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horiba LAQUA 2000 Series, Инструкция по эксплуатации

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Salinity Calibration 

22

●  Salinity Calibration

 Calibration is necessary for accurate salinity measurement. To perform salinity calibration 

using EC2000 or PC2000 meter, follow the procedure detailed below:

 Prerequisites

• Clean the conductivity electrode with DI (deionized) water and wipe it with tissue paper.

• Switch on the meter and plug in the conductivity electrode.

• Prepare salinity standard required for calibration.

• Ensure that the meter is in 

SAL

 mode. 

• Dip the conductivity electrode in the salinity standard until the hole at the upper part of the 

electrode is immersed.

• Before salinity calibration, set the required salinity type. The available salinity types are:

      -NACL

      -SEA.W 

(Seawater)

• The default salinity type is 

NACL

.

 

To set a desired salinity type, refer to “P3.2 Salinity Type 

Setup” on page 50.

• User can adjust the salinity value by calibration.

To abort an ongoing calibration process at any point of time, press the 

key.

Note

  

Tip

Содержание LAQUA 2000 Series

Страница 1: ...Instruction Manual Benchtop pH ORP ION Conductivity Meter LAQUA PH2000 LAQUA ION2000 LAQUA EC2000 LAQUA PC2000...

Страница 2: ......

Страница 3: ...butable to repair or modification by any person not authorized by HORIBA Advanced Techno Co Ltd Any malfunction or damage attributable to the use in an environment not specified in this manual Any mal...

Страница 4: ...II MEMO...

Страница 5: ...llation Environment This product is designed for the following environment Overvoltage category II Pollution degree 2 Maximum operating altitude 2000 m above sea level Range of application For indoor...

Страница 6: ...es and accumulators will contribute to reducing wasteful consumption of natural resources and protecting human health and the environment from potential negative effects caused by hazardous substance...

Страница 7: ...correct the interference at his own expense Any changes or modifications not expressly approved by the party responsible for compliance could void the user s authority to operate the equipment Korea...

Страница 8: ...AC adapter 1 2 Cable 2 Stand 2 Printer 2 Electrode 2 SJ T 11364 This form is prepared in accordance with SJ T 11364 GB T 26572 Denotes that the amount of the hazardous substance contained in all of t...

Страница 9: ...ded will result in death or serious injury This is to be limited to the most extreme situations This indicates a potentially hazardous situation which if not avoided could result in death or serious i...

Страница 10: ...utiliser le produit de mani re garantir son utilisation correcte et s re De m me rangez le manuel dans un lieu s r de mani re pouvoir vous y reporter lorsque cela est n cessaire Le contenu du pr sent...

Страница 11: ...gt riktlinjerna i EN61326 1 Om den anv nds i industrimilj er kan de elektromagnetiska st rningarna orsaka tekniska fel hos produkten Om produkten ska anv ndas i s dana milj er kan anv ndaren beh va vi...

Страница 12: ...zaradcze Produkt jest przeznaczony do u ycia w poni szym rodowisku zdefiniowanym w normie EN61010 1 Kategoria przepi ciowa II Stopie zanieczyszczenia 2 NLD Veiligheidsinformatie Lees deze handleiding...

Страница 13: ...For Your Safety XI JPN EN61326 1 EN61010 1 II 2...

Страница 14: ...ing in a fire or an accident Harmful chemicals Some electrodes are used with hazardous standard solutions Handle them with care The internal solution of pH electrode is highly concentrated potassium c...

Страница 15: ...ween the instrument and a personal computer referred to as PC in the rest of this document may fail because of environmental conditions such as electromagnetic noise Do not use an object with a sharp...

Страница 16: ...on XIV Manual Information Description in this manual This interprets the necessary points for correct operation and notifies the important points for handling the product This indicates reference info...

Страница 17: ...cting an Electrode 6 Changing the Operation Mode 7 Changing the Measurement Parameter 9 Calibration 10 pH Calibration 10 ORP mV Calibration 13 Ion Calibration 15 Conductivity Calibration 18 TDS Calibr...

Страница 18: ...2 TDS Setup 45 P3 SAL Setup 48 Data Setup 52 General Setup 56 Clock Setup 62 Maintenance and Storage 65 Contact for Maintenance 65 Maintenance and Storage of the Instrument 65 Maintenance and Storage...

Страница 19: ...conductivity resistivity TDS salinity and temperature This section describes the package content key features and product components of LAQUA 2000 series benchtop meters Package Content After opening...

Страница 20: ...me clock Automatic Temperature Compensation ATC with temperature calibration Adjustable auto shut off time 1 to 30 minutes Auto stable auto hold and real time measurement modes with reading stability...

Страница 21: ...Auto Hold modes 4 Appears when the measured value display is stable and fixed in Auto Hold mode 5 Temperature Display Area Displays the measured temperature temperature unit and ATC MTC 6 Measured Val...

Страница 22: ...buffer values and conductivity standards Electrode Icon pH Average Slope Ion Average Slope Conductivity Average Calibration Factor Salinity Calibration Factor Excellent 95 0 to 105 0 90 1 to 199 9 0 9...

Страница 23: ...from the measurement mode to the data mode MODE key In the measurement mode changes measurement parameters SET key Switches from the measurement mode to the setup mode ENTER key Determines the select...

Страница 24: ...form calibration measurement it is necessary to use the appropriate electrode for measurement parameter Use the following procedure to correctly connect the electrode to the instrument 1 Insert the el...

Страница 25: ...four available modes depending on the purpose of use The status icon indicates the current mode Icon Name Function Measurement mode Performs measurement Calibration mode Performs calibration Data mode...

Страница 26: ...mode Press the key to change to the measurement mode Calibration mode In the measurement mode press the key to change to the calibration mode Data mode In the measurement mode press the key to change...

Страница 27: ...an electrode corresponding to the measurement parameter is required In the measurement mode the measurement parameter can be changed by pressing the key Model Measurement Parameters PH2000 pH ORP mV...

Страница 28: ...buffer Perform two point calibration using pH 7 and 4 for acidic sample pH 7 and 10 for alkaline sample Perform three point calibration using pH 7 4 and 10 if you are unsure of the expected sample pH...

Страница 29: ...ll be a sound indicating that reading is stable 4 Press the ENT key to confirm and save calibration data 5 Meter displays CAL DONE indicating end of the pH calibration procedure Electrode icon pH buff...

Страница 30: ...value 5 Press the ENT key to confirm and save calibration data 6 Meter displays CAL DONE indicating end of the pH calibration procedure Electrode icon and number of calibration points done e g 1 PT fo...

Страница 31: ...that the solution level is at least 3 cm from the electrode tip Absolute value measurement mode and relative value measurement mode are the two types of measurement mode available for ORP mV measurem...

Страница 32: ...es 4 Wait for the to stabilize When it stabilizes there will be a sound indicating that reading is stable 5 Use the and keys to adjust the mV value to the ORP standard solution value 6 Press the ENT k...

Страница 33: ...nd mmol L mol L For selecting the ion electrode type or setting the valence of the ion to be measured refer to P1 2 Ion Electrode Type Setup on page 35 Seven ion electrode types are available NH3 Ammo...

Страница 34: ...going calibration process at any point of time press the key It is recommended to clear the previous calibration data before performing calibration For erasing the calibration data refer to P1 3 Calib...

Страница 35: ...nt location 4 Press the ENT key to confirm and save calibration data 5 Meter displays CAL DONE that indicates end of the ion calibration procedure Electrode icon and number of calibration points done...

Страница 36: ...andard until the hole at the upper part of the electrode is immersed Salinity TDS and resistivity of a sample solution are calculated from the measured value of conductivity In conductivity calibratio...

Страница 37: ...able 4 Press the ENT key to confirm and save calibration data 5 Meter displays CAL DONE indicating end of the conductivity calibration procedure Electrode icon and calibrated conductivity standard ico...

Страница 38: ...able 4 Use the and keys to enter the electrical conductivity value of the conductivity standard Press the key to adjust the decimal point location 5 Press the ENT key to confirm and save calibration d...

Страница 39: ...will be recalculated accordingly Set the appropriate TDS curve Available TDS curves in the meter are as follows LINR Linear KCl curve with adjustable factor from 0 40 to 1 00 442 Myron L 442 non line...

Страница 40: ...Prepare salinity standard required for calibration Ensure that the meter is in SAL mode Dip the conductivity electrode in the salinity standard until the hole at the upper part of the electrode is imm...

Страница 41: ...hat reading is stable 4 Use the and keys to enter the salinity standard value 5 Press the ENT key to confirm and save calibration data 6 Meter displays CAL DONE indicating end of the salinity calibrat...

Страница 42: ...it with tissue paper Switch on the meter and plug in the electrode and temperature sensor Dip the electrode in a solution with known temperature until its temperature sensor is immersed Wait for 5 min...

Страница 43: ...Press the key to switch to temperature calibration mode Meter displays measured temperature value 3 Use the and keys to adjust the temperature to the required value 4 Press the ENT key to confirm and...

Страница 44: ...ve the measured data press the ENT key Meter displays the location number of the saved data for 2 seconds and then the previous screen automatically If the data storage limit reaches 2000 memory data...

Страница 45: ...the communication port of the PC 2 Install the DAS in the PC and follow the procedures in the DAS instruction sheet Printing Data Connect the instrument to a printer using the phono to 25 pin d sub pr...

Страница 46: ...e Default pH buffer group in buffer setup is USA You can change it to NIST NIST2 DIN or CUST Custom if required Erasing previous calibration data is recommended for accurate calibration Default calibr...

Страница 47: ...ENT key P1 1 BUFF screen appears 3 Press the ENT key default BUFF USA appears 4 Use the keys to change the pH buffer group to NIST NIST2 DIN or CUST 5 Press the ENT key P1 1 BUFF screen appears This...

Страница 48: ...BUFF screen appears 3 Press the key P1 2 RESOL screen appears 4 Press the ENT key default resolution 0 001 screen appears 5 Use the keys to change the resolution to 0 01 or 0 1 6 Press the ENT key P1...

Страница 49: ...ears 3 Press the key P1 2 RESOL screen appears 4 Press the key P1 3 C ALR screen appears 5 Press the ENT key default DAYS screen appears 6 Use the and keys to set number of days from 1 to 90 7 Press t...

Страница 50: ...ars 4 Press the key P1 3 C ALR screen appears 5 Press the key P1 4 C CLR screen appears 6 Press the ENT key default CCLR NO screen appears 7 Use the keys to change to YES This erases the calibration d...

Страница 51: ...mode Default ion concentration unit is g L mg L g L You can change it to ppm ppt or mmol L mol L if required Default ion electrode type is NH3 Ammonia You can change it to CL Chloride FL Fluoride NO3...

Страница 52: ...the ENT key P1 1 UNIT screen appears 3 Press the ENT key default g L mg L g L appears 4 Use the keys to change the ion concentration unit to ppm ppt or mmol L mol L 5 Press the ENT key P1 1 UNIT scre...

Страница 53: ...appears 5 Use the keys to change the electrode type to CA Calcium POT Potassium NO3 Nitrate FL Fluoride CL Chloride or CUST Custom If CUST is selected default CHRG 1 screen appears after pressing ENT...

Страница 54: ...Ion Setup 36 key key key key...

Страница 55: ...2 TYPE screen appears 4 Press the key P1 3 C CLR screen appears 5 Press the ENT key default CCLR NO screen appears 6 Use the keys to change to YES This erases the ion calibration data 7 Press the ENT...

Страница 56: ...value is 1 0000 You can set a value in between 0 0700 to 13 000 Default conductivity unit is S cm You can change the unit to S m Default auto calibration setup is ON To perform manual calibration cha...

Страница 57: ...ey P1 1 CELL screen appears 3 Press the ENT key default CELL 1 0000 appears 4 Use the and keys to set the cell constant in between 0 0700 to 13 000 Use the key to move the decimal point 5 Press the EN...

Страница 58: ...he ENT key P1 1 CELL screen appears 3 Press the key P1 2 UNIT screen appears 4 Press the ENT key default UNIT S cm appears 5 Use the keys to change the conductivity unit to S m 6 Press the ENT key P1...

Страница 59: ...ears 3 Press the key P1 2 UNIT screen appears 4 Press the key P1 3 A CAL appears 5 Press the ENT key default A CAL ON screen appears 6 Use the keys to change to OFF This enables the manual calibration...

Страница 60: ...the key P1 2 UNIT screen appears 4 Press the key P1 3 A CAL appears 5 Press the key P1 4 T CFF appears 6 Press the ENT key default 2 00 appears 7 Use the keys to set the temperature coefficient in bet...

Страница 61: ...screen appears 4 Press the key P1 3 A CAL appears 5 Press the key P1 4 T CFF appears 6 Press the key P1 5 T REF appears 7 Press the ENT key default 25 0 C appears 8 Use the keys to set the reference t...

Страница 62: ...1 3 A CAL appears 5 Press the key P1 4 T CFF appears 6 Press the key P1 5 T REF appears 7 Press the key P1 6 C CLR appears 8 Press the ENT key default NO screen appears 9 Use the keys to change to YES...

Страница 63: ...on the meter Ensure that the meter is in TDS measurement mode Default TDS curve is LINR Linear You can change the TDS curve to 442 or EN EN27888 or NACL NaCl For LINR curve default multiplier factor...

Страница 64: ...default FACT LINR appears 5 Use the keys to select a TDS curve If LINR is desired press ENT key to select and use and keys to set a factor in between 0 40 to 1 00 default 0 50 6 Press the ENT key P2...

Страница 65: ...3 Press the ENT key P2 1 FACT screen appears 4 Press the key P2 2 UNIT screen appears 5 Press the ENT key default UNIT mg L g L screen appears 6 Use the keys to change the TDS unit to ppm ppt 7 Press...

Страница 66: ...nsure that the meter is in salinity measurement mode Default salinity unit is ppt parts per thousand You can change the unit to percentage Default salinity type is NACL NaCl You can change the salinit...

Страница 67: ...creen appears 3 Press the key P3 SAL screen appears 4 Press the ENT key P3 1 UNIT screen appears 5 Press the ENT key default UNIT ppt appears 6 Use the keys to change the salinity unit to 7 Press the...

Страница 68: ...SAL screen appears 4 Press the ENT key P3 1 UNIT screen appears 5 Press the key P3 2 TYPE screen appears 6 Press the ENT key default TYPE NACL NaCl appears 7 Use the keys to change the salinity type t...

Страница 69: ...P3 1 UNIT screen appears 5 Press the key P3 2 TYPE screen appears 6 Press the key P3 3 C CLR screen appears 7 Press the ENT key default C CLR NO appears 8 Use the keys to change to YES This erases th...

Страница 70: ...nction follow the procedure detailed below Prerequisites Switch on the meter Keep the meter in either pH or ion or conductivity mode Default data log interval is which indicates no data log interval h...

Страница 71: ...P2 1 P4 1 LOG screen appears 4 Press the ENT key default log interval appears 5 Use the and keys to set the data log interval from 2 to 999 seconds 6 Press the ENT key P2 1 P4 1 LOG screen appears Th...

Страница 72: ...P2 2 P4 2 PRINT screen appears 5 Press the ENT key default NO appears 6 Use the keys to change to YES This prints all stored data 7 Press the ENT key LOC END screen appears briefly after the last dat...

Страница 73: ...ppears 4 Press the key P2 2 P4 2 PRINT screen appears 5 Press the key P2 3 P4 3 D CLR screen appears 6 Press the ENT key default NO appears 7 Use the keys to change to YES This erases all data 8 Press...

Страница 74: ...mode is activated Default reading stability mode setup in measurement mode is Auto Stable AS You can change it to Auto Hold AH or Real Time RT Default auto shut off time is 30 minutes You can set the...

Страница 75: ...gs both and are inactivate 1 Press the key P1 PH ION COND screen appears 2 Press key P2 P4 DATA screen appears 3 Press key P3 P5 GEN screen appears 4 Press the ENT key P3 1 P5 1 STBLE screen appears 5...

Страница 76: ...4 Press the ENT key P3 1 P5 1 STBLE screen appears 5 Press the key P3 2 P5 2 A OFF screen appears 6 Press the ENT key default auto shut off time 30 minutes appear 7 Use the and keys to adjust the auto...

Страница 77: ...pears 4 Press the key P3 1 P5 1 STBLE screen appears 5 Press the key P3 2 P5 2 A OFF screen appears 6 Press the key P3 3 P5 3 C F screen appears 7 Press the ENT key default temperature unit C appears...

Страница 78: ...P5 2 A OFF screen appears 6 Press the key P3 3 P5 3 C F screen appears 7 Press the key P3 4 P5 4 PASS screen appears 8 Press the ENT key default PASS OFF appears 9 Press the key PASS ON screen appears...

Страница 79: ...2 P5 2 A OFF screen appears 6 Press the key P3 3 P5 3 C F screen appears 7 Press the key P3 4 P5 4 PASS screen appears 8 Press the key P3 5 P5 5 RESET screen appears 9 Press the ENT key default reset...

Страница 80: ...equisites Switch on the meter Keep the meter in either pH or ion or conductivity mode Setting the date and time is necessary before using the instrument for the first time Date and time are captured c...

Страница 81: ...y P4 1 P6 1 DATE screen appears 6 Press the ENT key default set year appears 7 Use the and keys to change the year 8 Press the ENT key default set month appears 9 Use the keys to change the month 10 P...

Страница 82: ...ears 5 Press the ENT key P4 1 P6 1 DATE screen appears 6 Press the key P4 2 P6 2 TIME screen appears 7 Press the ENT key default set hour appears 8 Use the and keys to change the hour 9 Press ENT key...

Страница 83: ...soft dry cloth If it is difficult to remove the dirt wipe it gently with a cloth moistened with alcohol The instrument is made of solvent resistant materials but is not resistant to all chemicals Do n...

Страница 84: ...ated below depending on the type of dirt After cleaning rinse the electrode with pure water or deionized water However for pH and ORP electrodes different cleaning solutions should be used to clean di...

Страница 85: ...ctrode is stored the concentration of the reference internal solution outer tube may change For this reason replace the reference internal solution outer tube with a dropper or similar tool about once...

Страница 86: ...in deionized water or with the protective cap filled with deionized water and attached to the electrode To store the electrode for a long period clean it well and attach the protective cap filled wit...

Страница 87: ...y the pH buffer Check the calibration solution and use fresh one if required STD ERR Cannot auto recognize standard solution The instrument cannot identify the standard solution Check the calibration...

Страница 88: ...librated has been exceeded Clear the calibration data Cause How to solve problem The electrode is dirty Clean the electrode The electrode is cracked Replace the electrode The wrong internal solution i...

Страница 89: ...rode that is appropriate for the sample check the pH electrode selection guide in our catalogue or refer to our website Cause How to solve problem The electrode is dirty Clean the electrode The electr...

Страница 90: ...place the electrode Calibration is not performed or performed incorrectly Perform calibration correctly Instrument defect Check as explained below Cause How to solve problem Effect of the sample solut...

Страница 91: ...rent from sea level To eliminate the pressure difference between the inside and outside of the instrument briefly open and then close the serial connector cover After opening correctly close the cover...

Страница 92: ...ture The meter is intelligent to detect the temperature and pH value associated with buffer when calibration is performed It remembers all the temperature vs pH value for all the standards The pH vs t...

Страница 93: ...70 4 03 6 84 9 07 11 98 45 1 70 4 04 6 83 9 04 11 84 50 1 71 4 06 6 83 9 01 11 70 55 1 72 4 08 6 83 8 99 11 57 Temp C pH 1 68 pH 4 01 pH 6 86 pH 10 01 pH 12 46 0 1 67 4 01 6 98 10 32 13 42 5 1 67 4 01...

Страница 94: ...7 5 1 09 3 10 4 66 6 87 9 43 13 37 10 1 09 3 10 4 66 6 84 9 37 13 37 15 1 09 3 08 4 65 6 82 9 32 13 17 20 1 09 3 07 4 65 6 80 9 27 12 96 25 1 09 3 06 4 65 6 79 9 23 12 75 30 1 10 3 05 4 65 6 78 9 18 1...

Страница 95: ...5 16 70 1173 10 72 94 4 17 71 1199 10 95 96 3 18 73 1225 11 19 98 2 19 74 1251 11 43 100 2 20 76 1278 11 67 102 1 21 78 1305 11 91 104 0 22 79 1332 12 15 105 9 23 81 1359 12 39 107 9 24 82 1386 12 64...

Страница 96: ...Printout Summary 78 Appendix 2 pH mV Relative mV Printer Format Measurement...

Страница 97: ...Printout Summary 79 Ion Conductivity Resistivity...

Страница 98: ...Printout Summary 80 Salinity TDS...

Страница 99: ...Printout Summary 81 Printer Format Data Log...

Страница 100: ...Printout Summary 82 Ion pH Printer Format Calibration...

Страница 101: ...Printout Summary 83 Conductivity Salinity...

Страница 102: ...ution 4 Significant digits Accuracy 0 3 full scale or 0 2 mV whichever is higher Calibration Points Up to 5 Conductivity Range 0 000 to 1 999 S cm k 0 1 2 00 to 19 99 S cm k 0 1 1 20 0 to 199 9 S cm k...

Страница 103: ...00 to 10 00 Resolution 0 1 ppt 0 01 Accuracy 0 2 full scale Salinity Curves NaCl Seawater Calibration Option Yes Temperature Range 30 0 to 130 0 C 22 0 to 266 0 F Resolution 0 1 C F Accuracy 0 5 C 0...

Страница 104: ...Power Rating AC Adapter Input Voltage 100 240VAC 10 50 60Hz Power Rating Instrument Input Voltage 7V Power Consumption 0 7 W 100 mA Dimensions 155 L x 150 W x 67 H mm Weight Approx 765g for PH2000 ben...

Страница 105: ...0 19 99 mS m 0 000 1 999 mS m Display Range Cell Constant 0 1 cm 1 1 cm 1 10 cm 1 OR Over Range 0 200 2 000 S cm 20 0 199 9 mS cm 2 00 19 99 mS cm 200 1999 S cm 20 0 199 9 S cm 2 00 19 99 S cm 0 000 t...

Страница 106: ...88...

Страница 107: ......

Страница 108: ...yoto 601 8551 Japan http www horiba adt jp For any questions regarding this product please contact your local agency or inquire from the following website http global horiba com contact_e index htm Lo...

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