Suez Sievers UPW Boron Analyzer Operation And Maintenance Manual Download Page 1

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Water Technologies & Solutions

Ultrapure Water (UPW)

Boron Analyzer

operation and maintenance manual

www.sieversinstruments.com

DLM 71000-03 EN

Rev. B

1.06 firmware or later

Summary of Contents for Sievers UPW Boron Analyzer

Page 1: ...Water Technologies Solutions Ultrapure Water UPW Boron Analyzer operation and maintenance manual www sieversinstruments com DLM 71000 03 EN Rev B 1 06 firmware or later...

Page 2: ...East and Africa contact Technical Support at 44 161 864 6800 To order standards or replacement parts contact Customer Care at 1 800 255 6964 or your local service provider For a copy of the Declaratio...

Page 3: ...4 DLM 71000 03 EN Rev B Identification Records Analyzer serial number _______________________ This is located on the side of the Analyzer Date Analyzer received _______________________ This is the war...

Page 4: ...SUEZ 2018 4 of 104 DLM 71000 03 EN Rev B THIS PAGE IS INTENTIONALLY LEFT BLANK...

Page 5: ...arranty 14 Limitation of Remedies and Liability 15 Warnings 17 Chapter 1 Introduction 23 Chapter 2 System Description 25 System Specifications 25 System Components 26 Fluidics Components 26 Multistrea...

Page 6: ...stalling the Analyzer 32 Location 32 Consumables Installation 33 Equipment Needed 33 Installing the Reagent 34 Option 1 34 Option 2 35 Installing the Reagent and Zero Columns 36 Reagent Column 36 Zero...

Page 7: ...lay 50 Selected Mode 50 Maintenance Alert Area 50 Countdown Clock 50 Information Display 50 Menu Control Options 50 Soft Launch Keys 50 Started and Stopped Stages of Operation 50 Soft Launch Keys 51 M...

Page 8: ...e the Terminal Block TB5 70 Step Two Configure the Analyzer 71 Step Three Connect the RS 232 Cable to the Computer 71 Step Four Cycle the Analyzer Power 71 Step Five Configure Serial Communication Pro...

Page 9: ...agent Column and Zero Column Installation Information 85 Setting the Reagent Column and Zero Column Warning Levels 86 Pump Tubing 86 Removing the Existing Pump Tubing 87 Installing the New Pump Tubing...

Page 10: ...SUEZ 2018 10 of 104 DLM 71000 03 EN Rev B Chapter 9 Message and Error Codes 97 Overview 97 Message Log 98 Specific Messages 99 Index 101...

Page 11: ...Block TB5 70 Table 5 RS 232 Data Format 72 Table 6 RS 232 Commands 73 Table 7 Description of Output for the GDR Get Data Card Record Command 73 Table 8 Binary Outputs on Terminal Block TB3 75 Table 9...

Page 12: ...41 Figure 6 Fluidics Block Diagram 46 Figure 7 Boron Analysis Conductivity Profile 47 Figure 8 Front Panel Display in the Stopped State 49 Figure 9 Front Panel Display in the Started State 49 Figure 1...

Page 13: ...ted KimWipe is a trademark of the Kimberly Clark Corporation Rheodyne is a registered trademark of the IDEX Corporation Seiko is a registered trademark of Seiko Instruments Swagelok is a registered tr...

Page 14: ...me instances suitable instruments may be available for short duration loan or lease SUEZ warrants that any labor services provided shall conform to the reasonable standards of technical competency and...

Page 15: ...structions stated in the Operation and Maintenance Manual Usage of non recommended maintenance materials may void a warranty claim The remedies provided herein are the customer s sole and exclusive re...

Page 16: ...SUEZ 2018 16 of 104 DLM 71000 03 EN Rev B THIS PAGE IS INTENTIONALLY LEFT BLANK...

Page 17: ...the metal enclosure only If this instrument is used in a manner not specified by SUEZ the protection provided by the instrument may be impaired The wall plug of the AC power cord is the main disconnec...

Page 18: ...to indica que el usuario debe consultar el manual para ver las instrucciones de manejo Este s mbolo indica el terminal de protecci n a tierra masa del analizador Para protecci n cont nua contra el pel...

Page 19: ...l incendie changez le fusible par un fusible du m me type et valeur Ce symbole indique qu aux fins de conformit avec la directive 2002 96 CE de l Union Europ enne concernant les mat riels lectronique...

Page 20: ...Weise verwendet wird die nicht von SUEZ festgelegt ist kann der durch dieses Instrument gebotene Schutz beeintr chtigt werden Dies ist ein Ger t der Sicherheitsklasse I und darf nur mit einem Netzkab...

Page 21: ...rme alle specifiche per I prodotti in Classe I Il cavo di alimentazione dalla rete deve essere munito di terra Questo un prodotto di Classe A Se utilizzato in un ambiente domestico pu generare interfe...

Page 22: ...type en waarde Indien het toestel niet gebruikt wordt volgens de richtlijnen van SUEZ gelden de veiligheidsvoorzieningen niet meer Dit is een produkt van veiligheidsklasse I Het toestel moet aangeslo...

Page 23: ...CHAPTER 3 INSTALLATION covers the gamut of steps needed to get the Analyzer fully functional from unpacking to installation CHAPTER 4 BASIC ANALYZER OPERATION provides both an overview and details of...

Page 24: ...SUEZ 2018 24 of 104 DLM 71000 03 EN Rev B Chapter 1 Introduction THIS PAGE IS INTENTIONALLY LEFT BLANK...

Page 25: ...ppb B whichever is greater 15 M cm 15 40 C 0 1 0 5 L min 10 40 C 20 100 psig 138 689 kPa Typically 12 months 15 micron pre filtration Gravity drain no back pressure Designed for use at altitudes up t...

Page 26: ...second type is a boron specific resin that removes any boric acid in the sample Pressure Switch Detects when there is little or no flow to the Analyzer Reagent Pump Continuously pumps the reagent from...

Page 27: ...eceives the conductivity and temperature measurements from the conductivity cell It contains an analog to digital converter that converts the analog signals from the conductivity cell into digital sig...

Page 28: ...ng is detected A resistivity error is detected New boron data is ready A fatal error is detected The Analyzer is in standby and not running For information on how to configure the alarms and binary ou...

Page 29: ...nearly to 50 at 40 C A non corrosive atmosphere located away from excessive HCl acid or other corrosive vapors Located away from excessive EMI electromagnetic interference Located away from or isolate...

Page 30: ...ers provided Flow rate between 0 05 and 0 2 L min per sample stream Water pressure between 20 and 100 psi at the Analyzer Maximum sample tubing length from water sampling point less than 100 feet Samp...

Page 31: ...dampened towels may be needed to clean area after reagent fill ESD wrist strap Unpacking the Analyzer Note Although reasonable safeguards against shipping damage have been taken and the Analyzer is f...

Page 32: ...ired on each sample inlet Vent plug Tubing cutter Data Card Reader including CD and instructions 3 Lift the Analyzer from the box Two people should always handle the Analyzer by gripping the sheet met...

Page 33: ...the outside of the Analyzer If filling reagent through the fill port on the top of the Analyzer no additional equipment is needed If access to the fill port is limited reagent may be filled using the...

Page 34: ...nalyzer If this port is not accessible install the reagent using Option 2 below 1 Remove the fill port cap and set aside 2 Remove the cap from the reagent bottle and pour the reagent into the Analyzer...

Page 35: ...the Analyzer As the last of the reagent is pumped out of the bottle some air will enter the line and be pushed into the reservoir This is normal 10 Turn the hand pump vent valve counterclockwise to re...

Page 36: ...on top and the side hole facing away from the Analyzer Push the middle of the column into the holder dark gray plastic bracket centered on the right side of the Analyzer and then push the column up i...

Page 37: ...nect the Analyzer end of the tubing to the inlet of the 15 micron filter provided 3 Cut a 3 inch length of 1 4 inch OD sample tubing provided and connect one end to the outlet of the 15 micron filter...

Page 38: ...ll drain tubing and the vented drain should be positioned lower than the level of the Analyzer to minimize back pressure on the drain lines Note Do NOT connect the two drain lines using a tee or other...

Page 39: ...be primed This is accomplished by using the priming valve The priming valve is located near the bottom of the Analyzer in front of the reagent pump Note A panel plug is installed in the I O cable wir...

Page 40: ...position and close the door This procedure clears most of the air from the pump head and allows for better performance of the reagent pump Note Proper operation of the reagent pump can be verified by...

Page 41: ...to the printer port on the Analyzer and the other end to the parallel port on the printer Figure 5 Printer Port Configuring the Analyzer Initial Stream Configuration Multistream units are shipped wit...

Page 42: ...Slope Calibration Cell Offset Calibration Calibration Verification Chapter 5 InstrumentLocation None Customizable 14 character text field Chapter 5 Clock Date Time in CO USA Customizable Chapter 5 STR...

Page 43: ...ments of 5 Chapter 5 I O SETTINGS Binary Inputs Disabled State startorstop StreamX enablesor disables a specific stream Chapter 6 AC Frequency 60Hz 50Hz Chapter 6 AnalogOutputs one per stream No Outpu...

Page 44: ...ral hours of operation and should clear after that allowing the Analyzer to conduct a full countdown to sample measurement The Analyzer should be allowed to rinse down for approximately 12 24 hours be...

Page 45: ...measurement is obtained Due to the highly ionized nature of the reaction very low levels of boron are detectable Measurement Techniques The fluidics block diagram in Figure 6 shows the basic componen...

Page 46: ...mple that is free of boron Sample Measurement During a sample measurement the UPW sample is sent directly to the injection valve The sample is measured as the conductivity peak when an injection of re...

Page 47: ...rforms a zero measurement takes 10 sample measurements performs a zero measurement takes 10 sample measurements performs a zero measurement then takes the last 5 sample measurements Data Output There...

Page 48: ...SUEZ 2018 48 of 104 DLM 71000 03 EN Rev B Chapter 4 Basic Analyzer Operation THIS PAGE IS INTENTIONALLY LEFT BLANK...

Page 49: ...rolled by firmware within the Analyzer The firmware is accessed through the Main Menu on the front panel The front panel display contains the illustrated components as shown in Figure 8 and Figure 9 F...

Page 50: ...Amount of time remaining to perform selected mode once it has started Information Display Messages measurements and instructions are displayed in this area Menu Control Options The available menus or...

Page 51: ...n or reject calibration constants ACCEPT Accepts an operation or calibration constants NEXT Proceeds to next step in the procedure EDIT Makes changes to existing settings AL Alarm Number AN Analog Out...

Page 52: ...y the options for each stream 5 Press ENTER while the BORON DATA option is highlighted to display the most recent data for the stream Up to twenty four historical values are displayed as text The data...

Page 53: ...fault value is selected by pressing the AUTO key The AUTO key calculates the scale adjustment based upon currently displayed data to best fit on the screen The LEFT arrow key advances data based upon...

Page 54: ...em For the PUMP TUBING REAGENT ZERO BORON RESIN and DI RESIN maintenance items the age of the item is displayed along with the time remaining until the component must be replaced For the DATA CARD mai...

Page 55: ...e log by code number 3 Press EXIT once to exit the message log and return to the previous menu or twice to return to the Main Menu For a more detailed description of error and warning messages reviewC...

Page 56: ...P FLUSH TIME 2 minutes SAMPLE METHOD Individual ANALYSIS TIME 12 minutes STREAM SETTINGS STREAM 1 Enabled 10 Samples Stream STREAM 2 3 4 Disabled MODE There are five modes operations available ANALYSI...

Page 57: ...The spaces may be filled with a letter digits 0 9 or a blank 3 Use the UP and DOWN arrow keys to scroll through the letters numbers and the blank 4 Move the cursor to the next space by pressing the R...

Page 58: ...keys to highlight the submenu name and press ENTER FLUSH TIME This option is used to set the amount of time in minutes that the instrument will flush down after switching streams The default is 2 minu...

Page 59: ...s in more frequent reports of boron concentration but consumes reagent more quickly than at an analysis time of 12 minutes To change the ANALYSIS TIME 1 Use the UP and DOWN arrow keys and press ENTER...

Page 60: ...being reported one after every fifth sample measurement 2 Use the UP and DOWN arrow keys to increase or decrease the number of samples In INDIVIDUAL mode the number will increase from 5 to 240 in inc...

Page 61: ...ELL CONSTANTS This option displays the constants that describe the specific conductivity cell and thermistor that are installed in the Analyzer These constants are preset at the factory and should not...

Page 62: ...alyzer MAINTENANCE This option will print the maintenance status of the five maintenance items To print any of these options 1 Use the UP and DOWN arrow keys to highlight the desired option and press...

Page 63: ...the DISPLAY CONTRAST and the ALARM OUTPUTS These options do not affect how the Analyzer operates when it is performing a mode of operation To access the TOOLS menu 1 Select TOOLS from the Main Menu D...

Page 64: ...SUEZ 2018 64 of 104 DLM 71000 03 EN Rev B Chapter 5 System Configuration THIS PAGE IS INTENTIONALLY LEFT BLANK...

Page 65: ...g the wiring procedure Removal of a terminal block is recommended for wiring To remove a terminal block power down the Analyzer and unplug the power cord Use insulated needle nosed pliers to gently wi...

Page 66: ...follows Step One Wire Terminal Block TB6 The data from the Analyzer may be recorded using the 4 20 mA outputs located on terminal block TB6 The Analyzer has four analog outputs located on the terminal...

Page 67: ...show that it can be edited 2 Connect a multimeter to the analog output that is to be calibrated to determine the correct digital to analog setting 3 Press SET to activate the 4 mA analog signal The s...

Page 68: ...et within the Analyzer There are ten choices available for an alarm output OFF BORON STREAM X STATE RES ERROR ANY STREAM ERROR RES ERROR STREAM X READY STREAM X RES WARN ANY STREAM BORON ANY STREAM RE...

Page 69: ...ows 1 Press SETUP from the Main Menu to access the SETUP menu 2 Using the UP and DOWN arrow keys highlight INPUT OUTPUT and press ENTER 3 In the INPUT OUTPUT menu highlight ALARM OUTPUTS and press ENT...

Page 70: ...the Terminal Block TB5 The RS 232 output is located on terminal block TB5 Remove terminal block TB5 and wire in the standard fashion The non isolated RS 232 is not available in this version of the fir...

Page 71: ...L PORT to access the settings for the Analyzer s serial port Using the UP and DOWN arrow keys highlight the desired baud rate and press ENTER or press EXIT to exit the SERIAL PORT menu without saving...

Page 72: ...e computer to NONE For example using HyperTerminal 1 Under PORT PROPERTIES click on the SETTINGS tab 2 Click on the ASCII Setup button 3 Click on the box next to Echo Characters Locally 4 Click the OK...

Page 73: ...nds Table 6 contains a list of commands available to communicate with the Analyzer through the RS 232 port Table 7 contains a description of the output fields in the GDR Get Data Card Record command T...

Page 74: ...is low enough to trigger an error or warning ERROR The ERROR setting causes the binary output to activate when an error condition occurs on the Analyzer RES ERROR STREAM X The RES ERROR STREAM X setti...

Page 75: ...ire the next input output or close the Analyzer door turn on the Analyzer and proceed with the following instructions 1 Press SETUP from the Main Menu to access the SETUP menu 2 Using the UP and DOWN...

Page 76: ...ble individual streams on a multi stream unit The Analyzer is equipped with five binary inputs Remove terminal block TB4 and wire in the standard fashion Table 10 Binary Inputs on Terminal Block TB4 N...

Page 77: ...n DISABLED STATE and the various STREAM X choices To enable the STATE or the STREAM X choices press NEXT to highlight the polarity choices 8 Use the arrow keys to toggle between Polarity OPEN and Pola...

Page 78: ...ate of the serial RS 232 output The default baud rate is 19 200 In order to use the RS 232 output this value must match the baud rate of the computer to which the RS 232 is connected To modify the ser...

Page 79: ...4 20 mA output Alarms and binary outputs can be activated based on boron concentration or error condition for the stream Individual or averaged readings can be selected An initial flush for each stre...

Page 80: ...tions will result in the Analyzer only monitoring the stream of interest Increasing the number of samples defined for the stream that is rapidly changing will provide more analysis time on that stream...

Page 81: ...reservoir it will complete the current analysis cycle then stop and display the following warning message Unable to perform analysis Reagent level too low Although not required you can drain the old r...

Page 82: ...in the right rear corner If this port is not accessible with the bottle of reagent then install the reagent using Option 2 below 2 Unscrew and remove the fill port cap 3 Remove the cap from the bottle...

Page 83: ...ttle Failure to vent the reagent bottle could result in reagent spillage during the subsequent steps 11 Remove the reagent refiller assembly by disconnecting the 1 4 inch OD PFA tube from the valve on...

Page 84: ...et this warning level to specify the number of days to be alerted prior to the reagent needing to be replaced 1 through 90 days default is 30 The warning message is displayed as an R in the maintenanc...

Page 85: ...the right side of the Analyzer and then push the column up into its mounting location until it snaps into place You will notice the release pin come out and then snap back in as the column is installe...

Page 86: ...ORON RES for the zero column and press ENTER 4 Highlight EDIT WARNING LEVEL and press ENTER 5 Use the UP and DOWN arrow keys to adjust the warning level to the desired number of days Once the warning...

Page 87: ...ertical waste tube assembly 12 Disconnect the short tubes sample pump inlets from the bulkhead barb fittings 13 Press the EJECT key The tubing will work its way through the pump in a counter clockwise...

Page 88: ...fault is 30 The warning message is displayed as a T in the maintenance alert area of the screen To edit the number of days 1 Press SETUP from the Main Menu 2 Highlight MAINTENANCE and press ENTER 3 Hi...

Page 89: ...1 2 inch section An O ring seals the fitting body to the OD of the tubing so make sure the outside surface of the tubing is in good condition Reusing the same tube in a fitting may require re cutting...

Page 90: ...k connections The sample line filters have 1 4 inch Swagelok connections These are the only fittings in the Analyzer that require tools you will need 7 16 inch wrenches for the 1 8 inch Swagelok conne...

Page 91: ...Data Card 1 If the Analyzer is currently operating press STOP on the front panel to put the Analyzer in a stopped state 2 Turn off power by toggling the On Off switch on the side of the Analyzer to th...

Page 92: ...at the factory using highly reliable conductivity cells This calibration is stable and does not require checking at regular intervals Cleaning Instructions When cleaning the instrument use only a cle...

Page 93: ...and accessories box are shipped with the Analyzer On Site Repair The Analyzer s modular construction enables rapid troubleshooting and replacement of modules that are available from SUEZ Customer Care...

Page 94: ...ate Performed By Notes Year 2 Reagent Zero Boron Column 12 months Reagent Column 6 months Pump Tubing 12 months Year 3 Reagent Zero Boron Column 12 months Reagent Column 6 months Pump Tubing 12 months...

Page 95: ...pter 8 Maintenance Maintenance Item Period Date Performed By Notes Year 5 Reagent Zero Boron Column 12 months Reagent Column 6 months Pump Tubing 12 months Year 6 Reagent Zero Boron Column 12 months R...

Page 96: ...SUEZ 2018 96 of 104 DLM 71000 03 EN Rev B Chapter 8 Maintenance THIS PAGE IS INTENTIONALLY LEFT BLANK...

Page 97: ...mbers F Fatal Error M Maintenance W Warning ERROR CATEGORY ERROR NUMBERS ERROR CATEGORY ERROR NUMBERS Code 0 Operating System F 102 170 Code 13 Fluidics W 1401 1406 Code 1 Firmware F 201 243 Code 14 F...

Page 98: ...occurred the date and time of the most recent occurrence and a brief description of the error or warning A message log displaying 0 for the OF OCCURRENCES and NOT APPLICABLE for LAST means that no er...

Page 99: ...not able to detect a peak to allow the boron level to be determined Possible cause corrective action Very low reagent concentration replace the reagent Sample pump is not operating observe rotation I...

Page 100: ...SUEZ 2018 100 of 104 DLM 71000 03 EN Rev B Chapter 9 Message and Error Codes THIS PAGE IS INTENTIONALLY LEFT BLANK...

Page 101: ...t Information 2 D Data Card format 92 replacement 91 Declaration of Conformity 14 Display front panel 50 E Electrical Components installation 38 Error Codes 97 F Fluidics components and connections 88...

Page 102: ...SUEZ 2018 102 of 104 DLM 71000 03 EN Rev B Index Trademarks 13 Troubleshooting overview 97 W Warnings Deutsch 20 Dutch 22 English 17 Espa ol 18 Fran ais 19 Italiano 21 Warranty 14...

Page 103: ...Notes SUEZ 2018 103 of 104 DLM 71000 03 EN Rev B 104...

Page 104: ...Notes SUEZ 2018 104 of 104 DLM 71000 03 EN Rev B 104...

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Suez Sievers UPW Boron Analyzer, Operation And Maintenance Manual

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