Varian 450-GC, Руководство пользователя

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Installation
Page: 30 User Manual 450-GC Varian, Inc.
For 1177 and 1079 PTV Injectors
ECD FID
TCD
a
TSD PFPD
Initial column oven temp (
°
C) 80 80 80 80 80
Initial column oven hold time (min) 1 1 1 1 1
Program 1 column oven final temp (
°
C) 200 200 200 200 200
Program 1 column oven ramp rate (°C/min) 20 20 20 20 20
Program 1 column oven hold time (min) 5 5 5 5 5
Injector temp (
°
C)
220 220 220 220 220
Detector temp (
°
C)
300 300 220 300
300
b
Range 1 12 0.05 12 10
Initial Autozero On On On On On
TSD bead current (amps) - - -
3.0
±
0.3
-
Injection mode Splitless
Initial split state ON
Step 1 time (min) 0.01
Step 1 split state OFF
Step 2 time (min) 1.00
Step 2 split state ON
Step 2 split ratio 20
Table 14: Varian Test Sample 1177 and 1079 Conditions
Prepare the Test Sample
You are now ready to prepare your sample. For preparation of samples for
automated injection, please refer to the CP-8400 AutoSampler section on page
121.
You may inject your sample neat or diluted in a solvent. The Varian PFPD test
sample should be diluted 1:30 in iso-octane if you intend to use it for a splitless
injection. The choice of solvents depends on a number of factors, including
component solubility, type of detector and polarity of the analytical column.
Select solvents that match the polarity of your column.
a
a
T
TC CD D R Re ef f e er r e en nc ce e F Fllo ow w – – R Ra atte e f f o or r c ca ar r r r iie er r g ga as s f f llo ow w tth hr r o ou ug gh h tth he e r r e ef f e er r e en nc ce e c ce ellll iis s 2 20 0
±±
1
1 m mL L//m miin n..
b b
D
De ep pe en nd ds s o on n a ap pp plliic ca attiio on n:: S S--m mo od de e 2 20 00 0°°C C,, P P--m mo od de e 3 30 00 0°°C C a an nd d N N--m mo od de e 2 25 50 0°°C C..