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Electrothermal INTEGRITY 10, Инструкция

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 Page 7 of 80 

                                    M8024 Issue 3.4                                         

For use with master product           

 

                                                                                                                                                                                                                                         software V3.5.1.8 and above.

                                   

 

 

 

 

 

Do not

 touch the inside of the cells when the product is in operation.  

Take care when handling HOT & COLD glassware 
 

 

Do not

 lean or stretch over the unit when in operation. 

 

           Keep the Mains Plug and Lead set cable away from the heating surface. 

 

 

 

Touch Screen Warning.

 The screen is impervious to Acetone. It is recommended that any 

chemical spillage is wiped off the screen immediately. 
 

 

Warning

: Standard glassware supplied for the Integrity product is not designed for high 

pressure applications. Maximum operating pressure of standard glassware with Inerting cap 
fitted is 0.5bar. 

 

 
 

 

ATS10075 
24mm 
diameter 
Glassware

 

Borosilicate glass, 1.6mm wall thickness. General glassware is not pressure tested.   

 
Warning

: Glass vessels can explode or implode violently, either spontaneously from stress 

failure caused by pressure or vacuum, or from accidental impact.  
Carefully check glass vessels for star cracks, scratches or etching marks before each use. 
Cracks can increase the likelihood of breakage or may allow chemicals to leak into the 
equipment.  
Conduct all pressure and vacuum operations in glass vessels behind adequate shielding and 
use Personnel Protective Equipment (Full face guard, gloves, protective clothing) during 
handling. 
 

 

Risk assessment is required by user to ensure adequate safety precautions / use of, screens 
, hoods,  PPI etc. for process being operated  with due regard to use of glassware  at 
pressures other than atmospheric. 
 

Test undertaken by Electrothermal Engineering  on sample new glassware at ambient 
temperature, assembled with ATS10377 inerting cap, (tested under water)  indicate withstand 
pressure of 0.5 bar gauge. 
 
When intering cap is fitted, the septum cap can acts as a pressure relief valve which can 
open suddenly and blow out (with  some velocity) at pressures over 2 bar gauge.  (NB: 
Sampling probes inserted through Septum cap may restrict this pressure relief action.) 

 

Risk assessment is required by end user to ensure adequate safety precautions / use of, 
screens , hoods,  Personal Protective Equipment etc. for process being operated  with 
glassware at pressures other than atmospheric. 
 
Warning: When inerting cap is fitted, the septum cap can acts as a pressure relief valve which 
can open suddenly and blow out (with some velocity) at pressures approaching 2 bar gauge.  
(NB: Sampling probes inserted through Septum cap may restrict this pressure relief action.) 

 

For high pressure applications, please contact : 

[email protected]

 

 

For high pressure applications, please contact Bibby Scientific Help 

 

 

Additional 

pressure safety 
information. 

 

ATS10377 
Inerting Cap  

 
See below 

Viton (main seal 

and o rings) 

 

Viton is resistant to a wide range of chemicals including oils, aqueous media and most 
other fluids. Recommend check for specific chemicals by reference to internet search 
engine. Numerous web sites give data on Viton chemical resistance. 

 http://www.dupontelastomers.com/Products/Viton/viton.asp

 

PFTE Cap and 

valve spindle 

PTFE is resistant to a wide range of chemicals, including  ozone, chlorine, acetic acid, 
ammonia sulphuric acid and hydrochloric acid. The only chemicals known to affect these 
coatings are molten alkali metals and highly reactive fluorinating agents. 
Recommend check for specific chemicals by reference to internet search engine. 
http://www2.dupont.com/Teflon_Industrial/en_US/tech_info/prodinfo_ptfe.html 

Содержание INTEGRITY 10

Страница 1: ...Page 1 of 80 M8024 Issue 3 4 For use with master product software V3 5 1 8 and above Integrity 10 Reaction Station Power Supply unit INTEGRITY 10 REACTION STATION PS20000 INSTRUCTION BOOK ...

Страница 2: ...16 7 5 Turn Unit Off Page 16 7 6 Splash Screen Page 16 7 7 Clock and Date settings Page 17 7 8 Communication Protocol Selection Page 19 7 9 View Firmware Release Set Page 20 7 10 Manual Control Page 20 7 11 Profile Control Page 27 7 12 Name and Storing a Profile Page 37 7 13 Stored Profile View and Copy Page 42 7 14 Saving an Experiment Page 46 7 15 Reviewing Stored Experiment Data Page 50 7 16 Ou...

Страница 3: ... any purpose except as authorised in writing by Bibby Scientific Limited Bibby Scientific Limited reserves the right to alter change or modify this document without prior notification In the interest of continued development Bibby Scientific Limited reserve the right to alter or modify the design and or assembly process of their products without prior notification This product is manufactured in G...

Страница 4: ...obe Over Head Stirrer and Dossing pumps can all be added to further enhance your system The system is completed with a Reflux unit designed to prevent fluid sample solution losses from open exposed glass vessels test tubes See accessories or refer to customer support 1 5 For standalone use the Integrity 10 is easy to set up using the touch screen With an intuitive menu system operation is both qui...

Страница 5: ...in order preserve the protection afforded by the equipment To prevent injury or equipment damage it is the manufacturer s recommendation that all persons using this equipment are suitably trained before use 2 2 Symbols defined Caution risk of danger See note or adjacent symbol Protective conductor terminal to be earthed Do not loosen or disconnect Caution risk of electric shock Recyclable Packing ...

Страница 6: ...rd or other means of extraction Consult your company practice Ensure equipment is used on a clean dry non combustible solid work surface with at least 300mm suitable clearance all around from other equipment Ensure the PSU is positioned on a clean dry non combustible surface with a sufficient space for the power cable to Integrity 10 and mains input lead and plug set to enter exit without undue be...

Страница 7: ...ed with ATS10377 inerting cap tested under water indicate withstand pressure of 0 5 bar gauge When intering cap is fitted the septum cap can acts as a pressure relief valve which can open suddenly and blow out with some velocity at pressures over 2 bar gauge NB Sampling probes inserted through Septum cap may restrict this pressure relief action Risk assessment is required by end user to ensure ade...

Страница 8: ...fied in accordance with ASTM D 1418 as VMQ Recommend check for specific chemicals by reference to internet search engine 316 Stainless Steel gas nozzle Recommend check for specific chemicals by reference to internet search engine 316 Stainless steel 2mm dia sampling hole bung Recommend check for specific chemicals by reference to internet search engine ...

Страница 9: ...PLEASE SEE SECTION 5 10 For your future reference please record your products Serial and Model numbers PS20000 Unit Serial Number PS20000 Unit Model Cat Number PS20000 PSU Serial Number PS20000 PSU Model Cat Number Item Description Qty 1 Instruction book 1 2 Integrity 10 PSU 1 3 Integrity 10 UNIT 1 4 Mains cord and lead set illustration only A R 5 Stir bars Pkt10 1 6 Power cable assembly illustrat...

Страница 10: ...be undertaken by competent trained personnel using suitable test equipment environment DC test voltage should be no more than 1 414 times normal AC test value for a class I grounded equipment The test equipment process should incorporate a discharge procedure to remove any stored DC charge that may remain on the PSU 5 1 2 This equipment must be earthed grounded to a fixed earth grounded mains sock...

Страница 11: ...on the end user should ensure that the cooling water supply is of distilled water quality 2 Additives are not recommended 3 A coolant inline filter is recommended to filter to 75 micron This should be checked cleaned at intervals to suit local operating conditions 4 Minimal annual service check by Bibby Scientific Limited or it s designated service agent is recommend which includes flushing back f...

Страница 12: ...sposed of in accordance with regulations Do Not dispose of product in a fire as batteries may explode 6 6 EuP and Eco Operation The chiller and Integrity 10 complete the full reaction system For optimised operation observe the following Do not set the chiller to operate at temperatures below 5 C Do not use a chiller larger than the specification required See recommended chillers section 11 Parts a...

Страница 13: ... Bus socket for driving accessories 6 In out coolant water supply 7 4 pin CEEP plug 8 Data plate label Found on underside of the Reaction unit 9 Touch sensitive screen 10 USB ports Master and Slave 11 Ethernet RJ45 Socket 12 GSIOC protocol socket 13 RS232 485 protocol socket 14 SD card slot Power supply overview 15 On Off button switch 16 Front grill Cooling vents 17 Earth test point 18 IEC mains ...

Страница 14: ...re at a safe to touch Between 40 and 5 C Always turn off the coolant water supply before removing the drip tray Insert reduction sleeve 7 2 1 Insert reduction sleeves by pushing them straight into the cells Reduction sleeves may be fitted into any position Remove reduction sleeve 7 2 2 Release the latch on the top of the Integrity unit and lift off the drip tray 7 2 3 Push in the oil seal retentio...

Страница 15: ...plied by Electrothermal into the SD card slot Card to have contacts facing the back Leave the SD card in place during use The SD card is acting as the system hard drive Note Your SD card has been programmed for use specific with the Integrity system for which it was supplied If the card is swapped with another SD card programmed for use with another integrity system the touch screen buttons may no...

Страница 16: ...e power on switch The Integrity 10 can be used in conjunction with STEM Integrity control software or it can be run in standalone mode In standalone mode the Integrity 10 can be set up and run via manual control or via a profile set up 7 5 Turn Unit off 7 5 1 Depress the Power Supply button once again to turn off the unit 7 6 Splash Screen 7 6 1 When the Integrity 10 is first powered up it will go...

Страница 17: ...Accurate clock time is required when using data storage facility as experiment data stored is time stamped 7 7 1 With the Integrity 10 connected to mains power and water supply as detailed section 5 turn on as detailed in 7 4 7 7 2 A splash screen will appear to indicate the unit is functioning and performing a self check activity 7 7 3 A home screen will appear Touch the settings Icon to enter se...

Страница 18: ...screen from which you commence operation Alternative method May reduce button pressing 7 7 7 Touch the display field you wish to set 7 7 8 Select the setting required from the touch pad screen Touch the green tick to except the setting or touch the Red cross to clear the field and re enter the field setting The Green back arrow will take you back to the previous screen Note Daylight saving time se...

Страница 19: ...ity 10 connected to mains power and water supply as detailed Section 5 turn on as detailed in 7 4 7 8 2 A splash screen will appear to indicate the unit is functioning and performing a self check activity 7 8 3 A home screen will appear Touch the settings Icon to enter settings mode Note Setting mode can only be entered immediately after the Integrity has been switch on Once run settings have been...

Страница 20: ...software version set number is displayed across the bottom of the setting screen The Integrity 10 can be used in conjunction with STEM Integrity control software or it can be run in standalone mode In standalone mode the Integrity 10 can be set up and run via manual control or via a profile set up 7 10 Manual Control Note Ice will form round the Integrity 10 cell assemblies when the unit is run fo...

Страница 21: ...tly touching the button position on the touch screen glass panel 7 10 4 Either or both the desired temperature or Stir speed must be entered All other fields are optional Greyed out fields indicate an optional setting Temperature Set Touch the field box on the display screen to enter a setting into the appropriate field To enter a temperature setting touch the temperature field box By touching the...

Страница 22: ... field allows selection Use the keypad to enter the required temperature setting Press the button to accept the temperature value entered But touching the button the setting entered in that field will be removed 7 10 6 Stir Speed The display is returned to the field selection screen Continue entering field setting For example set the stir speed Touch the Stir speed field 7 10 7 As with the process...

Страница 23: ...red run time using the keypad Note Enter the time in minutes Example 4 hours 25 minutes is 265 minutes Note Maximum run time entry is 9999 minutes 166 hours and 39 minutes 7 10 10 Ramp The optional field of Ramp rate may be changed using the same procedure Touch the field box to select the setting keypad Note The default setting for ramp rate is 5 0 C per minute Graduations can be set as low as 0 ...

Страница 24: ...ng using the keypad 7 10 14 Copy Function Once the user has completed entering all the required field entries the entered settings may be copied over into another cell Touch the copy button to write the settings to the internal clipboard The home screen is now shown Touch the cell you wish to copy the setting into and the fields will have the copied setting filled in You may now press start The ce...

Страница 25: ...0 17 Touch the adjust button and then select the Manual control from the next screen 7 10 18 Select the field or fields to be adjusted as per the original run setup 7 10 19 Check the All cells spot if you wish to apply the change to all cells or touch the copy button for pasting the change into selected other cells 7 10 20 Touch the green tick button to accept and commence running the change Note ...

Страница 26: ...stir speed In this example the stirring facility was not activated 7 10 22 The graph is accumulative and will auto rescale as a cell is run 7 10 23 When a Green band is seen around the cell this indicates the cell has setting written to the field s The cell may not be running but it has been set ready for operation 7 10 24 A Red band around the cell indicates the cell has finished a run and associ...

Страница 27: ...0 C 7 11 1 A profile will allow the user to set up and run a step cycle and if required repeat that same cycle as many as 10 times 7 11 2 From the home screen touch the required cell the profile is to be set up in This time select the Profile setup button 7 11 3 This next screen shows a profile step To complete the profile all fields must be completed Once a field has change from a grey state it c...

Страница 28: ...r once the entire temperature has been entered As with manual control the will take you back to the previous screen This button is used to except a value and the is used to remove an incorrect field entry Use the keypad to enter you initial start temperature 7 11 5 Initial hold time is a similar in operation to the previous field Touch the field to enter the required setting All white field boxes ...

Страница 29: ... Initial hold time field 7 11 7 Initial Ramp The initial ramp rate is the rate of temperature change required The Initial ramp may be set to decrease in temperature as well as increase Touch the field to enter the require setting Note The default setting for ramp rate is 5 0 C per minute Graduations can be set as low as 0 1 C per minute When 0 0 is entered the ramp rate will climb as rapidly as po...

Страница 30: ...green tick button to except the set value Note To enter 25 6 Press 2 then 5 then 6 followed by the minus sign 7 11 11 Set Maximum Upper Limit To help reduce exothermic reaction when mixing certain chemicals a maximum upper temperature limit may be set When the Integrity10 senses an unregistered change in temperature state action will be taken to prevent the change exceeding the set maximum tempera...

Страница 31: ...ch the red cross If you have changed your mind and no longer wish to set a maximum Upper limit touch the back button to return to the previous screen and the touch the red cross Note To enter 25 6 Press 2 then 5 then 6 followed by the minus sign 7 11 13 Plateau time This is the length of time the user wishes to have the unit run at the target temperature The data field to enter the required time v...

Страница 32: ...sh to set a maximum Upper limit touch the back button to return to the previous screen and the touch the red cross 7 11 15 Final Temperature The final temperature is the temperature you wish the profile conclude the step at Touch the field to select the keypad for entering the required settings 7 11 16 Use the keypad to enter the final temperature value This can be a negative value as well as a po...

Страница 33: ...minute Graduations can be set as low as 0 1 C per minute When 0 0 is entered the ramp rate will climb as rapidly as possible to the desired target temperature 7 11 18 Use the keypad to make the field entry Touch the green tick button to except the set value 7 11 19 Hold Time This is the time the user wishes to have the final temperature sit at before either completing the run profile and switching...

Страница 34: ...4 hours 25 minutes is 265 minutes 7 11 21 Stir Speed The stir speed default is 0 RPM At this speed the stir facility is turned off Turn the stir function on by entering a value The smallest lowest stir speed that may be selected is 250RPM The maximum stir speed value that may be set is 1200RPM Touch the field to enter setting entry mode 7 11 22 Use the keypad to enter a stir speed value ...

Страница 35: ...enter via the keypad the number of times they wish to set up a loop Use the green Tick to except the loop setting or touch the red cross to clear the entry field and enter another Touch the back arrow to return to ramp loop selection screen 7 11 25 It is quite likely the finishing temperature of each loop will be different to the start temperature The next screen provides the user with the option ...

Страница 36: ...date See Save Profile The user may select to copy the profile to the clipboard so that it may be pasted into other cell profiles Touch the green tick to return to the home screen and start the cell profile running 7 11 27 Copy and Paste a Profile Once the copy button has been pressed this profile is copied to the internal clip board and can be pasted into other cells 7 11 28 Start Touch the Start ...

Страница 37: ...ation the Integrity 10 will turn off All field settings will be lost Part written data may be extracted manually from the SD card using an SD card reader All previously stored data written to the SD card will be safe 7 12 Naming and Storing a Profile The profile that has been set in Section 7 11 may be named In addition extra information about the nature and composite of the experiment may be adde...

Страница 38: ...u back to the previous screen 7 12 3 Profile Name From the screen below use the keyboard to name the profile The back button will take you back to the previous screen Use this button to remove an incorrect field entry This button is used to except the field entry By touching this button the field entry is accepted You are taken back to the Profile field selection screen 7 12 4 Owner From the field...

Страница 39: ...ld to select the keyboard from which to enter the recipe details 7 12 6 Composition From the field selection screen touch the Composition field to select the keyboard from which to enter composition details 7 12 7 Concentration From the field selection screen touch the Concentration field to select the keyboard from which to enter concentration details ...

Страница 40: ...acter G in upper or lower case Enters a numeric value of 5 Enters the Alpha character H in upper or lower case Enters a numeric value of 6 Enters the Alpha character I in upper or lower case Enters a numeric value of 7 Enters the Alpha character J in upper or lower case Enters a numeric value of 8 Enters the Alpha character K in upper or lower case Enters a numeric value of 9 Enters the Alpha char...

Страница 41: ...or lower case Enters a backslash symbol Enters the Alpha character U in upper or lower case or Upper case character selection Red indicates uppercase selected Deselect by touching red button Enters the Alpha character V in upper or lower case Enters the Alpha character A in upper or lower case Enters the Alpha character W in upper or lower case Enters the Alpha character B in upper or lower case E...

Страница 42: ... viewed at anytime regardless of what other functions the Integrity 10 is performing The only exception to this is when the screen is locked because of an external control source See section 7 18 Note A profile can t be stored once the associated experiment run has been completed It can be stored before and during the run of an experiment All of this may be undertaken while other cells are in use ...

Страница 43: ...ofiles 7 13 4 Touch the profile title to be viewed It will then become highlighted 7 13 5 Touch the green tick button to accept and view selected profile 7 13 6 You are now able to view the selected profile Scroll down using the scroll bars to view the profile settings as well as named field entries Touch the green tick button to return to the profile selection screen Touch the green back arrow bu...

Страница 44: ... 7 13 8 Touch the cell button that is to have the profile copied to Note Ensure the cell selected is one that is not in operation 7 13 9 Touch the profile selection button to bring up the profile entry field screen 7 13 10 Touch the paste button to populate all the fields with the copied profile settings Touch the green back arrow button to return to the home screen in order to select a different ...

Страница 45: ...er product software V3 5 1 8 and above Delete a stored profile 7 13 11 From the profile information display screen touch the Delete Profile button 7 13 12 Touch the green tick to delete the profile Touch the red cross to cancel the profile deletion ...

Страница 46: ...from both the profile selection or manual control modes All Experiments are filed using a cascade tree 7 14 1 When an experiment run is complete or the experiment has been stopped running a red ring is displayed around to the cell button To clear the ring and use the cell again the user must opt to save the experiment data or decline the save experiment option This done by touching the red highlig...

Страница 47: ...selection screen 7 14 5 Experiment Owner From the field selection screen touch the Owner field to select the keyboard from which to enter the owner details 7 14 6 Recipe From the field selection screen touch the Recipe field to select the keyboard from which to enter the recipe details 7 14 7 Composition From the field selection screen touch the Composition field to select the keyboard from which ...

Страница 48: ...tration field to select the keyboard from which to enter composition details Clearing cell without saving Data 7 14 9 Touch the red cell button as seen in the illustration below 7 14 10 You will now see the screen as illustrated Now press the Red cross button If the fields have entries written to them touching this button will clear out all field entries ...

Страница 49: ... If all the fields are blank then you are taken to the following cancel operation screen as illustrated 7 14 12 Touch the Green tick to accept data cancellation or the red cross to return to the field entry screen The Red cell ring will change back to Grey The cell is now ready for further use ...

Страница 50: ...on to this is when the screen is locked because of an external control source See section 7 18 7 15 1 From the home screen with or without any cells in use touch the View results Profiles button 7 15 2 The next screen asks the user if they wish to view stored profiles or view stored experiment data To view Stored Experiment data touch the tick button associated with the stored profile statement No...

Страница 51: ...ng on the expansion button From here you can view all the stored experiments for that day Touch the expansion again to close the cascade Select the experiment to be viewed by touching on it to highlight it Confirm selection by touching the green tick 7 15 5 Use the scroll bars to view all setting and title information associated with this experiment Note The back button will take you back to the h...

Страница 52: ... 7 15 6 Touch the green tick button to view the raw recorded data The screen will look like the illustration below View Data in Graphical Format 7 15 7 Touch the Graph button to view the data presented in a graphical format 7 15 8 To return to raw data format touch the green tick button ...

Страница 53: ...een see section 7 15 6 and 7 15 7 Insert a USB Flash Drive into the Master USB socket fount on the front of the Integrity unit see 7 1 After a 10 second or less time gap the USB down load button will appear on the screen 7 16 2 Touch the button and the raw data and a read my file containing the experiment parameter settings will automatically download 7 16 3 Once the down load is complete a down l...

Страница 54: ...ack constant information on the exact sample temperature The Integrity 10 is fed the temperature from the thermocouples via the Multitemp adjusts and monitors the contents temperature according to the temperature setting in both manual or profile control 7 17 1 Take the Multitemp unit ATS10001 Option accessory and connect it to the Integrity 10 unit Plug the D type connector into the RS232 socket ...

Страница 55: ...ocouple is place well inside the solution 7 17 7 Turn on the Integrity 10 unit and operated as previously described Again the home screen will be seen after the warm up Note the thermometer symbol indicating connection 7 17 8 Press the cell button to select the cell for operation 7 17 9 From the Manual or Profile control selection screen touch the check box to confirm the use of In contents contro...

Страница 56: ...plication on the host PC 7 18 3 With all the services connected to the Integrity turn on and wait for the home screen to appear 7 18 4 You have no control over the Integrity unit and no setting or adjustments can be made using the Integrity touch screen 7 18 5 A Lock icon appears in the cell buttons on the home screen to indicate which cells have been set running using external integrity software ...

Страница 57: ...electrical components and result in a reduced performance leading to shorted times between service requirements Stir speed range 350 1200 rpm Viscosity capacity Glycerine at 25 C Recommended stir bar AZS4235 10 Pack 12 x 4 5mm cylindrical AZS4206 10 Pack 10 x 6mm Oval Note Stir performance only guaranteed when using recommended stir bar Measurement Measured temperature range 40 to 160 C Temperatur...

Страница 58: ...t Excellent Resistance Excellent Resistance Acetic acid glac anh Major Effect Major Effect Excellent Resistance Excellent Resistance Acetic anhydride Major Effect Major Effect No data No data Aceto acetic ester Major Effect Major Effect No data No data Acetone Major Effect Major Effect Major Effect Major Effect Other Ketones Major Effect Major Effect No data No data Acetonitrile No data No data No...

Страница 59: ...ct Major Effect Major Effect Major Effect Caustic soda potash Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance Cellulose paint No data No data No data No data Chlorhydric aci 10 No data No data Excellent Resistance Excellent Resistance Chlorhydric aci 37 No data No data Excellent Resistance Major Effect Cholrates of Na K Ba Excellent Resistance Excellent Resistan...

Страница 60: ...t Major Effect Major Effect Major Effect Milk products Excellent Resistance Major Effect No data No data Moist air Excellent Resistance Excellent Resistance No data No data Molasses Excellent Resistance Major Effect No data No data Monoethanolamine Major Effect Major Effect No data No data Naptha Excellent Resistance Major Effect No data No data Napthalene Major Effect Major Effect No data No data...

Страница 61: ...istance Excellent Resistance No data No data Sulphites Excellent Resistance Major Effect No data No data Sulphonic acids No data No data No data No data Sulphur Excellent Resistance No data No data No data Sulphur dioxide dry Excellent Resistance Major Effect Excellent Resistance Major Effect Sulphur dioxide wet Excellent Resistance Major Effect Excellent Resistance Major Effect Sulphur dioxide 96...

Страница 62: ...Page 62 of 80 M8024 Issue 3 4 For use with master product software V3 5 1 8 and above Dimensions Unit Not to Scale Weight 9 5 Kg Location dimension For use in robotic stations Not to Scale ...

Страница 63: ...rs long Moulded IEC plug and Lead set supply cord H05 V V F Replace only with equivalent cable Mains cord and moulded IEC plug and lead set cable USA 3 core earthed ground 2 meters long Moulded IEC plug and Lead set supply cord SJT V W 1 105 Replace only with equivalent cable Lead set plug and fuse UK Only 13A BS1362 Dimensions PSU Not to Scale Weight 10 5 Kg 8 3 The Ingress Protection rating for ...

Страница 64: ...i e The Integrity 10 unit must not be connected when the PSU is being tested The Integrity 10 unit operates at low voltage 15V DC and must not be subjected to dielectric withstand Flash Hi Pot testing DC dielectric withstand flash Hi Pot testing shall only be undertaken by competent trained personnel using suitable test equipment environment DC test voltage should be no more than 1 414 times norma...

Страница 65: ...ntended as a guide Should spillage occur with a toxic or hazardous fluid then special precautions may be necessary Observe special precautions for handling contaminated substances see Section 9 3 9 3 Decontamination If the equipment has been exposed to toxic radiological or biological contamination the Responsible Body is responsible for carrying out appropriate decontamination If hazardous materi...

Страница 66: ... on 9 4 1 Turn off the Integrity Disconnect it from the Power Supply Unit Disconnect the chilled water supply 9 4 2 Release the drip tray by pulling forward on the release catch against the spring pressure 9 4 3 Lift the drip tray clear of the Integrity 10 unit by lifting the front end and then disengaging the back of the drip tray from under the rear handle plate lip 9 4 4 Using a Torx screwdrive...

Страница 67: ... Pull the top edge of the panel away from the unit and then lift side panel clear 9 4 6 Using a narrow bladed pair of pliers grip and lift out the two retention pins associated with the faulty cell Reserve the pins for re fitment 9 4 7 Lift the cell clear of the Integrity unit assembly and disconnect the IP65 connector plug from the socket by lifting the latch and pulling apart ...

Страница 68: ...l and reconnect the IP65 plug to the socket Insure the retention clip of the IP65 plug found on the loom is fully gripped over the latch of the cell 9 4 9 Push fit the cell back into position ensuring the copper heat exchanger lugs containing the O rings engage into the coolant feed return holes of the spine assembly ...

Страница 69: ...he side panel cover and engage the lugs as illustrated into the slots on the underside of the chassis 9 4 12 Slide the panel forward towards the front of the unit ensuring the V lugs sit over the chassis fastening brackets 9 4 13 Fasten the covers into position using the screws improved during the removal process using Torx screwdriver 9 4 14 Refit the drip tray cover ...

Страница 70: ...il all failed cells have been replaced and named 9 4 15 Having just replaced the cell as detailed 9 4 1 to 9 4 14 turn on the coolant water supply and check for any signed of leakage 9 4 16 Reconnect to the Power Supply Unit and turn on see 7 4 The Integrity will go through the power up routine of displaying the Splash screen When the selection screen appears confirm the correct cell has been repl...

Страница 71: ...drive then copy the received file to your USB flash drive The folder will be titled Integrity 10 Copy the folder and all sub folders and files contained within to your flash drive using your PC 9 5 2 Turn off your Integrity unit via the I O button on the Power Supply see paragraph 7 5 9 5 3 Insert your flash drive into the Master USB socket found on the front of the Integrity unit 9 5 4 Turn on yo...

Страница 72: ...er over temperature With cell position indicated The cell will have to be replaced See Section 9 4 for cell replacement This Warning shows a faulty condition with the cell number 2 One or more cells may display this message at the same time however if all the cells are affected another warning message will be displayed See 9 6 2 Possible cause is blocked flow chamber in the cell heat exchanger Che...

Страница 73: ...other piece of equipment returning chilled water at a temperature above 35 C Low coolant flow rate which is insufficient to remove the heat from the heat exchangers less than 2 5 L per minute Note The chilled water flow rate must be continuous at minimum rate of 2 5 litres min at 5 C The coolant system should be able to dissipate heat energy at 1100W with a coolant temperature of 5 C Running all 1...

Страница 74: ...ault condition This illustration screen shot shows a cell failure with cell position number 2 The cell will have to be replaced See Section 9 4 for cell replacement Possible causes are as follows PT100 failed open circuit Thermistor failure Heater or Thermal fuse failed Thermo electric peltia device failure To return to the home screen and view the performance of other operational cells touch the ...

Страница 75: ... Power Supply Unit Contact the manufacturer as detailed in Section 10 Customer support Turn off the Integrity 10 as per section 7 4 and disconnect from the mains electricity supply 9 6 7 Error Message Probe Error When the warning symbol appears in a single cell button and the cell button turns red touch the cell button to display the fault condition If an external probe is being used and it is eit...

Страница 76: ...h the back button 10 CUSTOMER SUPPORT For help and support in using this product please contact Customer Services at the following address Bibby Scientific Limited Beacon Road Stone Staffordshire ST15 0SA Great Britain Tel 44 0 1785 812121 Fax 44 0 1785 810405 General enquiries info bibby scientific com Order enquiries sales bibby scientific com Technical support electrothermalhelp bibby scientifi...

Страница 77: ... card Programmed Please quote your integrity unit serial number when ordering 1 AZS4323 Power cable assembly 1 AZS4323 1 Power cable assembly USA Please state destination when ordering 1 Accessories Order Number Description Quantity ATS10001 Multitemp 10 External thermometer module 1 ATS10002 Infer Red Probe Multi box kit 1 ATS10011 Test Tubes 24mm OD threaded round bottomed 12 ATS10016 Test Tube ...

Страница 78: ... 1 8 and above Recommended Recirculating Chillers NESLAB ThermoFlex 1400 for light use where no more than 3 cell are required to perform below 15 C at any given time NESLAB ThermoFlex 2500 for general use Please consult Customer Service See paragraph 10 for further details ...

Страница 79: ...elow A Blood body fluids Pathological specimens YES NO Provide details if YES B Biodegradable material that could become a hazard YES NO Provide details if YES C Other biohazard YES NO Provide details if YES D Chemical or substances hazardous to health YES NO Provide details if YES E Radioactive substances State name s and quantities of isotopes and checks made for residual activity YES NO Provide...

Страница 80: ... sales bibby scientific com Technical support electrothermalhelp bibby scientific com www electrothermal com For the America s and Canada contact Techne Incorporated 3 Terri Lane Suite 10 Burlington NJ 08016 USA Toll free 800 225 9243Tel 609 589 2560 Fax 609 589 2571 Email labproducts techneusa com Http www techneusa com Part of the Bibby Scientific group of companies STEM is a trade name owned by...

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