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Nanopure™ Analytical 2-1

Thermo Scientific

Section 2

Introduction

Congratulations on your purchase of a Thermo Scientific Nanopure

Analytical ultrapure water system. This water purification system is

designed to provide high resistivity, reagent grade water that exceeds

ASTM Type I, ISO 3696 and CLSI-CLRW Type I standards. It uses a

four-stage deionization process combined with a 0.2 micron filter to polish

suitable feed water (distilled, deionized, or reverse osmosis) of up to 18.2

megohm-cm. Water resistivity is continuously monitored by a resistivity

cell and displayed on a digital display.

The electronics can be verified and calibrated utilizing a N.I.S.T. Traceable

Calibration module. See accessory ordering information.

Please read the instructions carefully to ensure that you receive maximum

benefit from the Nanopure Analytical. Also, please fill out and return the

enclosed warranty registration card as it will help us assure you of proper

warranty coverage.

Do not use this product for anything other than its intended purpose.

General Usage

Содержание 1367

Страница 1: ...e Analytical Ultrapure Water System Series 1367 Operating Manual and Parts List LT1367X1 Rev 0 _________________________________________________________________________________ Part of Thermo Fisher Scientific ...

Страница 2: ...MANUAL NUMBER LT1367X1 7007143 0 6 9 10 Transfer to Marietta was LT1367X1 3 4 10 ccs REV ECR ECN DATE DESCRIPTION By Preface Nanopure Analytical i Models covered in this manual Model number Voltage D11901 7143 100V 240V ...

Страница 3: ...stments and maintenance must be performed by qualified service personnel s Material in this manual is for information purposes only The contents and the product it describes are subject to change without notice Thermo Fisher Scientific makes no representations or warranties with respect to this manual In no event shall Thermo be held liable for any damages direct or incidental arising out of or re...

Страница 4: ... equipment that has been put on the market after 13 August 2005 This product is required to comply with the European Union s Waste Electrical Electronic Equipment WEEE Directive 2002 96 EC It is marked with the WEEE symbol Thermo Fisher Scientific has contracted with one or more recycling disposal companies in each EU Member State European Country and this product should be disposed of or recycled...

Страница 5: ...nt parts or provide you with on site service We can also provide you with a quotation on our Extended Warranty for your Thermo Scientific products Whatever Thermo Scientific products you need or use we will be happy to discuss your applications If you are experiencing technical problems working together we will help you locate the problem and chances are correct it yourself over the telephone with...

Страница 6: ...mote Location 5 3 Water Connections 5 5 Atmospheric Drain Connection 5 6 Feed Water Connection 5 6 Tubing Installation 5 6 Electrical Connections 5 7 Controls 6 1 Control Panel 6 1 Main Power Switch 6 1 Switches 6 2 Initial Operation 7 1 Cartridge Pack Installation 7 1 Initial Rinse 7 2 System Cleaning Procedure 7 3 Normal Operation 8 1 Automatic Dispensing 8 2 Dispensing Water 8 2 Section 1 Secti...

Страница 7: ...er Float or Pressure Switch 10 1 Dispense Overflow Cutoff Float 10 2 Electronic Calibration w Optional Cal Mod 10 3 Remote Volumetric Dispenser 10 4 Computer Printer Set Up 11 1 Connect Communicate through RS 232 Port 11 1 Hyperterminal 11 1 Procomm 11 2 Connecting and Starting the Printer 11 3 Maintenance and Servicing 12 1 Cell Cleaning 12 1 System Cleaning 12 2 Cartridge Pack Replacement 12 4 S...

Страница 8: ...ation technology employs one or more of the following chemicals electrical devices mercury vapor lamps steam and heated vessels Care should be taken when installing operating or servicing Thermo Scientific products The specific safety notes pertinent to this product are listed below Warnings To avoid electrical shock always 1 Use a properly grounded electrical outlet of correct voltage and current...

Страница 9: ...mpliance with instructions in this manual Failure to comply with the above could result in explosion and personal injury 3 Avoid splashing cleaning solutions on clothing or skin 4 Ensure all piping connections are tight to avoid chemical leakage 5 Ensure adequate ventilation 6 Carefully follow manufacturer s safety instructions on labels of chemical containers and material safety data sheets 7 Dep...

Страница 10: ...ater distilled deionized or reverse osmosis of up to 18 2 megohm cm Water resistivity is continuously monitored by a resistivity cell and displayed on a digital display The electronics can be verified and calibrated utilizing a N I S T Traceable Calibration module See accessory ordering information Please read the instructions carefully to ensure that you receive maximum benefit from the Nanopure ...

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Страница 12: ...e front door Feed Water Requirements Types RO DI distilled TOC Less than 1 0 ppm Turbidity 1 0 N T U maximum Pressure Range Gravity feed to 20 psig 1 38bar 1 41 kg cm2 max Temperature Range 4 C 40 C 40 104 F TDS CaCO3 70 ppm Silica 1 ppm Silt 5 SDI Product Water Water Quality Resistivity 18 2 mΩ cm Pyrogen TOC 5 10 ppb Bacteria 0 01 CFU ml Flow Rate Up to 2 L min maximum at minimum inlet feed wate...

Страница 13: ... C to 65 C 10 to 85 relative humidity RH Declaration of Conformity We hereby declare under our sole responsibility that this product conforms with the technical requirements of the following standards EMC EN 61000 3 2 Limits for Harmonic Current Emissions EN 61000 3 3 Limits for Voltage Fluctuations and Flicker EN 61326 1 Electrical Equipment for Measurement Control and Laboratory Use Part I Gener...

Страница 14: ...t below are removed from the packaging materials before discarding Put the Nanopure Analytical on a bench Cleaning Cartridge CMX25 Wall Bracket Unit BC1190X12 Wall Bracket Remote Display BC1190X10 Accessory Parts Bag includes Feed Water Tube 3 8 O D TU1119X7 Drain Tube 14 O D TU1190X12 Display Cable WHX20 Blank Display DL1190X18 Plug Adapter CEX42 Power Cords Also required for installation Custome...

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Страница 16: ... and construction as well as fastener type must be considered when mounting this unit The mounting surface and fasteners selected must be capable of supporting a minimum of 150 lbs 68kg Inadequate support and or fasteners may result in damage to mounting surface and or equipment If you are unsure of mounting surface composition condition and construction or correct fasteners consult your building ...

Страница 17: ...ll in a convenient location that is accessible to water an atmospherically vented drain and electricity 1 Locate the wall bracket packed separately from the unit 2 Using the wall bracket as a template locate and drill the mounting holes in the wall A minimum of four customer supplied fasteners will be required two on the top and two on the bottom 3 Attach the wall bracket to the wall using the cus...

Страница 18: ...n be removed from the unit and mounted at a convenient location within 10 ft 3 1 m of the unit To remove the control panel from the unit 1 Turn the unit OFF and disconnect it from the power supply 2 Slide the control panel upward about 1 4 64 cm to 3 8 95 cm just enough to clear connector on top cover pull forward and remove The control panel fits tightly in the unit so it may be difficult to remo...

Страница 19: ... pin connector on the back top right of the unit and the other end to the connector on the bottom of the control panel 7 Tighten the cable screws on each end to secure the cable to the unit and control panel 8 The control panel may now be mounted on the wall Caution Repeated removal and replacement of the control panel from the top cover may eventually cause it to become damaged Note A bracket is ...

Страница 20: ...atmospheric drain connection until it bottoms out s Nanopure Analytical 5 5 Thermo Scientific Section 5 Installation Water Connections Remote 1 Remote 2 Feed Water Inlet Atmospheric Drain Accudispense control cable Overflow Float Connection Figure 5 2 Water Connections Left Side of Unit Figure 5 3 Water Connections Right Side of Unit ...

Страница 21: ...O D tubing that is approximately 6 ft 1 9 m long The atmospheric drain fitting is located on the lower left side of the Nanopure Analytical 2 Route the other end of the drain water tubing to an atmospherically vented drain and make a connection Ensure there are no kinks in the tubing and that it proceeds on a downward plane Proceed to Initial Operation To make tubing connections refer to Figures 5...

Страница 22: ...odule Before connecting the power cord to the power module install the proper fuses in the fuse holder Refer to Figure 5 6 Nanopure Analytical 5 7 Thermo Scientific Section 5 Installation Electrical Connections COLLET TUBING TYPICAL FITTING Figure 5 4 Mark Tubing Insertion Length Figure 5 5 Push Collet Back to Remove Fuse Holder Power Switch Power Cord Figure 5 6 Electrical Connections ...

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Страница 24: ...nsity brightness of the display may be adjusted according to user preference See Adjusting Display Brightness in User Settings of this manual A single LED located on the top of the control panel will illuminate to inform you of the system status as follows LED is not illuminated System is OFF or in Idle mode Solid Green LED System is recirculating and operating normally Blinking Green LED System i...

Страница 25: ...read Standby during periods of inac tivity and Recirculating and the time remaining during the 10 minute recirculation DISPENSE allows you automatically deliver water from the unit Please refer to Automatic Dispensing in the User Settings section of this manual for information UP and DOWN arrows allow you to scroll between menu options items and values BACK allows you to return to the previous men...

Страница 26: ...so that it mates with the unit manifold 4 Lower unit manifold until it is flush with the top of the cartridge pack Nanopure Analytical 7 1 Thermo Scientific Part Application Diamond Kit Organic Free R O Distilled Feed D50280 Ultra Low Organics Type 1 Water Reverse Osmosis or Distilled Water Feed Diamond Kit Organic Free Deionized Feed D50281 Ultra Low Organics Type 1 Water Deionized Water Feed DIa...

Страница 27: ...ect the appropriate power cord remove and install the two fuses into the fuse draw in the power entry module U K customers use cord CRX100 and fuses for 240V installation Warning Use a properly grounded electrical outlet of correct voltage and current handling capacity 5 Connect attach to proper electrical outlet and the unit 6 Turn the unit on by turning the main power switch to the I ON position...

Страница 28: ... hours to complete Clean your Nanopure as follows 1 If you have installed an Accudispense volumetric remote dispenser place it in Manual Mode From the Idle display press the UP or DOWN arrow until display reads Clean Unit 2 Press ENTER 3 Unit display will ask if you have Disconnected Inlet Water NO 4 Disconnect feed water supply at the quick disconnect inlet valve on left side of unit 5 Press the ...

Страница 29: ...in this manual Failure to comply could result in explosion and personal injury s Note After cleaning is complete the cleaning timer will need to be reset refer to Resetting the Cleaning Timer for another six month timing sequence s 13 Press the UP or DOWN arrow to select YES and press ENTER Display will now read Unit Cleaning 14 Unit may now be left unattended until display reads Cleaning Complete...

Страница 30: ...lications where low TOC water is required a rinse of 15 20 liters through the cartridges and 0 2 micron filter may be necessary s Caution Never dispense water without first installing hose barb provided in parts bag or final filter supplied with cartridge pack s Nanopure Analytical 7 5 Thermo Scientific Section 7 Initial Operation System Cleaning Procedure cont 0 2 Micron Filter Figure 7 3 Install...

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Страница 32: ...al start up the purity meter may display MΩ cm or uS cm This is caused by air in the cell and should be replaced by a resistivity reading almost immediately If the dots aren t replaced by a value after one minute refer to the Troubleshooting section of this manual s 6 Allow the water s resistivity to rise to the desired purity before drawing off water 7 The system should be left On or in Standby d...

Страница 33: ...howing purity 1 Place a container under the dispenser 2 Press DISPENSE Water will start dispensing immediately Display will read xx MΩ cm xx Liters Remaining or xx MΩ cm xx Seconds Remaining or AUTO DISPENSE OFF depending on which dispensing method was last chosen in the auto dispense menu Note Press any switch except ENTER to stop dispensing Display will read Auto Dispense Interrupted by User s N...

Страница 34: ...6 Press the UP or DOWN arrow until the desired value 100 75 50 or 25 is displayed 7 Press ENTER 8 Press BACK until you return to the Idle display 1 From the Idle mode when display reads Nanopure Idle xx xx xx xx xx xx press the BACK switch until the display reads LANGUAGE 2 The currently selected language is displayed on line 2 of the display 3 Press the UP or DOWN arrow to select the language des...

Страница 35: ... DOWN arrow to choose Yes then press ENTER 6 Press the UP or DOWN arrow until you reach the desired month Press ENTER 7 Press the UP or DOWN arrow until you reach the desired day Press ENTER 8 Press the UP or DOWN arrow until you reach the desired year Press ENTER 9 When prompted with Set Time press the UP or DOWN arrow to choose Yes then press ENTER This is to set the time of day 10 Press the UP ...

Страница 36: ...rom the Idle mode when the display reads Nanopure Idle xx xx xx xx xx xx press the UP or DOWN arrow until the display reads Advanced Menu 7 Press ENTER 8 Proceed through the options by pressing ENTER until Set Cell Constant is displayed 9 Press the UP or DOWN arrow to select Yes 10 Press ENTER 11 Note that the digits are entered from left to right 12 Press the UP or DOWN arrow to change the blinki...

Страница 37: ...fer to Auto Standby section to have the unit automatically enter Standby Mode each day at a predetermined time chosen by the user s Note If you have installed an Accudispense volumetric remote dispenser its Purity Above Setpoint LED will slowly blink when the water system is in Standby Mode s The Nanopure Analytical electronics include a user programmable set point which alerts you when water qual...

Страница 38: ...otal fluid volume entering the Nanopure Analytical Point of drawoff accuracy will be compromised if you are dispensing water volumetrically while simultaneously drawing water manually through the remote dispenser accessory s Note Once Volumetric or Timed Dispensing values are set they will remain in memory until changed by the user To turn the dispense method OFF select OFF in the Dispense Method ...

Страница 39: ... 4 Press ENTER Display will read Time Setting xx Minutes 5 Press the UP or DOWN arrows to set the desired time value Press ENTER UP arrow 1 up to 5 min then increments by 5 minutes DOWN arrow Decrement by 1 minute Maximum 40 minutes Minimum 1 minute 1 From the normal recirculating mode when the display is showing purity press the UP or DOWN arrow until the display reads System Flush Press ENTER 2 ...

Страница 40: ...p or DOWN arrow until the display reads Temperature Compensation Press ENTER 2 Press the UP or DOWN arrow to select OFF or ON Press ENTER 3 Press BACK to return to the normal recirculating mode Auto Standby is factory set to NO This option allows for a convenient method for the user to ensure that the Nanopure Analytical unit will be placed in Standby at a predetermined time each day This is espec...

Страница 41: ... is factory set to NO This option will lock out any type of automatic dispense out of the unit Accudispense accessory D13661 will still operate normally This will prevent accidental dispensing from the unit if it is located under a counter or similar area such that the unit dispenser is not in sight of the user but the display is i e remote mounted display Note When UNIT UNDER COUNTER is set to YE...

Страница 42: ... 1 Disconnect the unit from the electrical power 2 If using the D8964 float switch follow the installation instructions included with the float switch for installation into a tank 3 If using the D2706 low pressure switch install the PVC tee supplied with D2706 in the incoming water line Screw the switch into the top of the tee then connect the inlet tubing of the Nanopure Analytical into the remai...

Страница 43: ...overflows if the entered stored volume of a previous container has not been changed and is set for a volume greater than the carboy being filled Finally the accessory can be useful for automatic time dispenses as it is usually difficult to ensure the set time will equal a specific volume of water 1 Prior to initialing an automatic dispense time or volumetric plug AY1367X1 into connector on back ri...

Страница 44: ... a calibration of the Nanopure purity sensing electronics traceable to N I S T standards 1 Disconnect power cord from the unit 2 Unlatch and open the right door Remove the 2 screws and remove the cover plate over the PC boards 3 Locate the outlet cell connection on the circuit board and remove the outlet cell connection at J2 4 Connect the N I S T calibration module to the connection point J2 To O...

Страница 45: ...ke up to two minutes to complete s 11 Press BACK to return to the Idle mode 12 Turn the main power switch to the OFF O position Unplug the unit 13 Remove the calibration module and reconnect the cell 14 Reattach the cover plate and close and latch the door 15 Reconnect the power cord The calibration procedure is complete Refer to the Operating Instructions for your manual or Accudispense volumetri...

Страница 46: ...for NO 5 Press ENTER 6 Now during the normal Recirculation mode date time purity and temperature readings will be sent to the computer once per minute 7 Run your Microsoft Windows program Open Hyperterminal located in the accessories directory give your setting a name and choose a symbol 8 In the Connect Using box select direct to COM2 or COM1 as port depending on your computer and click OK 9 Usin...

Страница 47: ... DOWN arrow until the display reads Advanced Menu 3 Press ENTER 4 From the Printer Attached display Press the Up or DOWN arrow for NO 5 Press ENTER 6 The unit will now during the normal Recirculation mode send a purity and temperature reading to the computer once per minute 7 Open DOS window and change directory to procomm directory 8 Open procomm executable 9 Press ALT F10 for configuration scree...

Страница 48: ...pson printer Plug the printer power cord into an electrical outlet 3 Turn the Nanopure ON 4 Turn the printer ON 5 From the Idle display press the UP or DOWN arrow until display reads Advanced Menu 6 Press ENTER 7 From the Printer Attached display press the Up or DOWN arrow for YES 8 Press ENTER 9 Press BACK twice to return to the Idle mode 10 During normal Recirculation mode a purity and temperatu...

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Страница 50: ...and depressurize See System Depressurization section 2 Turn unit OFF Open right side door and remove PC board cover 3 Disconnect cable from J2 and snip plastic cable tie located on the inside top of unit 4 Unscrew and remove the cell by turning the gray bushing counterclockwise Carefully remove O ring to clean the cell 5 Wash the cell in a mild detergent solution or a 10 inorganic acid solution fo...

Страница 51: ...kage Ensure adequate ventilation Carefully follow manufacturer s safety instructions and material safety data sheets This device to be used with water feeds only Cleaning agents must be used in compliance with instructions in this manual Failure to comply could result in explosion and personal injury s It is best to perform cleaning procedures early in the afternoon After cleaning is complete appr...

Страница 52: ...tem 10 Replace luer cap on injection port Close door 11 Press the UP or DOWN arrow to select YES and then press ENTER Display will now read Reconnected Water NO 12 Attach feed water supply removed in Step 4 13 Press the UP or DOWN arrow to select YES and press ENTER Display will now read Unit Cleaning 14 Unit may now be left unattended until the display reads Cleaning Complete Press ENTER 15 After...

Страница 53: ...nd replace your cartridge pack is dependent on your feed water s characteristics your purity requirements and your usage Clean your Nanopure Analytical and replace the cartridge pack when the product water purity drops below acceptable levels of resistivity when organic levels become too high or if a new 0 2 micron filter clogs rapidly after installation even though the cartridge pack was thorough...

Страница 54: ...ctions in the Initial Operation section Replace the 0 2 micron final filter whenever any of the following conditions occur the product water flow rate is reduced or bacteria break through Caution Do not overtighten the 0 2 micron filter or use excessive force in seating it Filter can be damaged by overtightening or excessive force s Note If a newly installed 0 2 micron filter clogs rapidly after i...

Страница 55: ...ower supply by removing the power cord directly below the main power switch on right side of unit Locate the fuse drawer above the power cord receptacle 2 Pull out the fuse drawer located in the power entry module 3 Remove old fuses and replace with fuses of the same type and rating See Replacement Parts 4 Replace fuse drawer 5 Reattach the power cord 6 Operate normally Warning Replace fuses with ...

Страница 56: ...in reservoir feed water line pressure switch or jumper plug not connected to pump interlock Connect the pump protector jumper plug or pressure switch cord to the receptacle located on the upper left hand section of the Nanopure Insufficient feed water pressure or volume to satisfy the Nanopure Open feed water line shut off connect feed water line to Nanopure and ensure sufficient pressure or suffi...

Страница 57: ...orm the calibration function WITHOUT the calibration module as if you had it answer YES to prompt The display will read Calibration failed but this will clear any incorrect offset to zero Display reads Overpressure Error 0 2 micron filter clogged Replace final filter as indicated in 0 2 Micron Filter Replacement Display reads Meter Board Problem PC board communication error Turn the Nanopure OFF I...

Страница 58: ...late a replacement interval compatible with your usage pattern The replacement of consumable parts is discussed in the Maintenance and Servicing section to assist you in accomplishing your own service Consumables may be ordered separately and in some cases as an expendables kit Check with your Technical Services representative for additional information on the expendables kit Description Catalog N...

Страница 59: ... the General Maintenance Parts and Safety Stock sections Description Catalog No Recommended Quantity Quick Disconnect Inlet CUX11 1 Quick Disconnect Insert 3 8 tube CUX9 1 Cartridge Pack O Rings GSX68 4 Description Catalog No Recommended Quantity Display SW1190X2 1 External Display Cable remote display use WHX20 1 Main PC Board PC1190X4 Recirculation Pump Motor PU1190X1 1 Pressure Regulator PM1190...

Страница 60: ...eck first with your dealer If the dealer cannot process your request then contact our Technical Services Department Prior to returning any materials contact our Technical Services Department for a Return Materials Authorization number RMA Material returned without an RMA number will be refused Ordering Procedures Description Catalog No N I S T Calibration Module E896X5 Low Pressure Switch D2706 Fl...

Страница 61: ...arnstead Thermolyne Vx xx Style English Advanced menu Diagnostics menu Air Purge Purity display up or down keys pressed Change Units System flush Auto Dispense Menu Temperature Compensation dispense key pressed enter key pressed C back key pressed force print line Arrow Legend Keypress Options Automatic Entry Menu Wrap around power switch turned on Depressurize Optional Printer Remote Gun Date For...

Страница 62: ...H2 AC POWER HARNESS WH3 CAL BOARD HARNESS WH4 PRESSURE SW HARNESS WH5 METER BOARD HARNESS WH6 DISPLAY HARNESS WH7 GROUND WIRE WM1 CAL METER HARNESS WH9 LAMP HARNESS WH8 S2 MEMBRANE SWITCH E2 NIST MODULE TIMEKEEPER SC1 WM896X2 WM1190X2 D11901 E896X4 CE896X2 CEX183 SW1190X1 TNX116 PU1190X1 PC896X2 PC1190X2 E896X5 PC1190X4 ME1190X1 WH1190X1 WH1190X6 WH1190X5 WH1190X4 WH1190X3 WH1190X2 SCX223 RY1190X3...

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Страница 64: ...Thermo Scientific 401 Millcreek Road Marietta Ohio 45750 United States www thermofisher com ...

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