Feet optional 102659 00 Cable DB25M to Open End Six Feet optional 6219 Cable RS 232 optional 102888 00 Terminal Board PCB Assembly DB37F standard with all instruments 102891 00 Terminal Board PCB Assembly DB37M stand...

Page 170: ...lowering the partition panel Figure 7 3 Removing the Measurement Bench and Lowering the Partition Panel Measurement Interface Board Reaction Chamber Assy Mirror Housing Assy Flash Intensity Assy PMT Assy Chamber Inlet Assy Flash Lamp Housing Flash Trigger Assy Kicker Assy Fan Pump Solenoid Valves Opt I O Expansion Board Opt Digital Output Board Mother Board Input Board Assy HVPS Power Supply Front...

Page 171: ...n be damaged by small amounts of static electricity A properly ground antistatic wrist strap must be worn while handling any internal component 1 Turn instrument OFF and unplug the power cord 2 If the instrument is mounted in a rack remove it from the rack 3 Remove the cover 4 Disconnect the plumbing connections at the rear of the measurement bench Pass Through Connectors Partition Panel Loosen Ca...

Page 172: ... partition panel securing the top of partition panel to the measurement bench and lower the panel being careful not to put excessive tension on the cables 11 Replace the measurement bench by following previous steps in reverse Use the following procedure to replace the fuse Equipment Required Replacement fuses refer to the Replacement Parts List in this chapter 1 Turn instrument OFF and unplug the...

Page 173: ... unplug the power cord and remove the cover 2 Disconnect the pump power cable from the AC PUMP connector on the measurement interface board 3 Remove both lines from the pump 4 Loosen the four captive screws holding the pump bracket to the shock mounts and remove the pump assembly Figure 7 4 Replacing the Pump 5 Install the new pump by following the previous steps in reverse 6 Perform a leak test a...

Page 174: ...unts of static electricity A properly ground antistatic wrist strap must be worn while handling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Remove the fan guard from the fan and remove the filter 3 Pull the power connector off the fan 4 Remove the four fan mounting screws and remove the fan 5 Install a new fan following the previous steps in reverse Fi...

Page 175: ...ty assembly cable from the FLASH INT connector on the measurement interface board b Heater cable from AC BENCH connector on the measurement interface board c PMT BNC cable from the input board connector d PMT power cable from the HVPS e LED cable from the LED connector on the measurement interface board f Flasher assembly from the FLASH TRIG connector on the measurement interface board g Green gro...

Page 176: ...tical bench These mirrors do not come in contact with the sample gas and should not be cleaned Cleaning the mirrors can damage the mirrors Use the following procedure to replace the flash lamp Figure 7 7 Equipment Required Flash lamp Philips screwdriver Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly ground antistatic wrist strap must be w...

Page 177: ... 4 Loosen the retaining screw on the top of the lamp housing and pull out the socket assembly and lamp Figure 7 7 Replacing the Flash Lamp and Flash Trigger Assembly 5 Remove the old lamp from the socket assembly by pulling straight out and insert the new lamp 6 Insert the socket assembly into the lamp housing tighten the retaining screw and reconnect the flash trigger cable 7 Re install the bench...

Page 178: ...this chapter then return to the beginning of this step 10 At the Set Flash Voltage Adjustment Man screen use until the SUPPLY voltage is 1000V 11 Press to store the value 12 Perform a PMT Voltage Adjustment and recalibrate the instrument Refer to PMT Voltage Adjustment in this chapter and the calibration procedures in the Calibration chapter Use the following procedure to replace the flash trigger...

Page 179: ... retaining screw and reconnect the flash trigger cable 7 Re install the bench Use the following procedure to replace the flash intensity assembly Equipment Required Flash intensity assembly Phillips screwdriver small Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly ground antistatic wrist strap must be worn while handling any internal compo...

Page 180: ...hilips screwdriver Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly ground antistatic wrist strap must be worn while handling any internal component 1 Turn analyzer OFF unplug the power cord and remove the cover 2 Disconnect the high voltage cable from the PMT power supply cable connector and unplug the BNC cable from the input board connec...

Page 181: ...ll a new PMT follow previous steps in reverse 6 Perform a photomultiplier tube calibration See PMT Voltage Adjustment in this chapter Use the following procedure to replace the PMT high voltage power supply Figure 7 10 Equipment Required PMT high voltage power supply Philips screwdriver Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly groun...

Page 182: ...supply towards the rear slightly and lift it off the base screws Figure 7 10 Replacing the PMT High Voltage Power Supply HVPS 4 Loosen two screws on the input box assembly and lift the input box assembly off the bracket 5 Remove the four screws securing the power supply to the bracket and remove the power supply 6 To install the power supply follow the previous steps in reverse 7 Recalibrate the i...

Page 183: ...OEF to 1 000 4 Set the Averaging Time to 10 seconds Refer to Averaging Time in the Operation chapter 5 Connect the calibration gas and allow the instrument to sample calibration gas until the reading stabilizes 6 From the Main Menu press to scroll to Service press to scroll to PMT Supply Settings and press The PMT Supply Settings screen appears Note If Service Mode is not displayed refer to Access...

Page 184: ...ound antistatic wrist strap must be worn while handling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect all the power supply electrical connections Note connector locations to facilitate re connection 3 Loosen the captive screw securing the power supply to the chassis plate and lift out the power supply 4 To install the DC power supply follow th...

Page 185: ...tics press to scroll to Test Analog Outputs and press The Test Analog Outputs screen displays 3 Press to scroll to the desired channel corresponding to the rear panel terminal pins where the meter is connected and press The Set Analog Outputs screen displays 4 Press to set the output to zero The Output Set To line displays Zero 5 Check that the meter is displaying a zero value If the meter reading...

Page 186: ... Rear Panel Analog Input and Output Pins Table 7 4 Analog Output Channels and Rear Panel Pin Connections Voltage Channel Pin Current Channel Pin 1 14 1 15 2 33 2 17 3 15 3 19 4 34 4 21 5 17 5 23 6 36 6 25 Ground 16 18 19 35 37 Current Output Return 16 18 20 22 24 Current Outputs Analog Voltage Inputs Analog Voltage Outputs ...

Page 187: ...er to the channel to be adjusted and set to voltage or current as appropriate Figure 7 12 shows the analog output pins and Table 7 4 identifies the associated channels 2 From the Main Menu press to scroll to Service press to scroll to Analog Out Calibration and press The Analog Output Cal screen displays Note If Service Mode is not displayed refer to Accessing the Service Mode in this chapter then...

Page 188: ...ter replacing the optional I O expansion board These procedures include selecting analog input channels calibrating them to zero volts and then calibrating them to full scale using a known voltage source Use the following procedure to calibrate the input channels to zero volts 1 From the Main Menu press to scroll to Service press to scroll to Analog Input Calibration and press The Analog Input Cal...

Page 189: ...to calibrate the input channels to full scale by applying a known voltage to the channels Equipment Required DC voltage source greater than 0 volts and less than 10 volts 1 Connect the known DC voltage source to the input channel 1 8 to be calibrated Figure 7 12 shows the analog output pins and Table 7 4 identifies the associated channels 2 From the Main Menu press to scroll to Service press to sc...

Page 190: ...by small amounts of static electricity A properly ground antistatic wrist strap must be worn while handling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect plumbing from the pressure transducer assembly Note the plumbing connections to facilitate reconnection 3 Disconnect the pressure transducer cable from the measurement interface board 4 Loose...

Page 191: ...s available and not a vacuum pump adjust only the span setting A rough check of the pressure accuracy can be made by obtaining the current barometric pressure from the local weather station or airport and comparing it to the pressure reading However since these pressures are usually corrected to sea level it may be necessary to correct the reading to local pressure by subtracting 0 027 mm Hg per f...

Page 192: ...u appears Note If Service Mode is not displayed refer to Accessing the Service Mode in this chapter then return to the beginning of this step 4 At the Pressure Sensor Cal screen press to select Zero The Calibrate Pressure Zero screen appears 5 Wait at least 10 seconds for the zero reading to stabilize then press to save the zero pressure value 6 Disconnect the pump from the pressure transducer 7 P...

Page 193: ...component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect the plumbing connections from the flow transducer Note the plumbing connections to facilitate reconnection 3 Disconnect the flow transducer cable from the FLOW connector on the measurement interface board 4 Remove the two screws securing the flow transducer to the kicker bracket and remove the flow transducer 5...

Page 194: ...service procedures in this manual are restricted to qualified representatives If the equipment is operated in a manner not specified by the manufacturer the protection provided by the equipment may be impaired Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly ground antistatic wrist strap must be worn while handling any internal component 1 ...

Page 195: ...beginning of this step 4 At the Flow Sensor Cal screen press to select Zero The Calibrate Flow Zero screen appears 5 Wait at least 10 seconds for the zero reading to stabilize then press to save the zero flow value 6 Reconnect the pump cable to the AC PUMP connector on the measurement interface board 7 Connect a calibrated flow sensor at the SAMPLE bulkhead on the rear panel 8 Press to return to t...

Page 196: ...n instrument OFF unplug the power cord and remove the cover 2 Disconnect heaters from the AC BENCH cable 3 Using the 5 32 inch wrench remove the four screws securing the optical bench to the floor plate Figure 7 6 4 Lift the optical bench from the floor plate to gain access to the heater assembly 5 Remove two retaining screws and washers from each heater and remove the heaters Figure 7 15 6 Apply ...

Page 197: ...Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly ground antistatic wrist strap must be worn while handling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect the plumbing connections from the flow transducer the optical bench and the rear bulkhead Note the plumbing connections to facilitate ...

Page 198: ...nt temperature thermistor Figure 7 17 Equipment Required Thermistor Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly ground antistatic wrist strap must be worn while handling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Squeeze the thermistor latch and pull the thermistor from the AMB TEMP connec...

Page 199: ...WARNING The service procedures in this manual are restricted to qualified representatives If the equipment is operated in a manner not specified by the manufacturer the protection provided by the equipment may be impaired Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly ground antistatic wrist strap must be worn while handling any internal ...

Page 200: ...ot NIST traceable 3 From the Main Menu press to scroll to Service press to scroll to Temperature Calibration and press The Calibrate Ambient Temperature screen appears Note If Service Mode is not displayed refer to Accessing the Service Mode in this chapter then return to the beginning of this step 4 Wait at least 10 seconds for the ambient reading to stabilize use and to enter the known temperatu...

Page 201: ... previous steps in reverse Use the following procedure to replace the optional I O expansion board Figure 7 19 Note After replacing the optional I O expansion board calibrate the current outputs and the analog voltage inputs See the Analog Output Calibration procedure and the Analog Input Calibration procedure in this chapter Equipment Required I O expansion board Nut driver 3 16 inch I O Expansio...

Page 202: ...2 Unplug the I O expansion board cable from the EXPANSION BD connector on the motherboard 3 Remove the two standoffs holding the I O expansion board connector to the rear panel Figure 7 20 4 Pop off the board from the mounting studs and remove the board 5 To install the I O expansion board follow previous steps in reverse 6 Calibrate the analog current outputs and analog voltage inputs per the pro...

Page 203: ...f static electricity A properly ground antistatic wrist strap must be worn while handling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Remove the I O expansion board optional if used See the I O Expansion Board Replacement procedure in this chapter 3 Disconnect the digital output board ribbon cable from the motherboard 4 Using the nut driver remove the ...

Page 204: ...ndling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Remove the I O expansion board optional if used See the I O Expansion Board Replacement procedure in this chapter 3 Remove the digital output board See the Digital Output Board Replacement procedure in this chapter 4 Unplug all connectors from the motherboard Note connector locations to facilitate reco...

Page 205: ...Removing the Measurement Bench and Lowering the Partition Panel in this chapter to lower the partition panel then proceed to the next step below 2 Unplug all connectors Note the locations of the connectors to facilitate reconnection 3 Unscrew the two screws at the top of the measurement interface board Pop off the measurement interface board from the two bottom mounting studs and remove the board ...

Page 206: ...by small amounts of static electricity A properly ground antistatic wrist strap must be worn while handling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Remove the three ribbon cables and the two wire connector from the front panel board 3 Pop off the board from the two top mounting studs and remove the board by lifting it up and off the slotted bottom ...

Page 207: ...mponents can be damaged by small amounts of static electricity A properly ground antistatic wrist strap must be worn while handling any internal component Do not remove the panel or frame from the module The polarizing plate is very fragile handle it carefully Do not wipe the polarizing plate with a dry cloth it may easily scratch the plate Do not use alcohol acetone MEK or other Ketone based or a...

Page 208: ...anel board 3 Remove the four screws at the corners of the LCD module 4 Slide the LCD module out towards the top of the instrument 5 Replace the LCD module by following previous steps in reverse For additional assistance service is available from exclusive distributors worldwide Contact one of the phone numbers below for product support and technical information or visit us on the web at www thermo...

Page 209: ...tructure and includes a description of the system electronics and input output connections and functions as follows Model 43i Trace Level Enhanced hardware components Figure 8 1 include Hydrocarbon kicker Optics Flash lamp Condensing lens Mirror assembly Relay Lens Light baffle Trigger pack Reaction chamber Bandpass filter Photomultiplier tube Photodetector Flow sensor Pressure transducer Capillar...

Page 210: ... the hydrocarbon kicker The kicker may be optionally mounted to the bench to provide heating The optics section provides the light source for the fluorescence reaction and optimizes the reaction with a system of lenses and mirrors It includes a flash lamp condensing lens mirror assembly relay lens and light baffle Hydrocarbon Kicker Optics Measurement Interface Board Reaction Chamber Assy Mirror H...

Page 211: ...mary and secondary monochromaters The circular baffle helps keep stray light from entering the detection volume The flash lamp trigger assembly pulses the UV flash lamp at a rate of 10 times per second for improved signal to noise ratio and long term stability The lamp is operated in the pulsed mode for six major reasons Long life High optical intensity improved signal to noise ratio Small size Lo...

Page 212: ...nsor is used for measuring the flow of sample gas in the measurement system The pressure transducer or pressure sensor measures the reaction chamber pressure The capillary along with the pump is used to control flow in the sample line The vacuum pump draws the reacted gases out of the reaction chamber The processor software tasks are organized into four areas Instrument Control Monitoring Signals ...

Page 213: ...n seconds the measurement is reported every 10 seconds The one second average of the other analog inputs are reported directly no additional signal conditioning is performed by the high level processor The calculation begins by flashing the lamp 10 times per second After the lamp flash a sample and hold circuit on the input board is used to sample the PMT output The raw accumulated counts are scal...

Page 214: ...ch controls all power to the instrument and is accessible on the front panel The motherboard contains the main processor power supplies a sub processor and serves as the communication hub for the instrument The motherboard receives operator inputs from the front panel mounted function key panel and or over I O connections on the rear panel and sends commands to the other boards to control the func...

Page 215: ...tors located on the measurement interface board include Data communication with the motherboard 24V and 120VAC power supply inputs Fan and solenoid outputs 120VAC outputs for the pump and temperature control Flow and pressure sensors Ambient temperature sensor Bench heater PMT high voltage supply Input board Flash trigger Flash intensity Diagnostic LED The flow sensor assembly consists of a board ...

Page 216: ...perating when the operating condition of the flash lamp is unknown The input board accepts the current signal from the PMT and converts it to a voltage which is scaled by a factor of approximately 1 10 or 100 depending on the full scale range of the SO2 channel The scaled voltage signal is converted to a frequency and sent to the microprocessor The digital output board connects to the motherboard ...

Page 217: ... inputs and to output analog currents via a connector located on the rear panel of the instrument It contains local power supplies a DC DC isolator supply a sub processor and analog circuits Eight analog voltage inputs are provided with an input voltage range of 0V to10VDC Six current outputs are provided with a normal operating range of 0 to 20 mA External I O is driven from a generic bus that is...

Page 218: ...endent of the voltage outputs The current outputs are isolated from the instrument power and ground but they share a common return line Isolated GND The optional I O expansion board includes eight analog voltage inputs These inputs are used to gather measurement data from third party devices such as meteorological equipment The user may assign a label unit and a voltage to user defined unit conver...

Page 219: ...ctional serial interface can be configured for either RS 232 or RS 485 The serial baud rate is user selectable in firmware for standard speeds from 1200 to 19 200 baud The user can also set the data bits parity and stop bits The following protocols are supported C Link Streaming Data Modbus Slave Geysitech Bayern Hessen The Streaming Data protocol transmits user selected measurement data via the s...

Page 220: ...ound The instrument uses a four wire RS 485 configuration with automatic flow control SD Refer to Table 8 2 for the DB9 connector pin configuration Table 8 2 RS 485 DB Connector Pin Configuration DB9 Pin Function 2 receive 8 receive 7 transmit 3 transmit 5 ground An RJ45 connector is used for the 10Mbs Ethernet connection supporting TCP IP communications via standard IPV4 addressing The IP address...

Page 221: ... Manual 8 13 The external accessory connector is not used in the Model 43i Trace Level Enhanced analyzer This port is used in other models to communicate with smart external devices that may be mounted hundreds of feet from the analyzer using an RS 485 electrical interface External Accessory Connector ...

Page 222: ...System Description I O Components 8 14 Model 43i Trace Level Enhanced Instruction Manual Thermo Fisher Scientific ...

Page 223: ...ol dilution gas flow it should not be used as a basis for instrument zero and span adjustments calibration updates or adjustment of ambient data Whenever there is an indication of possible instrument drift or malfunction a full zero and multipoint calibration Level 1 should be performed prior to corrective action For further information on zero span and calibration of air pollution monitors refer ...

Page 224: ...ling the assembly upward Completely remove the oven 3 Separate the glass chamber from the top assembly by twisting and gently pulling the glass away from the top Note Keep the glass clean when handling it 4 Place the permeation tube s in the glass chamber 5 Attach the glass chamber to the top assembly by gently pushing the two together with a slight twisting motion 6 Replace the glass chamber asse...

Page 225: ... 1 atm Permeation Tube Q K R ppm Output o Where R permeation rate in ng min Q0 flow rate of gas scc min into the charcoal scrubber during span mode K constant for the specific permeant 24 45 MW MW molecular weight K SO2 0 382 Use the following procedure to install and configure the permeation oven 1 Physically install the permeation oven and valves into the instrument and connect the cables and pl...

Page 226: ...Therm menu 10 Remove resistor from POJ1 and re attach the gas thermistor 11 Connect a resistance of approximately 3 8 KΩ across pins 3 and 4 of POJ3 12 Go to the Factory Cal Oven Therm menu from the Perm Oven Settings menu in the Service menu Select Low Point enter the exact value of the resistor and press to calibrate the low resistance point 13 Press to return to the Factory Cal Oven Therm menu ...

Page 227: ...he permeation tube is then determined by weight loss in the actual oven being used You can use either of the two calibration methods presented here One method involves performing the Setting Perm Oven Temperature procedure and then continuing with the Setting Temperature with Water Bath procedure Alternatively you can perform the Setting Perm Oven Temperature procedure and then continue with the S...

Page 228: ...o the water bath next to an NIST traceable thermometer if necessary use an extension cable to reach 2 Turn on the power to the water bath Using an NIST traceable thermometer with a resolution of 0 01 C adjust the water bath to 45 C 3 From the Permeation Oven menu in the Service menu select Cal Gas Thermistor Water Bath Enter the thermistor temperature from the thermometer and press Figure 9 3 CAL ...

Page 229: ...elect known resistor CAL GAS THERM RESISTOR CURRENTLY 4369 Ohms SET TO 04369 Ohms MOVE CURSOR ª CHANGE VALUE SAVE RANGE AVG DIAGS ALARM Figure 9 4 Cal Gas Therm Resistor Screen 4 Enter the exact value of the attached resistor and press to save the offset 5 Remove the resistor and reconnect the gas thermistor 6 Make sure the charcoal scrubber is connected to the ZERO bulkhead on the rear panel 7 Wa...

Page 230: ...mined to a precision of 1 2 10 For the most accurate work use the permeation tube in the same oven that was used to determine the weight loss of permeation tube Use the following procedure to determine the release rate by transfer standard 1 Make sure the oven has been calibrated as described in the Permeation Tube Oven Calibration procedure described previously Also make sure that the Transfer St...

Page 231: ...d outputs The 25 pin terminal board assembly is included with the optional I O expansion board Refer to Terminal Board PCB Assemblies in the Installation chapter for information on attaching the cable to the connector board For associated part numbers refer to the Servicing chapter The optional terminal block and cable kits provide a convenient way to connect devices to the instrument These kits b...

Page 232: ...color codes for pins 1 37 are for 37 pin cables Table 9 1 Cable Options Description Cable Length DB37M to open end Six feet DB37F to open end Six feet DB25M to open end Six feet RS 232 Table 9 2 Color Codes for 25 Pin and 37 Pin Cables Pin Color Pin Color 1 BLACK 20 RED BLACK 2 BROWN 21 ORANGE BLACK 3 RED 22 YELLOW BLACK 4 ORANGE 23 GREEN BLACK 5 YELLOW 24 GRAY BLACK 6 GREEN 25 PINK BLACK 7 BLUE E...

Page 233: ...The analyzer can be installed in the configuration described in Table 9 3 and shown in Figure 9 5 through Figure 9 8 Table 9 3 Mounting Options Mounting Type Description Bench Positioned on bench includes mounting feet and front panel side trim handles EIA rack Mounted in an EIA style rack includes mounting slides and front panel EIA rack mounting handles Retrofit rack Mounted in a Thermo non EIA ...

Page 234: ...Optional Equipment Mounting Options 9 12 Model 43i Trace Level Enhanced Instruction Manual Thermo Fisher Scientific Figure 9 5 Rack Mount Option Assembly ...

Page 235: ...Optional Equipment Mounting Options Thermo Fisher Scientific Model 43i Trace Level Enhanced Instruction Manual 9 13 Figure 9 6 Bench Mounting ...

Page 236: ...Optional Equipment Mounting Options 9 14 Model 43i Trace Level Enhanced Instruction Manual Thermo Fisher Scientific Figure 9 7 EIA Rack Mounting ...

Page 237: ...Optional Equipment Mounting Options Thermo Fisher Scientific Model 43i Trace Level Enhanced Instruction Manual 9 15 Figure 9 8 Retrofit Rack Mounting ...

Page 238: ......

Page 239: ...and or a Return Material Authorization RMA which may include biohazard decontamination procedures and other product specific handling instructions and c then if applicable Buyer may return the defective Products to Seller with all costs prepaid by Buyer Replacement parts may be new or refurbished at the election of Seller All replaced parts shall become the property of Seller Shipment to Buyer of ...

Page 240: ...Buyer shall pay Seller therefor at Seller s then prevailing time and materials rates ANY INSTALLATION MAINTENANCE REPAIR SERVICE RELOCATION OR ALTERATION TO OR OF OR OTHER TAMPERING WITH THE PRODUCTS PERFORMED BY ANY PERSON OR ENTITY OTHER THAN SELLER WITHOUT SELLER S PRIOR WRITTEN APPROVAL OR ANY USE OF REPLACEMENT PARTS NOT SUPPLIED BY SELLER SHALL IMMEDIATELY VOID AND CANCEL ALL WARRANTIES WITH...

Page 241: ...ge B 14 Datalogging on page B 16 Calibration on on page B 23 Keys Display on page B 26 Measurement Configuration on page B 27 Hardware Configuration on page B 31 Communications Configuration on page B 34 I O Configuration on page B 38 I O Configuration on page B 38 Each command sent to the analyzer must begin with the American Standard Code for Information Interchange ASCII symbol or byte value eq...

Page 242: ...sage will be received The example that follows sends the incorrect command set unit ppm instead of the correct command set gas unit ppm Send set unit ppm Receive set unit ppm bad cmd The save and set save params commands stores parameters in FLASH It is important that each time instrument parameters are changed that this command be sent If changes are not saved they will be lost in the event of a ...

Page 243: ...el 450i only B 12 alarm internal temp max Reports sets internal temperature alarm maximum value B 12 alarm internal temp min Reports sets internal temperature alarm minimum value B 12 alarm pressure max Reports sets pressure alarm maximum value B 13 alarm pressure min Reports sets pressure alarm minimum value B 13 alarm sample flow max Reports sets sample flow alarm maximum value B 13 alarm sample...

Page 244: ...cratch pad into stream list B 22 copy srec to sp Sets copies current srec selection into the scratch pad B 22 copy stream to sp Sets copies current streaming data selection into the scratch pad B 22 custom Reports sets defined custom range concentration B 29 data treatment lrec srec Reports sets the current selection of data treatment for concentrations in the lrecs or srecs B 21 date Reports sets...

Page 245: ... coefficients B 8 high so2 coef Reports sets high range SO2 coefficients B 24 high sp conc Reports sets high span concentration B 25 host name Reports sets host name string B 37 instr name Reports instrument name B 37 instrument id Reports sets instrument id B 37 internal temp Reports current internal instrument temperature B 9 isc iscreen Retrieves framebuffer data used for the display B 26 lamp ...

Page 246: ... records that can be stored B 19 lrec per Reports sets long record logging period B 20 malloc lrec Reports sets memory allocation for long records B 20 malloc srec Reports sets memory allocation for short records B 20 me menu Simulates pressing menu pushbutton B 26 mode Reports operating mode in local service or remote B 38 no of lrec Reports sets number of long records stored in memory B 20 no of...

Page 247: ...umber of short records B 17 srec format Reports sets output format for short records ASCII or binary B 18 srec layout Reports current layout of short record data B 19 srec mem size Reports maximum number of short records B 19 srec per Reports sets short record logging period B 20 stream per Reports sets current set time interval for streaming data B 22 stream time Reports sets a time stamp to stre...

Page 248: ...2 The example that follows sets the low range averaging time to 120 seconds Send set low avg time 8 Receive set low avg time 8 ok Table B 2 Averaging Times Selection Averaging Time seconds 0 1 seconds 1 2 2 5 3 10 4 20 5 30 6 60 7 90 8 120 9 180 10 240 11 300 so2 high so2 low so2 These commands report the measured SO2 concentration when operating in single range or high and low SO2 when operating ...

Page 249: ...ature compensation is off a temperature of 30 C is used as the default temperature even though the actual internal temperature is 27 2 C The example that follows shows that temperature compensation is on and that the internal temperature is 27 2 C Send internal temp Receive internal temp 27 2 deg C pmt voltage This command reports the current PMT voltage The example that follows reports that the c...

Page 250: ...ve react temp 45 2 deg C flags This reports 8 hexadecimal digits or flags that represent the status of the flash lamp LED pressure and temperature compensation status gas units gas mode and alarms To decode the flags each hexadecimal digit is converted to binary as shown in the Table B 1 It is the binary digits that define the status of each parameter In the example that follows the instrument is ...

Page 251: ...follows sets the chamber temperature alarm maximum value to 55 0 C Send set alarm chamber temp max 55 0 Receive set alarm chamber temp max 55 0 ok alarm conc so2 min alarm conc so2 max These commands report the SO2 concentration alarm minimum and maximum values current setting The example that follows reports that the SO2 concentration minimum is 5 2 ppb Send alarm conc so2 min Receive alarm conc ...

Page 252: ... example that follows sets the converter temperature alarm maximum value to 215 0 C Send set alarm converter temp max 215 Receive set alarm converter temp max 215 ok alarm internal temp min alarm internal temp max These commands report the internal temperature alarm minimum and maximum value current settings The example that follows reports that the internal temperature alarm minimum value is 15 0...

Page 253: ...ssure max 215 ok alarm sample flow min alarm sample flow max These commands report the sample flow alarm minimum and maximum value current settings The example that follows reports that the sample flow alarm minimum value is 2 LPM Send alarm sample flow min Receive alarm sample flow min 2 l min set alarm sample flow min value set alarm sample flow max value These commands set the sample flow alarm...

Page 254: ...rts the current of the reference channel AGC circuit The example that follows reports that the current AGC intensity is 90 percent Send agc int Receive agc int 90 diag volt mb This command reports the diagnostic voltage measurements on the motherboard The sequence of voltages is Positive 24 positive 15 positive 5 positive 3 3 and negative 3 3 Each voltage value is separated by a space Send diag vo...

Page 255: ...set lamp setpoint value value 0 value 4095 These commands set the lamp setpoint in counts The example that follows sets the lamp setpoint to 100 counts Send set lamp setpoint 100 Receive set lamp setpoint 100 ok lamp int This command reports the current flash lamp intensity The example that follows reports that the current flash lamp intensity is 3867 Hz Send lamp int Receive lamp int 3867 Hz lamp...

Page 256: ... records Send set clr srecs Receive set clr srecs ok list din list dout These commands report the current selection for the digital outputs in the format Output no Index number variable name active state The active state for digital outputs is open or closed The active state for digital inputs is high or low Send list dout Receive list dout output index variable state 1 28 CONC ALARM closed 2 2 LO...

Page 257: ...1 Receive lr01 18 09 05 12 03 flags 5c000044 SO2 9658E 5 low SO2 8920E 5 Intt 28 6 Rctt 25 6 Pgast 0 00 Pres 720 3 Smpfl 0 489 PMt V 808 LmpV 449 Lmpi 4740E 1 erec This command returns a brief description of the main operating conditions at the time the command is issued i e dynamic data The example that follows shows a typical response The format is defined by the current settings of format and e...

Page 258: ...mand Send lrec 5 Receive lrec 100 5 18 09 05 12 03 flags 5c000044 SO2 9658E 5 low SO2 8920E 5 Intt 28 6 Rctt 25 6 Pgast 0 00 Pres 720 3 Smpfl 0 489 PMt V 808 LmpV 449 Lmpi 4740E 1 18 10 05 12 03 flags 5c000044 SO2 6923E 5 low SO2 6429E 5 Intt 28 6 Rctt 25 6 Pgast 0 00 Pres 720 3 Smpfl 0 489 PMt V 808 LmpV 449 Lmpi 4740E 1 18 11 05 12 03 flags 5c000044 SO2 8814E 5 low SO2 9488E 5 Intt 28 6 Rctt 25 ...

Page 259: ... data formats for data that is sent out in response to the erec lrec srec and related commands The example that follows shows a typical response For details on how to interpret the strings see Record Layout Definition later in this appendix Send lrec layout Receive lrec layout s s lx f f f f f f t D L ffffff so2 pmtv lmpv ain4 ain5 lmpi lrec mem size srec mem size These commands report the long an...

Page 260: ...gging period to 15 minutes Send set lrec per 15 Receive set lrec per 15 ok no of lrec no of srec These commands report the number of long and short records stored in the long and short records memory The example that follows shows that 50 long records have been stored in the memory Send no of lrec Receive no of lrec 50 recs malloc lrec malloc srec These commands report the currently set memory all...

Page 261: ...rations in lrec is minimum Send data treatment lrec Receive data treatment lrec min set data treatment lrec string set data treatment srec string string cur avg min max These commands set the data treatment to string where string is current average minimum or maximum for the concentration values recorded in the long records lrecs or short records srecs The example that follows sets the data treatm...

Page 262: ... index number 3 which is for the variable SO2 concentration Send sp field 1 Receive sp field 1 1 so2 set sp field number value number 1 32 is the maximum number of fields in long and short record lists number 1 18 is for streaming data lists This command sets the scratch pad field number item number in scratch pad list to value where value is the index number of a variable in the analog out variab...

Page 263: ...enables value where value is to attach or disable time stamp to streaming data string according to Table B 5 The example that follows attaches a time stamp to streaming data Send set stream time 0 Receive set stream time 0 ok Table B 5 Stream Time Values Value Stream Time 00 Attaches time stamp to streaming data string 01 Disables time stamp to streaming data string set cal so2 coef set cal high s...

Page 264: ...O2 coefficient is 1 200 Send so2 coef Receive so2 coef 1 200 set so2 coef value set coef so2 value set high so2 coef value set low so2 coef value These commands set the SO2 coefficients to user defined values to value where value is a floating point representation of the coefficient The example that follows sets the SO2 coefficient to 1 200 Send set so2 coef 1 200 Receive set so2 coef 1 200 ok so2...

Page 265: ...set low sp conc value These commands set the span concentrations to user defined values to value where value is a floating point representation of the span concentration in current selected units The example that follows sets the span concentration to 80 ppm in the single range mode Send set sp conc 80000 Receive set sp conc 80000 ok pres cal This command reports the pressure recorded at the time ...

Page 266: ...imulates pressing the front panel pushbuttons The numbers represent the front panel soft keys from left to right Send push enter Receive push enter ok isc iscreen This command retrieves the framebuffer data used for the display on the iSeries instrument It is 19200 bytes in size 2 bits per pixel 4 pixels per byte arranged as 320 by 240 characters The data is sent in RLE encoded form to save time i...

Page 267: ... screen This command is meant for backward compatibility on the C series Screen information is reported using the iScreen command above Send screen Receive screen This is an I series Instrument Screen Information not available range range so2 high range low range These commands report SO2 range in single range mode or the high and low ranges in dual or auto range mode If the mode is incorrect the ...

Page 268: ...ection These commands select the SO2 full scale ranges according to Table B 6 and Table B 7 The example that follows sets the SO2 full scale range to 100 ppm Send set range 3 Receive set range 3 ok Table B 6 Standard Ranges Selection ppm mg m3 0 0 05 0 2 1 0 1 0 5 2 0 2 1 3 0 5 2 4 1 5 5 2 10 6 5 20 7 10 25 8 C1 C1 9 C2 C2 10 C3 C3 Table B 7 Extended Ranges Selection ppm mg m3 0 0 5 2 1 1 5 2 2 10...

Page 269: ...to set the maximum concentration for any of the three custom ranges 1 2 or 3 to range value where value is a floating point number representing concentration in ppm or mg m3 The example that follows sets the custom 1 range to 55 5 ppm Send set custom 1 range 55500 Receive set custom 1 range 55500 ok range mode This command reports the current range mode Send range mode Receive range mode single se...

Page 270: ...xample that follows sets the instrument to zero mode that is the instrument is reading the sample gas Send set zero Receive set zero ok set span set span gas This command sets the zero span valves to the span mode The example that follows sets the instrument to span mode that is the instrument is sampling span gas Send set span Receive set span ok gas unit This command reports the current gas unit...

Page 271: ...r temperature compensation is on or off The example that follows shows the temperature compensation is off Send temp comp Receive temp comp off set temp comp onoff These commands turn the temperature compensation on or off The example that follows turns temperature compensation off Send set temp comp off Receive set temp comp off ok contrast This command reports the screen s level of contrast The ...

Page 272: ...hat follows reports that the converter temperature is set to 50 1 C Send conv set temp Receive conv set temp 50 1 deg C set conv set temp value This command sets the temperature that the SO2 converter is set to value where value is an integer representing degrees C The example that follows sets the converter temperature to 50 1 C Send set conv set temp 50 1 Receive set conv set temp 50 1 ok date T...

Page 273: ...actory calibrated parameters Send set default params Receive set default params ok lamp status This command reports the status of the flash lamp on or off The example that follows reports the flash lamp is on Send lamp status Receive lamp status on set lamp onoff These commands set the flash lamp on or off The example that follows turns the flash lamp off Send set lamp off Receive set lamp off ok ...

Page 274: ... save params ok time This command reports the current time 24 hour time The example that follows reports that the internal time is 2 15 30 pm Send time Receive time 14 15 30 set time hh mm ss hh hours mm minutes ss seconds This command sets the internal clock 24 hour time The example that follows sets the internal time to 2 15 pm Note If seconds are omitted the seconds default to 00 Send set time ...

Page 275: ...t addr gw 192 168 1 1 Receive set addr gw 192 168 1 1 ok addr ip This command reports the IP address of the analyzer Send addr ip Receive addr ip 192 168 1 200 set addr ip address This command sets the analyzer s IP address where address consists of four numbers ranging from 0 255 inclusive separated by Send set addr ip 192 168 1 200 Receive set addr ip 192 168 1 200 ok addr nm This command report...

Page 276: ... Send set baud 9600 Receive set baud 9600 ok dhcp This command reports the current state of use of DHCP on or off DHCP is used to assign an IP address to the analyzer automatically The example that follows shows that DHCP is on Send dhcp Receive dhcp on set dhcp onoff These commands enables and disables the DHCP service by either on or off Changes to this parameter will only take effect when the a...

Page 277: ... Format Reply Termination 00 CR 01 NL sum xxxx CR where xxxx 4 hexadecimal digits that represent the sum of all the characters bytes in the message host name This command reports the host name string Send host name Receive host name analyzer01 set host name string This command sets the host name string where string is 1 13 alphanumeric characters Send set host name analyzer01 Receive set host name...

Page 278: ...local set mode remote These commands set the instrument to local or remote mode The example that follows sets the instrument to the local mode Send set mode local Receive set mode local ok program no This command reports the analyzer s model information and program version number which will be dependant on the current version Send program no Receive program no iSeries 43i 01 01 10 003 set layout a...

Page 279: ...nt Output Range Values Range Output Range 1 0 20 mA 2 4 20 mA 0 cannot be set to this but may report Undefined analog vin channel This command retrieves the analog voltage input channel data both the calculated value and the actual voltage In the example that follows the calculated value of channel 1 is 75 325 degrees F volts are 2 796 This command responds with feature not enabled if the I O expa...

Page 280: ...ponding active state The example that follows reports the input 1 to be assigned an index number 3 corresponding to action of SO2 mode with the active state being high Send din 1 Receive din 1 3 SO2 MODE high set din channel index state This command assigns digital input channel 1 16 to activate the action indicated by index 1 35 when the input transitions to the designated state high or low Use l...

Page 281: ...efinable If any customization has been made to the analog output configuration the default selections may not apply Table B 12 Default Output Assignment D to A Function Single Range Dual Range Autorange 1 Voltage Output Low SO2 Low SO2 High Low SO2 2 Voltage Output Low SO2 High SO2 Range Status 3 Voltage Output Not Assigned Not Assigned Not Assigned 4 Voltage Output Not Assigned Not Assigned Not A...

Page 282: ...lows reports the list of analog output index numbers and variables Send list var aout Receive list var aout index variable 0 none 1 so2 11 intt 12 rctt 16 pres 17 smplfl 18 pmtv 19 lmpv 20 lmpi 21 ain1 22 ain2 23 ain3 24 ain4 25 ain5 26 ain6 27 ain7 28 ain8 relay stat This command reports the current relay logic normally open or normally closed if all the relays are set to same state that is all o...

Page 283: ...format specifier for parsing ASCII responses A format specifier for parsing binary responses In addition to these the Erec Layout contains A format specifier for producing the front panel displays In operation values are read in using either the ASCII or binary format specifiers and converted to uniform internal representations 32 bit floats or 32 bit integers These values are converted into text ...

Page 284: ... parse a 16 bit unsigned number 2 bytes m parse a 24 bit signed number 3 bytes M parse a 24 bit unsigned number 3 bytes l parse a 32 bit signed number 4 bytes L parse a 32 bit unsigned number 4 bytes There is an optional single digit d which may follow any of the numeric fields which indicates that after the field has been parsed out the resulting value is to be divided by 10 d Thus the 16 bit fie...

Page 285: ...at e g a field of 4 would be translated into the printf command of 3f Alternately the special character can precede the precision specifier this causes an indirection on the precision specifier which now becomes a field number This is useful when formatting for example numbers which have varying precision depending on the mode of the instrument Binary numbers can also have an optional precision sp...

Page 286: ... using the designated input format The input format is specified from the B through the subsequent semicolon I Indicates a button which pops up a selection list with input translation That is the values read are translated before they are compared to the selection list options L Indicates a button which pops up a selection list without any translation The output value is number of the selected opt...

Page 287: ... NO and the value the twenty first element of the data response interpreted as a floating point number There is a no translation button which creates a selection list of twelve Code nn options The number of the user selection is used to create the output command Mode 6 12 13x local remote service service 0 1 Tset mode s n This is a line which has a title of Mode and value taken from the sixth fiel...

Page 288: ...onal The bitfield will be one bit long starting in this case at the eleventh bit Background 7f 8Bd ddd set o3 bkg s n This shows the use of indirect precision specifiers for floating point displays The background value is taken from the 7th element and the precision specifier is taken from the 8th If the asterisk were not present it would indicate instead that 8 digits after the decimal point shou...

Page 289: ...instrument This is achieved by using the supported MODBUS commands listed below For details of the Model 43i Trace Level Enhanced MODBUS Protocol specification see the following topics Serial Communication Parameters on page C 2 TCP Communication Parameters on page C 2 Application Data Unit Definition on page C 2 Function Codes on page C 3 MODBUS Commands Supported on page C 8 Additional informati...

Page 290: ...MODBUS RTU over serial connections Note Device ID 0 used for broadcast MODBUS commands is not supported Device IDs 128 through 247 i e 0x80 hex to 0xF7 hex are not supported because of limitations imposed by C Link In MODBUS over TCP IP a MODBUS Application Protocol Header MBAP is used to identify the message This header consists of the following components Transaction Identifier 2 Bytes 0x0000 to...

Page 291: ... This section describes the various function codes that are supported by the Model 43i Trace Level Enhanced Read Coils Inputs reads the status of the digital outputs relays in the instrument Issuing either of these function codes will generate the same response These requests specify the starting address i e the address of the first output specified and the number of outputs The outputs are addres...

Page 292: ...mum allowed by instrument Quantity of outputs 2 Bytes 1 to maximum allowed by instrument Unit Identifier 1 Byte 0x00 to 0xFF Passed back in response Response Function code 1 Byte 0x01 or 0x02 Byte count 1 Byte N Output Status n Byte N N or N 1 N Quantity of Outputs 8 if the remainder not equal to zero then N N 1 Error Response Function code 1 Byte 0x01 or 0x02 Exception code 1 Byte 01 Illegal Func...

Page 293: ...54 floating point format This uses 2 sequential registers least significant 16 bits first The request specifies the starting register address and the number of registers Registers are addressed starting at zero Therefore registers numbered 1 16 are addressed as 0 15 The register data in the response message are packed as two bytes per register with the binary contents right justified within each b...

Page 294: ...ytes per register with the binary contents right justified within each byte For each register the first byte contains the high order bits and the second contains the low order bits Request Function code 1 Byte 0x03 or 0x04 Starting Address 2 Bytes 0x0000 to maximum allowed by instrument Quantity of Registers 2 Bytes 1 to maximum allowed by instrument Response Function code 1 Byte 0x03 or 0x04 Byte...

Page 295: ... respective action This function code is used to set a single action to either ON or OFF The request specifies the address of the action to be forced Actions are addressed starting at zero Therefore action number 1 is addressed as 0 The requested ON OFF state is specified by a constant in the request data field A value of 0xFF00 requests the action to be ON A value of 0x0000 requests it to be OFF ...

Page 296: ...nction 05 Output Address Hi 00 Output Address Lo 05 Output Value Hi FF Output Value Lo 00 Response Field Name Hex Function 05 Output Address Hi 00 Output Address Lo 05 Output Value Hi FF Output Value Lo 00 Tables C1 through C3 list the MODBUS commands supported for the Model 43i Trace Level Enhanced Table C 1 Read Registers for 43i Trace Level Enhanced Register Number Variable 40001 40002 SO2 CONC...

Page 297: ...38 FLASH VOLTS 40039 40040 FLASH REF 40041 40042 ANALOG IN 1 I O Expansion Board installed 40043 40044 ANALOG IN 2 I O Expansion Board installed 40045 40046 ANALOG IN 3 I O Expansion Board installed 40047 40048 ANALOG IN 4 I O Expansion Board installed 40049 40050 ANALOG IN 5 I O Expansion Board installed 40051 40052 ANALOG IN 6 I O Expansion Board installed 40053 40054 ANALOG IN 7 I O Expansion B...

Page 298: ...SERVICE 4 UNITS 0 ppb 1 μg m3 5 ZERO MODE 6 SPAN MODE 7 SAMPLE MODE 8 NOT USED 9 NOT USED 10 GEN ALARM 11 SO2 CONC MAX ALARM 12 SO2 CONC MIN ALARM 13 NOT USED 14 NOT USED 15 NOT USED 16 NOT USED 17 INT TEMP ALARM 18 CHAMB TEMP ALARM 19 CONVERTER TEMP 20 PGAS TEMP 21 PRESSURE ALARM 22 SAMPLE FLOW ALARM 23 FLASH REF ALARM 24 FLASH VOLTAGE ALARM 25 MOTHERBOARD STATUS ALARM 26 MEASUREMENT INTERFACE BO...

Page 299: ...rotocol MODBUS Commands Supported Thermo Fisher Scientific Model 43i Trace Level Enhanced Instruction Manual C 11 Coil Number Status 30 ZERO CHK CAL ALARM Zero Span Option 31 SPAN CHK CAL ALARM Zero Span Option ...

Page 300: ...MODBUS Protocol MODBUS Commands Supported C 12 Model 43i Trace Level Enhanced Instruction Manual Thermo Fisher Scientific ...

Page 301: ...mple zero span mode if valid for that instrument This is achieved by using the supported Geysitech commands listed below For details of the Model 43i Trace Level Enhanced Geysitech Protocol specification see the following topics Serial Communication Parameters on page D 1 TCP Communication Parameters on page D 2 Instrument Address on page D 2 Abbreviations Used on page D 2 Basic Command Structure ...

Page 302: ...nt Address is represented by address in the examples throughout this document Note Device IDs 128 through 247 are not supported because of limitations imposed by the C Link protocol The following is a list of abbreviations used in this document CR is abbreviation for Carriage Return ASCII code 0x0D STX is abbreviation for Start of Text ASCII code 0x02 ETX is abbreviation for End of Text ASCII code...

Page 303: ...ted by the two characters A B The checksum is referred to as BCC throughout this document The following commands are supported by the Geysitech protocol Instrument Control Command ST Data Sampling Data Query Command DA There are three control commands supported by the Geysitech protocol This control command is a single letter which triggers an action in the instrument These commands are active onl...

Page 304: ...d in response to DA command below The command structure for a data query command is as follows STX DA address ETX BCC The address is optional which means it can be left out completely The address if present must match the Instrument Address Additional space can be present after the address If the address is left out then no space is allowed in the query string A command with no address is also a v...

Page 305: ...ched to the response will have the address X where X keeps incrementing by 1 for each measurement included measured value is the concentration value in currently selected gas units represented as exponential representation with 4 characters mantissa and 2 characters exponent each with sign Mantissa sign and 4 digits The decimal point is assumed to be after the first digit and is not transmitted Ex...

Page 306: ...SP 0000000000 SP 003 SP 1175 01 SP 03 SP 04 SP Second Concentration 5 681 Address 2 Third Concentration 11 75 0000000000 SP CR The attached concentrations are in the selected gas units The measurements that are attached to the response if not valid in a particular mode then a value of 0 0 will be reported The following measurements reported in response to DA command are for the Model 43i Trace Lev...

Page 307: ...o gas On 0 0 0 0 0 1 0 0 Span gas On 0 0 0 0 1 0 0 0 Gas Unit Indication ppb OR ppm 0 0 0 1 0 0 0 0 Test LED On 0 0 1 0 0 0 0 0 Flash Lamp Off 0 1 0 0 0 0 0 0 Not used 1 0 0 0 0 0 0 0 Table D 2 Error Status for Model 43i Trace Level Enhanced D7 D6 D5 D4 D3 D2 D1 D0 Æ Bit 8 7 6 5 4 3 2 1 Æ Hex value 80 40 20 10 08 04 02 01 MSB LSB Error status Internal Temperature Alarm 0 0 0 0 0 0 0 1 Reaction Cha...

Page 308: ...Geysitech Bayern Hessen Protocol Geysitech Commands D 8 Model 43i Trace Level Enhanced Instruction Manual Thermo Fisher Scientific ...

Page 309: ...n is normally done using firs a zero gas then a span gas generated by dilution of a calibration gas cylinder Dilution is done by dynamic mixing of accurately known flows of span gas and zero gas For Trace Level analyzers mass flow controllers that are NIST traceable are required Nitric oxide and sulfur dioxide calibration standards between 1 and 10 ppm are readily available in specially treated cy...

Page 310: ... 25 psig is dried by passing the air through a heatless air dryer for example and then sent through a series of chemical reactors and or scrubbers Normally these include indicating silica gel Purafil activated charcoal and a fine 5 micron particulate filter When first used this brute force approach actually can generate enhanced impurity levels for Nox and SO2 as these gases desorb from the chemic...

Page 311: ...the United States Environmental Agency Tennessee Valley Authority Battelle National Labs and the Thermo Fisher Scientific Engineering Department have demonstrated that Trace Level analyzers are readily calibrated at the low concentration levels require for sub ambient monitoring Although extra care is required primarily in zero air generation users familiar with normal compliance requirements shou...

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