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Table of contents

BlueShadow Detector 50D Instructions V7659

iii

Creating a program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .6 .2

Running a program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .6 .3

Changing a program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .6 .4

Deleting a program line . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .6 .5

Deleting a program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .6 .6

Creating and running a program with preselectable start time

(Wake-Up Program) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .7

Device Links . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .7 .1

Creating a Link . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .7 .2

Running a Link . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .7 .3

Changing a Link . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .7 .4

Deleting link lines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .7 .5

Deleting a Link . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .8

Scan menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .8 .1

Autozero scan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 .8 .2

Wavelength scan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6. Functionality tests

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6 .1

Installation Qualification (IQ) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6 .2

Operation Qualification (OQ) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7. Troubleshooting

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7 .1 LAN . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7 .2

Possible problems and solutions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7 .3

System messages . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

8. Maintenance and care

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

8 .1

Maintenance contract . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

8 .2

Cleaning and caring for the device . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

8 .3

Cleaning the flow cell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

8 .3 .1

Rinsing the flow cell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

8 .3 .2

Cleaning the lens of an analytical flow cell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

8 .3 .3

Cleaning the light guide of a preparative flow cell . . . . . . . . . . . . . . . . . . . . . . . .

8 .4

Replacing the flow cell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

9. Transport and storage

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

9 .1

Taking the device out of operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

9 .2

Packing the device . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

9 .3

Transporting the device . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

9 .4

Storing the device . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

Содержание BlueShadow Detector 50D

Страница 1: ...Detector 50D Instructions Document no V7659 HPLC HPLC...

Страница 2: ...rland on case to case basis Phone 49 30 809727 111 workdays 9 17h CET Fax 49 30 8015010 Email support knauer net KNAUER Wissenschaftliche Ger te GmbH Hegauer Weg 38 14163 Berlin Germany Phone 49 30 80...

Страница 3: ...le misuse 5 2 2 User qualification 5 2 3 Operator responsibility 6 2 4 Personal safety equipment 6 2 5 Working with solvents 7 2 5 1 General requirements 7 2 5 2 Contamination by health threatening so...

Страница 4: ...the router 21 4 6 5 Integrating LAN into the company network 21 4 6 6 Controlling several systems separately in LAN 22 4 7 Remote control 23 4 7 1 Connector assignment 23 4 7 2 Connecting the pin hea...

Страница 5: ...can 47 5 8 2 Wavelength scan 47 6 Functionality tests 48 6 1 Installation Qualification IQ 48 6 2 Operation Qualification OQ 48 7 Troubleshooting 49 7 1 LAN 49 7 2 Possible problems and solutions 50 7...

Страница 6: ...PETP 64 Polyimide Vespel 65 Ethylene tetrafluorethylene copolymer ETFC Tefzel 65 Perfluorethylenpropylen Copolymer FEP Perfluoralkoxy Polymer PFA 65 Polyoxymethylene POM POM H TF 65 Polyphenylene sulf...

Страница 7: ...e and other instructions from the KNAUER web site www knauer net library 1 2 Signal words Possible dangers related to the device are distinguished in personal and material damages Symbol Meaning DANGE...

Страница 8: ...ns Violations of General Terms and Conditions GTC 1 4 2 Transport damage The packaging of our devices provides the best possible protection against transport damage However check the packaging for tra...

Страница 9: ...ot guarantee the functionality and safety of the device Operation in potentially explosive areas without special and additio nal explosion protection Contact the KNAUER Customer Support for more infor...

Страница 10: ...learly regulate and specify responsibilities for installation operation troubleshooting maintenance and cleaning and set clear rules Ensure that all personnel who work with the device have read and un...

Страница 11: ...could get onto hot surfaces in the interior Degas solvents before use and observe their purity 2 5 2 Contamination by health threatening solvents Contamination with toxic infectious or radioactive su...

Страница 12: ...wet rooms 2 7 Maintenance care and repair Avoiding electric shock Before performing any maintenance and ser vice work disconnect the device from the power supply Tools Use only tools recommended or pr...

Страница 13: ...quest form and decontamination report Devices which are shipped without the completed document Service request form and decontamination report will not be repaired If you would like to return a device...

Страница 14: ...avelength range of 190 750 nm UV to be covered without changing the lamp Within a system it is possible to measure four wavelengths simultane ously with the help of the software control Recording of a...

Страница 15: ...BlueShadow Detector 50D accessory kit Power cable Transport protection Valid documents BlueShadow Detector 50D Instructions V7654 Declaration of Conformity 3 3 Views 3 3 1 Front view The display with...

Страница 16: ...tegrator output Fig 2 Rear view 3 4 Symbols and signs The following symbols and signs can be found on the device Symbol Meaning High voltage hazard Electrostatic discharge hazard damages to system dev...

Страница 17: ...the sides Keep the included packing list for repeat orders Keep the original packaging for safe storage or transportation 4 2 Ambient conditions 4 2 1 Operation site Observe the following requirements...

Страница 18: ...riefly when the device is switched on Main connection The electrical power supply at the operation site must be connected directly to the nearest main power connection Grounding The connectors for the...

Страница 19: ...has been disconnected Procedure Process Figure 1 Unscrew the knurled head screws 3 of the cover plate 4 Hold the flow cell securely with your hand during this procedure 2 Pull out the slide with the f...

Страница 20: ...ith 1 8 or 1 4 connec tions Procedure Process Figure 1 Remove the threaded ring 1 using a hexagonal spanner 2 Remove stainless steel cover 2 and the PEEK spacer 3 3 Insert the stainless steel cover ag...

Страница 21: ...1 mm Please use a clean cloth and avoid touching the light guide with your fingers 4 Push the light guide together with the pressure bushing back into the cell 5 Insert the PEEK spacer 3 followed by...

Страница 22: ...rough the fitting 1 2 Push the clamping ring 3 onto capillary Fig 6 Capillary fitting 3 Manually screw together the capillary 5 and the flow cell 4 Tighten the fitting with the wrench Fig 7 Capillary...

Страница 23: ...is not supported This chapter describes how to set up a chromatography system in a local area network LAN and how a network administrator can integrate this LAN into your company network The descripti...

Страница 24: ...ck on the button Properties 6 Check the settings in the tab General The correct settings for the DHCP client are a Obtain an IP address automatically b Obtain DNS server address automatically 7 Click...

Страница 25: ...www knauer net router Process 1 To open the router configuration start your Internet browser and enter the IP address does not apply for all routers 2 Enter user name and password 3 Configure the rou...

Страница 26: ...ess If more than one chromatography systems are connec ted to the same LAN and you plan on controlling them separately you can use different ports to avoid interference Therefore the port number for e...

Страница 27: ...nnector 3Fan opening 4Pin header 5RS 232 port Fig 10 Connector pin assignment on rear side Signal Explanation EV 1 Event 1 Relay contact Both relay contacts are potential free floating Relay state ope...

Страница 28: ...TL input With a high level running programs are terminated and the message Error input activated appears Start IN TTL input With a high level a program is started in hold mode or a link with the corre...

Страница 29: ...eader The single ports are used to exchange control signals The device is switched off The power plug is disconnected from the device Depressor tool Electronic defect Connecting cables to the multi pi...

Страница 30: ...the option ANA LOG in the SETUP menu To use the analog port for controlling the detector you have to set a zero point and enter a scaling value Zero point at 0 V 000 nm Scaling 100 nm per Volt If 5 V...

Страница 31: ...ve been connected 5 2 Software control There are several options for controlling the device With keypad With chromatography software 5 2 1 Switching the detector on The device is switched by the power...

Страница 32: ...he current status LED Status Green Device is ready idle status Green flashing Device is running Yellow Firmware upload in progress Yellow flashing Device initialization Red A serious error occured Red...

Страница 33: ...sub menu Activation of numeric pad usage at input value Scan menu button Selection of the wave length range for the scan and the autozero scan Output of the saved scan data Standby button Sets device...

Страница 34: ...spectral edge filters to suppress the second diffraction order are automatically activated if the shortest wavelength in all active chan nels exceeds an internal default value The activated filter is...

Страница 35: ...SETTINGS DEVICE GLP LAMPS GLP DEVICE PROGRAMS and DEVICE LINKS use the menu button and the horizontal arrow keys Navigate through main menu 1 Press to access the menu 2 Navigate between menu points by...

Страница 36: ...34 Operation BlueShadow Detector 50D Instructions V7659 5 4 2 Menu structure overview Fig 15 Menu structure overview...

Страница 37: ...connection of the detector The connections are on the rear of the device Serial interface RS232 11520 RS232 38400 RS232 19200 RS232 9600 LAN DHCP Automatic network configuration LAN manual Manual net...

Страница 38: ...independent from the in tegration time default setting and can be used as a spec tral sources quality gauge Further the intensity of the signal channel allows you to draw conclusions about the measure...

Страница 39: ...nd remains active until the signal drops below the threshold value The thres hold always relates to the signal on the measurement channel The following event outputs can be selected via the Fraction p...

Страница 40: ...ing wavelength with a scaling factor of 100 nm V This wavelength WL can then be adjusted Thus a second calibration point is generated which modifies the scaling factor Note Before operating this confi...

Страница 41: ...serial number Operating time Detector operating time Motor Working Grating motor operating move ment time CALIBRATION INFO Menu shows the line density of the optical grating as well as the fine deviat...

Страница 42: ...zontal arrow keys to scroll through the list of stored programs Select a program number of your choosing from the cur rently displayed screen by using the vertical arrow keys or the confirmation key c...

Страница 43: ...xample Additionally event 1 is enabled during the second step Process Figure 1 Select the device programs menu Device Programs 2 Select a program number from the currently displayed screen 3 Adapt tim...

Страница 44: ...d press the up ward key to change the status from Hold H to Run R program starts running 5 You can again go back from Run R to hold H by pressing the downward key with the cur sor at the status symbol...

Страница 45: ...er a new value or use the vertical arrow keys 5 6 4 Deleting a program line Process Figure 1 Select the device programs menu 2 Select the program number you wish to change 3 Navigate to the to be dele...

Страница 46: ...d the program number you wish to start by navigating via the horizontal arrow keys and editing via the numeric keypad after pressing the confirmation key or using the vertical arrow key 4 To run the w...

Страница 47: ...onfirmation key combined with the numeric pad 3 Finally confirm the selected link by using the confirmation key 4 After selecting a link use the horizontal arrow keys to navigate through the two lines...

Страница 48: ...ursor to position P P Program in the display and enter the program number you wish to run 5 Move the cursor to position R R Repeat and edit the value number of repetitions for the specified program 6...

Страница 49: ...atus will switch to hold H 6 Navigate the cursor to the H hold position and start running the link via the upward ar row key The detector status will switch to R run mode 7 The link will start running...

Страница 50: ...via vertical arrow keys 5 7 4 Deleting link lines Process Figure 1 Select the Device Links menu 2 Select the link number you wish to change 3 Navigate to the to be deleted link line e g line 02 4 Chan...

Страница 51: ...length scan the UV spectrum of a sample is recorded The wavelength of light at the output gap is changed by turning the optical grating continuously During the procedure the light absorption is mea su...

Страница 52: ...lification OQ The Operation Qualification includes an extensive functionality test accor ding to KNAUER standard OQ documents The Operation Qualification is a standardized document and free of charge...

Страница 53: ...computer 2 Check the router settings Is the router set to DCHP server Is the IP address range sufficient for all the connected devices 3 Check all connections Are the patch cable connected to the LAN...

Страница 54: ...erfering light or an electronics error Insert the test cell Inspect the calibration with a weak absorbing eluent Baseline noise Inspect the flow cell assembly Fasten the knurled head screws on the flo...

Страница 55: ...ac tive program link First pause link then delete program Cannot edit pro gram from the run ning link First pause link then edit data using chro matography software Cannot initialize LAN Check cables...

Страница 56: ...50 program lines are possible Not enough space to store program Check the detector Check the number of pro gram lines A maximum of 50 program lines are possible P Program does not exist Create a progr...

Страница 57: ...me table is not loaded First load the program then start the pro gram Time table line is empty Edit the program line Too many lines in program Check the number of program lines A maximum of 100 progra...

Страница 58: ...V light can leak out from the flow cell or the fiber optic connectors Switch o the detector or the lamps 8 1 Maintenance contract The following maintenance work on the device may only be performed by...

Страница 59: ...to restore optimal sensitivity Note Dirty lenses or fiber optic connectors could falsify the measure ment Do not touch the lens or the fiber optic connector lends with bare hands Wear gloves 8 3 1 Ri...

Страница 60: ...part 3 Lens 4 Seal ring 1 2 3 4 Fig 16 Analytical flow cell Process 1 Using the allen screwdriver loosen the threaded ring 1 2 Using tweezers or by gently tapping on a clean surface remove the compre...

Страница 61: ...guide of a preparative flow cell The preparative flow cells have a rod shaped light guide instead of the concave lens of the analytical cells Device has been switched off Power plug has been pulled F...

Страница 62: ...off the seal The seal ring needs to be renewed during every cleaning of the fiber optics 5 Clean the light guide with a clean soft cloth or with an appropriate solvent in an ultrasonic bath Make sure...

Страница 63: ...of the flow cell 2 Unscrew the knurled head screws 3 of the cover plate 4 Hold the flow cell securely with your hand during this procedure 3 Pull out the slide with the flow cell 5 towards the front...

Страница 64: ...or storage If you want to return your device to KNAUER for repairs enclose the Service Request Form which can be downloaded from our website For a secure transport note the weight and dimensions of t...

Страница 65: ...r classifies to category 8 and 9 which among others comprises laboratory equipment All distributors and importers are responsible for the disposal of old devices as defined by the WEEE directive End u...

Страница 66: ...h 6 nm at H line FWHM Wavelength accu racy 1 5 nm verification with integrated hol mium oxide filter Wavelength preci sion 0 4 nm ASTM E1657 98 Noise 0 75 x 10 5 AU at 254 nm ASTM E1657 98 Drift 2 0 x...

Страница 67: ...rs number of lamp ignitions Display Matrix keypad 11 3 General Power supply Power input 100 240 V Output 50 60 Hz Maximum power consumption 75 Watt Protection type IP 20 Dimensions W H D 242 mm x 169...

Страница 68: ...40 C unless stated otherwise Please note that higher temperatures can signifi cantly affect the stability of different materials 12 2 Plastics Polyetheretherketone PEEK PEEK is a durable and resistant...

Страница 69: ...67 Chemical compatibility of wetted materials BlueShadow Detector 50D Instructions V7659...

Страница 70: ...terized by a high hardness a low coefficient of fric tion and thus low wear In addition it is highly biocompatible DLC is inert against all acids alkalis and solvents commonly used in HPLC Ceramic Cer...

Страница 71: ...e used or with a mixture of higher compatibility They are inert against almost all solvents Exceptions are biological appli cations which are metal ion sensible and applications with extreme cor rosiv...

Страница 72: ...UER instructions online www knauer net library KNAUER Wissenschaftliche Ger te GmbH Hegauer Weg 38 14163 Berlin Phone Fax E Mail Internet 49 30 809727 0 49 30 8015010 info knauer net www knauer net KN...

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