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ThermoFisher Scientific Ozone Primary Standard 49iQPS, Instruction Manual

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ThermoFisher Scientific Ozone Primary Standard 49iQPS Instruction Manual Download Page 32

Operation 

Calibration 

3-8

     49iQPS Instruction Manual 

Thermo Scientific 

 

The Calibration screen is used to make minor compensations to the O

3

 

concentration when the 49iQPS is being precisely matched to a NIST 
traceable O

3

 calibrator. 

Home Screen>Calibration 

 

The Calibration screen contains the following information: 

●

 

Adjust Background: 

Allows the user to adjust the zero background. 

●

 

Adjust Span Coefficient: 

Allows the user to adjust the span coefficient. 

●

 

Reset Bkg to 0.000 and Span Coef to 1.000: 

Resets all backgrounds and 

coefficients. 

●

 

Custom O

3

 Levels: 

User sets concentration for O

3

 levels. 

●

 

Calibration History: 

Lists all calibrations performed and calibration 

checks. 

 

Calibration

Summary of Contents for Ozone Primary Standard 49iQPS

Page 1: ...49iQPS Instruction Manual Ozone Primary Standard 117434 00 1Apr2020...

Page 2: ......

Page 3: ...y 3 1 Main Menus and Keypads 3 4 Numeric Keypad 3 5 Alphanumeric Keypad 3 6 Calibration 3 8 Adjust Background 3 9 Adjust Span Coefficient 3 10 Reset Bkg to 0 000 and Span Coef to 1 000 3 11 Custom O3...

Page 4: ...ocol Selection 3 78 Instrument Settings 3 79 Display Setup 3 80 Alarm Setpoints 3 81 Clock 3 84 Time Zone 3 88 Advanced Instrument Settings 3 91 Configuration 3 93 Security Access Levels 3 94 Change S...

Page 5: ...ment 6 19 Capillary Cleaning and or Replacement 6 22 Capillary O Ring Replacement 6 24 Power Supply Replacement 6 24 Step POL Board Replacement 6 26 49iQPS Photometer DMC 6 29 Photometer Lamp Replacem...

Page 6: ...es 8 1 Communication Board 8 2 RS 232 RS 485 Port 8 2 RS 485 External Accessory Port 8 3 Analog I O Board 8 4 Analog Voltage Inputs 8 4 Analog Voltage Outputs 8 5 Analog Output Calibration 8 6 Analog...

Page 7: ...Contents Thermo Scientific 49iQPS Instruction Manual vii GNU Lesser General Public License C 1 GNU Lesser General Public License C 1 Appendix C...

Page 8: ......

Page 9: ...Control DMC module design simplifies serviceability Each DMC module contains its own microprocessor control enabling functional performance validation at the module level Built in predictive diagnosti...

Page 10: ...ific experience to simplify daily operations Custom designed ePort software allows remote access to the instrument with a PC The ePort control mirrors the same GUI look and feel as the instrument touc...

Page 11: ...ure regulator to the reference solenoid valve to become the reference gas Io The second zero air stream flows through a pressure regulator ozonator and manifold to the sample solenoid valve to become...

Page 12: ...Introduction Principle of Operation 1 4 49iQPS Instruction Manual Thermo Scientific Figure 1 2 49iQPS Flow Schematic...

Page 13: ...D 425 45 mm W x 221 48 mm H Weight 34 53 lbs Analog I O 4 Isolated Voltage Inputs 0 10 V 6 Isolated Analog Voltages Outputs with 4 selectable ranges 6 Isolated Analog Current Outputs with 2 selectable...

Page 14: ...Introduction Dimensions 1 6 49iQPS Instruction Manual Thermo Scientific Figure 1 3 Bench Mount Assembly dimensions in inches mm Dimensions...

Page 15: ...Introduction Dimensions Thermo Scientific 49iQPS Instruction Manual 1 7 Figure 1 4 Rack Mount Assembly dimensions in inches mm...

Page 16: ...Introduction Dimensions 1 8 49iQPS Instruction Manual Thermo Scientific Figure 1 5 Rack Mount Requirements Figure 1 6 Rack Requirements Part 2...

Page 17: ...r immediately and hold for inspection The carrier is responsible for any damage incurred during shipment Use the following procedure to unpack and inspect the instrument 1 Remove the instrument from t...

Page 18: ...the cover Equipment required Phillips screwdriver 2 1 Unfasten the four 8 32 screws securing the cover shipping screws 2 Press in both latches located on top cover and hold while pulling up to remove...

Page 19: ...rument can be installed in the following configurations Bench Mount Rack Mount Positioned on bench includes installing feet See Figure 2 2 Equipment required Slot drive 5 16 inch 1 Fasten feet in posi...

Page 20: ...red Phillips drive 2 1 Start by gripping from the top corners of the front panel and pull outwards Figure 2 3 Removing the Front Panel 2 Unfasten the four 8 32 x 3 16 inch pan head screws 3 Slide ears...

Page 21: ...Installation and Setup Mounting Options Thermo Scientific 49iQPS Instruction Manual 2 5 Figure 2 4 Installing Ears and Handles...

Page 22: ...ilter on page 8 17 2 Connect the EXHAUST bulkhead to a suitable vent The exhaust line should be 1 4 inch OD with a minimum ID of 1 8 inch The length of the exhaust line should be as short as possible...

Page 23: ...Installation and Setup Setup Procedure Thermo Scientific 49iQPS Instruction Manual 2 7 Figure 2 5 49iQPS Rear Panel Figure 2 6 Atmospheric Dump Bypass Plumbing...

Page 24: ...t the instrument is warming up the mode warm up is displayed on the gas mode button in the title bar and the concentration calculation is turned off To disable warm up go to Settings Configuration 3 S...

Page 25: ...ton The User Interface located in the middle is where the Home Screen and all other screens are accessed The Home Screen has three Main Menu buttons located on the left side which include Calibration...

Page 26: ...al time status and alarms also predictive diagnostics and maintenance history Contains controls for operating the instrument communications and sets instrument options Concentration When in single mod...

Page 27: ...Operation Instrument Display Thermo Scientific 49iQPS Instruction Manual 3 3 Thermo Scientific Information button Shows contact information...

Page 28: ...ion Instrument Settings Display Setup Alarm Setpoints Language Clock Pump Enabled Advanced Instrument Settings Reboot Instrument Communications Configuration Security Access Levels Adjust Span Coeffic...

Page 29: ...ch as for flow rates temperatures or pressures the keypad screen will automatically display Initially the box above the keypad will display the current value Enter a new value using the keypad and the...

Page 30: ...tomatically display Initially the box above the keypad will display the current value Enter a new value using the keypad and then select the Enter button to set the new value or press the Cancel butto...

Page 31: ...Operation Instrument Display Thermo Scientific 49iQPS Instruction Manual 3 7...

Page 32: ...creen Calibration The Calibration screen contains the following information Adjust Background Allows the user to adjust the zero background Adjust Span Coefficient Allows the user to adjust the span c...

Page 33: ...ckground button The second button called Adjusted Concentration shows what the new O3 concentration would be based on the changed zero background Press the Calibrate button to save the adjusted zero b...

Page 34: ...Concentration button The second button called Adjusted Concentration shows what the new concentration would be based on the adjusted span coefficient Press the Calibrate button to save the adjusted s...

Page 35: ...reset the calibration configuration to factory defaults Home Screen Calibration Reset Bkg to 0 000 and Span Coef to 1 000 The Reset Bkg to 0 000 and Span Coef to 1 000 screen contains the following i...

Page 36: ...in no ozone production The range of percentages however are not linear Use the and buttons to move up and down and the and buttons to move left and right Home Screen Calibration Custom O3 Levels The...

Page 37: ...Calibration History Note Pressing the Calibration History button responds with Retrieving calibration log data it may take a few seconds The Calibration History screen contains the following informati...

Page 38: ...ollowing information View Data Log Last Hour User views last hour of historical data Table shows most recent data on top View Data Log Last 24 Hours User views 24 hour of historical data Table shows m...

Page 39: ...up and down and the and buttons to move left and right Home Screen Data View Data Log Last Hour Note Pressing the View Data Log Last Hour responds with Retrieving user log data it may take a few secon...

Page 40: ...nd down and the and buttons to move left and right Home Screen Data View Data Log Last 24 Hours Note Pressing the View Data Log Last 24 Hours responds with Retrieving user log data it may take a few s...

Page 41: ...Time Home Screen Data View Data Log User Defined Time Save Data Logging Start Time The View Data Log User Defined Time screen contains the following information Date Sets date of data logging start t...

Page 42: ...ation Date Sets date of data logging end time Time Sets time of data logging end time Save Data Logging End Time Pressing the Save Data Logging End Time button saves the end time and follows directly...

Page 43: ...p parameters for data logging and streaming data Home Screen Data Advanced Data Setup The Advanced Data Setup screen contains the following information Data Logging Setup User selects the parameters f...

Page 44: ...ften data is collected by setting the duration between logged data Data Treatment Toggles between Average Current Minimum and Maximum When set to average the average value during the period will be re...

Page 45: ...other but contain the same variable selections The list is based on the instrument s configuration Use the and buttons to scroll through the variables Select the variables to log by pressing the corr...

Page 46: ...ng Data Setup screen contains the following information Select Streaming Variables User selects which variables to stream Period Sets the time between streamed data Show Labels Toggles enabled disable...

Page 47: ...other but contain the same variable selections The list is based on the instrument s configuration Use the and buttons to scroll through the variables Select the variables to log by pressing the corr...

Page 48: ...lowing information Health Check View instrument status and alarms predictive diagnostics preventive maintenance alerts maintenance history email health check report files and contact Thermo Fisher Sci...

Page 49: ...rity passwords USB Drive User can update instrument firmware download data and change USB password Programmed Events Allows the user to set up to 20 different programs each with up to 31 events User C...

Page 50: ...s the following information Status and Alarms Allows the user to view the status and alarm menus Menus are broken down according to modules where the user can view instrument readings setpoints and al...

Page 51: ...e This symbol denotes there is an active alarm in the module Home Screen Settings Health Check Status and Alarms Home Screen Settings Health Check Status and Alarms More The Status and Alarms menu con...

Page 52: ...Displays peripherals support alarms and faults Valve and Pump Resets User can reset valve and pump power Analog I O Displays analog input output alarms and faults Digital I O Displays digital input ou...

Page 53: ...Across Photometer This column lists items associated with the photometer Value Displays the current value for each item Low Alarm Displays low alarm status for each item High Alarm Displays high alar...

Page 54: ...Displays OK Fail for lamp connection Lamp Short Displays OK Fail for lamp short Lamp Heater Current Displays the current lamp heater current Bench Temp Sensor Short Displays OK Fail for bench tempera...

Page 55: ...rent voltage readings Alarm limits are not changeable 15 Volts Displays current voltage readings Alarm limits are not changeable 24 0 Volts Displays current voltage readings Alarm limits are not chang...

Page 56: ...n lists items associated with the ozonator Value Displays the current value for each item Low Alarm Displays low alarm for each item High Alarm Displays high alarm for each item Units Displays units f...

Page 57: ...nostic Displays current voltage readings Alarm limits are not changeable 3 3 V Diagnostic Displays current voltage readings Alarm limits are not changeable 5 0 V Diagnostic Displays current voltage re...

Page 58: ...is visible only if the photometer option is installed All intensity screens function the same way Therefore the following example of the Intensity A Reference Gas screen applies to all screens as wel...

Page 59: ...fic 49iQPS Instruction Manual 3 35 Intensity B Sample Gas Displays sample gas Cell A Reference Gas Intensity Read only Cell A Reference Gas Noise Read only Cell B Reference Gas Intensity Read only Cel...

Page 60: ...l pressure check screens function the same way Therefore the following example of the Sample Pressure screen applies to all screens as well Home Screen Settings Health Check Status and Alarms Pressure...

Page 61: ...lists items associated with the flow and pressure module Value Displays the current value for each item Low Alarm Displays low alarm status for each item High Alarm Displays high alarm status for eac...

Page 62: ...upply Displays OK Fail of power supplies Power supply goes red if any voltages are outside their limits No voltage rows ever get highlighted 2 5V Diagnostic Displays current voltage readings Alarm lim...

Page 63: ...contains the following information Across Peripherals Support This column lists items associated with the peripherals support module Value Displays the current value for each item Low Alarm Displays...

Page 64: ...5V Diagnostic Displays current voltage readings Alarm limits are not changeable 3 3V Diagnostic Displays current voltage readings Alarm limits are not changeable 5 0V Diagnostic Displays current volt...

Page 65: ...the device needs to be reset Home Screen Settings Health Check Status and Alarms More Valve and Pump Resets The Valve and Pump Resets screen contains the following information Sample Cal Valve Reset...

Page 66: ...contains the following information Across Analog IO This column lists items associated with the analog I O Value Displays the current value for each item Low Alarm Displays low alarm status for each i...

Page 67: ...o voltage rows ever get highlighted 3 3V Diagnostic Displays current voltage readings Alarm limits are not changeable 5 0V Diagnostic Displays current voltage readings Alarm limits are not changeable...

Page 68: ...the following information Across Digital IO This column lists items associated with the digital I O Value Displays the current value for each item Reset Resets item Low Alarm Displays low alarm statu...

Page 69: ...oes red if any voltages are outside their limits No voltage rows ever get highlighted 3 3V Diagnostic Displays current voltage readings Alarm limits are not changeable 5 0V Diagnostic Displays current...

Page 70: ...larms More Serial Numbers The Serial Numbers screen contains the following information Instrument Instrument serial number Photometer Photometer serial number Ozonator Ozonator serial number Flow and...

Page 71: ...ing time If button is greyed out no maintenance is needed If button is blue maintenance is suggested Note This symbol denotes there is an active maintenance related warning in the module Home Screen S...

Page 72: ...Health Check Maintenance Home Screen Settings Health Check Maintenance Advanced Maintenance The Maintenance screen contains the following information Preventive Maintenance Shows suggested service in...

Page 73: ...reen contains the following information Across Component Device to be routinely serviced or replaced Interval in Months Expected period of time before a component needs to be checked and or serviced M...

Page 74: ...nterval for lamp heater Flow System Service interval for flow system components Pump Service interval for pump Capillaries Service interval for capillaries Ozone Scrubber Service interval for ozone sc...

Page 75: ...e diagnostics screen when applicable Home Screen Settings Health Check Maintenance Change Part The Change Part screen contains the following information Select Part User selects part to service from t...

Page 76: ...e and buttons to move up and down and the and buttons to move left and right Home Screen Settings Health Check Maintenance Maintenance History Note Retrieving maintenance history data it may take a fe...

Page 77: ...ive Email Health Check Report File to Technical Support Sends the health report file to technical support and the customer email addresses via email Email Health Check Report to Personal Account Sends...

Page 78: ...ngs Health Check iQ360 Get Started Home Screen Settings Health Check iQ360 Status and Renewal Request The iQ360 screen contains the following information Get Started Allows the user to access the menu...

Page 79: ...ck iQ360 Get Started The Get Started screen contains the following information Resend Subscription E mail Allows the user to request another subscription passcode if the email was never received Enter...

Page 80: ...nd Renewal Request The Status and Renewal Request screen contains the following information iQ360 Status Informs the user if the subscription is enabled iQ360 Subscription Expiration Date Informs the...

Page 81: ...creen Settings Measurement Settings The Measurement Settings screen contains the following information Averaging Time Sets the averaging time for the O3 sample measurement Gas Mode User can manually c...

Page 82: ...nds means that the moving average concentration of the last 300 seconds will be the output at each update Therefore the lower the averaging time the faster the front panel display and analog outputs r...

Page 83: ...on Manual 3 59 Home Screen Settings Measurement Settings Averaging Time dynamic filtering enabled The Averaging Time screen contains the following information Dynamic Filtering Enables disables dynami...

Page 84: ...he instrument is set to Home Screen Settings Measurement Settings Gas Mode The Gas Mode screen contains the following information Zero Used when calibrating the background of the instrument When press...

Page 85: ...standard pressure of 760 mmHg and a standard temperature of 0 C The temperature can be changed in the compensation screen Use the and buttons to select Home Screen Settings Measurement Settings Gas Un...

Page 86: ...Measurement Settings The Advanced Measurements Settings menu contains the following information Photometer Bench Settings User can set the detector gain This can be done manually or automatically Ozon...

Page 87: ...ettings Advanced Measurement Settings Photometer Bench Settings Home Screen Settings Measurement Settings Advanced Measurement Settings Photometer Bench Settings Continue to Photometer Bench Settings...

Page 88: ...urrent values for detector 2 If detector cal cell is pressed user can manually set the detector 2 cal value Auto Cal When Start is pressed the auto calibration process is initiated Please allow up to...

Page 89: ...s Measurement Settings Advanced Measurement Settings Ozonator Bench Settings Home Screen Settings Measurement Settings Advanced Measurement Settings Ozonator Bench Settings Continue to Ozonator Lamp P...

Page 90: ...o Cal When Start is pressed the auto calibration process is initiated Please allow up to 60 minutes for calibration to complete User can stop calibration by pressing the Stop button End Cal When Stop...

Page 91: ...ature variations The effects of internal instrument temperature changes on the instrument s subsystems and output have been empirically determined This empirical data is used to compensate for any cha...

Page 92: ...sor Calibration Starts calibration or resets default values Down Sensor 1 3 Reading Under the column labeled Reading current reading of each pressure sensor Atmospheric Sensor 1 3 Under the column lab...

Page 93: ...tion Communications Board Analog I O Settings for communicating with the instrument through analog I O settings This is only visible if selected in Settings Configuration Analog I O Digital I O Settin...

Page 94: ...t the instrument should respond with in response to a valid data query DA command Note Refer to the Bayern Hessen Protocol section in the Communications Manual for a detailed description Ethernet Prot...

Page 95: ...s disabled the static IP address is used Home Screen Settings Communications Wired TCP DHCP with DHCP enabled Home Screen Settings Communications Wired TCP DHCP with DHCP disabled The Wired TCP DHCP s...

Page 96: ...DHCP is disabled Static Netmask Static Netmask of instrument This is settable when DHCP is disabled Static Gateway Static Gateway of instrument This is settable when DHCP is disabled DNS Server Addres...

Page 97: ...e Screen Settings Communications Serial RS 232 485 The Serial RS 232 485 screen contains the following information Protocol User selects Streaming Modbus or Bayern Hessen Baud Rate User selectable bau...

Page 98: ...Analog In Allows the user to view and calibrate voltage inputs from external devices Analog Out Voltage Allows the user to view voltage outputs Analog Out Current Allows the user to view current mA o...

Page 99: ...Digital I O Home Screen Settings Communications Digital I O The Digital I O screen contains the following information Digital In Allows the user to view digital inputs from external devices Digital Ou...

Page 100: ...erver SMTP The Email Server SMTP screen contains the following information SMTP Server Address Address of the user s email server From Email Address The email address that goes in the From field in em...

Page 101: ...tings The Bayern Hessen Settings screen contains the following information Across Number Lists up to 8 registers that can selected by the user Register User selects the measured values to be logged Me...

Page 102: ...ilize the mobile app and or those communication protocols Press Commit changes button to save selections Yellow buttons indicate that the selection is enabled More than one can be chosen Home Screen S...

Page 103: ...tings screen contains the following information Display Setup Sets touchscreen display settings Alarm Setpoints View and set all available alarm setpoints Language Read only Clock Sets date and time P...

Page 104: ...r save option Home Screen Settings Instrument Settings Display Setup The Display Setup screen contains the following information Power Save Minutes before screen times out Toggles enable disable Power...

Page 105: ...larms screen See Status and Alarms on page 3 27 Use the and buttons to move up and down and the and buttons to move left and right Home Screen Settings Instrument Settings Alarm Setpoints The Alarm Se...

Page 106: ...Scientific Flow A Flow A pressure alarm Flow B Flow B pressure alarm Cell A Intensity Cell A intensity alarm Cell B Intensity Cell B intensity alarm Photometer Lamp Temp Photometer lamp temperature al...

Page 107: ...QPS Instruction Manual 3 83 The Language screen allows the user to choose from the following languages Home Screen Settings Instrument Settings Language The Language screen contains the following info...

Page 108: ...me zone and time server Home Screen Settings Instrument Settings Clock The Clock screen contains the following information Date User sets date Date Format User selects date format Time User sets time...

Page 109: ...hermo Scientific 49iQPS Instruction Manual 3 85 The Date screen allows the user to choose date Use the and buttons to move left and right to select month and year Home Screen Settings Instrument Setti...

Page 110: ...the user to choose from the following formats mm dd yyyy or dd mm yyyy Use the and buttons to select Home Screen Settings Instrument Settings Clock Date Format The Date Format screen contains the foll...

Page 111: ...l 3 87 The Time screen allows the user to choose from the following formats mm dd yyyy or dd mm yyyy Use the and buttons to select Home Screen Settings Instrument Settings Clock Time The Time screen c...

Page 112: ...nt Settings Clock Time Zone The Time Zone screen contains the following information Date Line West UTC 12 Samoa Time Zone UTC 11 Aleutian Time Zone UTC 10 Alaskan Time Zone UTC 9 Pacific Time Zone UTC...

Page 113: ...European Time UTC 1 Eastern European Time UTC 2 Further Eastern European Time UTC 3 Gulf Standard Time UTC 4 Yekaterinburg Time UTC 5 Omsk Time UTC 6 Indochina Time UTC 7 ASEAN Common Time UTC 8 Japa...

Page 114: ...odic clock updates Home Screen Settings Instrument Settings Clock Time Server The Time Server screen contains the following information Time Server Enables Disables periodic clock updates from an NTP...

Page 115: ...the plumbing configuration in their instrument Home Screen Settings Instrument Settings Advanced Instrument Settings Home Screen Settings Instrument Settings Advanced Instrument Settings 49iQPS Plumbi...

Page 116: ...pillary 1 Ozonator capillary and a Flow Pressure DMC that has 2 absolute pressure sensors on it the user would choose One Sample Capillary Two Sample Capillary If the instrument has 4 total capillarie...

Page 117: ...t press the Commit Changes button to save selections Yellow buttons indicate that the variable is selected More than one can be chosen Home Screen Settings Configuration The Configuration screen conta...

Page 118: ...ly Access The Security Access Levels screen contains the following information Current Security Access Full Access Read only User will be able to change all values Password is needed for full access C...

Page 119: ...tion Manual 3 95 Change Full Access Security Password Full access password can have a blank value or user selected password Change Instrument Password User can change instrument password Reset Instrum...

Page 120: ...View Only Access The Change Security to View Only Access screen contains the following information Set Access Level to View Only Programs the instrument to be in the view only access level where the...

Page 121: ...curity Password screen allows the user to set a new password for allowing full access Home Screen Settings Security Access Levels Change Full Access Security Password Home Screen Settings Security Acc...

Page 122: ...t security password Continue Proceeds to next screen Enter New Security Access Password User enters new security password Confirm New Security Access Password User confirms new security password for s...

Page 123: ...The Change Instrument Password screen allows the user to change the instrument password Home Screen Settings Security Access Levels Change Instrument Password Home Screen Settings Security Access Lev...

Page 124: ...t instrument password Continue Proceeds to next screen Enter New Instrument Password User enters new instrument password Confirm New Instrument Password User confirms new instrument password for spell...

Page 125: ...instrument serial number is 123456789 and the instrument firmware version is 1 6 8 ABCDE where the last five digits are the build number then the default instrument password number will be 1A2B3C4D5E6...

Page 126: ...e USB port When a USB drive is inserted the user is prompted to enter the password if a password has been set Home Screen Settings USB Drive The USB Drive screen contains the following information Fir...

Page 127: ...from the USB drive Home Screen Settings USB Drive Firmware Update Via USB Drive The Firmware Update Via USB Drive screen contains the following information Update Firmware User chooses firmware file...

Page 128: ...won t be recognized Also make sure the USB stick is formatted using the FAT or FAT32 file system 2 Plug a USB flash drive into the data port on the front panel of the unit or into one of the USB ports...

Page 129: ...on to start the firmware update process 5 Press the Update Firmware button 6 The on screen instructions will prompt the user to select the firmware update file and display what it is doing at each ste...

Page 130: ...not power off the instrument while the firmware update is in progress 8 The instrument should reboot automatically and should have the new firmware installed To check that the firmware was installed...

Page 131: ...ncludes a complete listing of data for all variables This is set at the factory Download System Log Consists of system log text files which include a listing of system errors Download Calibration Hist...

Page 132: ...he USB connection 1 Plug a USB flash drive into the USB connection on the front of the instrument If a USB password has been previously set you will be prompted to enter the USB password to continue P...

Page 133: ...transferring data to the USB drive Note Do not remove the USB drive from the instrument while the data is downloading 6 When the data download is complete the instrument will display a Success message...

Page 134: ...o Scientific The Change USB Password screen allows the user to set a new password for accessing USB Home Screen Settings USB Drive Change USB Password Home Screen Settings Security Access Levels Chang...

Page 135: ...rs current USB password Continue Proceeds to next screen Enter New USB Password User enters new USB password Confirm New Security Access Password User confirms new security password for spelling confi...

Page 136: ...ment serial number is 123456789 and the instrument firmware version is 1 6 8 ABCDE where the last five digits are the build number then the default USB password number will be 1A2B3C4D5E6789 Home Scre...

Page 137: ...brator events that can be programmed Each event can be assigned solenoid gas span setting ozonator span GPT NO2 span permeation span photometer mode and event duration Home Screen Settings Programmed...

Page 138: ...ogrammed Events View Programs The Programmed Events screen contains the following information Across Program Number This column lists the 20 programs Program Allows the user to enable disable individu...

Page 139: ...right Home Screen Settings Programmed Events Select Events 1 15 The Select Events screen contains the following information Across Program Events This column lists event numbers Action User enables d...

Page 140: ...ls found at the screen Health Check File Sharing and Support Home Screen Settings User Contact Information The User Contact Information screen contains the following information Business Name User Nam...

Page 141: ...ns our operating system on power up The bootloader may change to optimize hardware settings or if there are changes to the hardware If the button is blue an update to the bootloader is available If bu...

Page 142: ......

Page 143: ...quipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component For more in...

Page 144: ...nstrument OFF unplug the power cord and remove the cover 5 Mark the position of head parts relative to each other by drawing a line with a pencil This helps avoid incorrect assembly later 6 Undo the f...

Page 145: ...o the upper point 12 Screw the new diaphragm with connection rod disc and spacers clockwise onto the connection rod and tighten hand tight 13 Place the intermediate plate on housing in the position in...

Page 146: ...Maintenance Pump Rebuilding 4 4 49iQPS Instruction Manual Thermo Scientific Figure 4 2 Pump Rebuilding...

Page 147: ...the rear panel 3 Cap the OZONE out and VENT ports on the rear panel 4 Cap the Photometer reference side vent port internal to the unit 5 Connect the hand pump to the EXHAUST port on the rear panel 6...

Page 148: ...ific Use the following procedure to clean the mirrors Equipment required Hex drive 7 64 1 Unfasten nuts with hands No tool required Figure 4 3 Absorption Cleaning Removing Nuts 2 Pull up then pull out...

Page 149: ...s that the tube fits into Note Both absorption tubes are identical so they can be replaced in either position Replacement of absorption cells is opposite to that of removal Since the 49iQPS is a ratio...

Page 150: ...the detector side can be removed by removing the detector block and carefully removing the windows The windows on the source side can be removed by removing the source block to gain access to the win...

Page 151: ...es not start LEDs on front panel do not come on and display is blank No power Verify that the power cord is plugged in power is available and that it matches the voltage and frequency configuration of...

Page 152: ...Valve and Pump Resets Inspect and refurbish pump If pump motor is damaged replace pump Out of range pressure high upstream flow Too much positive pressure in sample line Regulate line to lower pressu...

Page 153: ...nts are too small or they are restricted The pump is not designed for this condition Alarm board communication failure Internal cables not connected properly Verify cables to DMC PCB are seated proper...

Page 154: ...recorder Sample is varying Run instrument on stable ozone source If quite no malfunction Foreign material in cell Clean cell Sticky solenoid valve Replace with known good solenoid valve Analyzer does...

Page 155: ...tration has exceeded range limit Check to ensure range corresponds with expected value If not select proper range Concentration low Check user defined low set point set to zero Alarm Lamp Heater Curre...

Page 156: ...eded Alarm Lamp Temp Sensor Short Ozone Defective sensor Replace sensor as needed Alarm Lamp Temp Sensor Open Ozone Defective sensor Replace sensor as needed Alarm Lamp Connection Ozone Defective lamp...

Page 157: ...ipment may be impaired CAUTION If the LCD panel breaks do not let the liquid crystal contact your skin or clothes If the liquid crystal contacts your skin or clothes wash immediately using soap and wa...

Page 158: ...st be worn while handling any internal component For more information about appropriate safety precautions see Safety Note If an antistatic wrist strap is not available be sure to touch the instrument...

Page 159: ...sh drive or company website at www thermofisher com For more information on installing new firmware see Installing New Firmware in the iQ Series Communications manual For a complete list of spare part...

Page 160: ...Servicing Replacement Parts List 6 4 49iQPS Instruction Manual Thermo Scientific Figure 6 2 49iQPS Component Layout Top View Figure 6 3 49iQPS Component Layout Side View...

Page 161: ...following procedure to replace the fuses 1 Turn instrument OFF and unplug the power cord 2 Remove fuse drawer located on the AC power connector 3 If either fuse is blown replace both fuses 4 Insert fu...

Page 162: ...rocedure to replace the filter 1 Turn instrument OFF and unplug the power cord 2 Starting with top right corner pull out to remove fan cover Figure 6 5 Start with Top Right Corner of Fan Cover 3 Repla...

Page 163: ...1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Unplug the fan cable J18 Figure 6 7 Unplugging the Fan Cable 3 Starting with top right corner pull out to remove fan cover 4...

Page 164: ...Servicing Fan Replacement 6 8 49iQPS Instruction Manual Thermo Scientific Figure 6 8 Replacing the Fan...

Page 165: ...rocedure to remove and replace the measurement side if necessary Equipment required Phillips drive 2 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Unplug the fan cable J18...

Page 166: ...S Instruction Manual Thermo Scientific Figure 6 10 Unplugging the DMC Cable 4 Gripping from the top corners of the front panel and pull outwards 5 Remove three 8 32 flat head screws Figure 6 11 Figure...

Page 167: ...Thermo Scientific 49iQPS Instruction Manual 6 11 6 Swing arm open 7 Unfasten captive hardware 8 Remove two 8 32 flat head screws 9 Pull measurement side out 10 Replace in reverse order Figure 6 12 Unf...

Page 168: ...ule Equipment required Wrench 1 4 1 Turn instrument OFF and unplug the power cord 2 Gripping from the top corners of the front panel and pull outwards 3 Unfasten four nuts Figure 6 13 Figure 6 13 Repl...

Page 169: ...Servicing LCD Module Replacement Thermo Scientific 49iQPS Instruction Manual 6 13 Figure 6 14 Remove Electrical Cables from LCD 7 Replace LCD module and reassemble in reverse order...

Page 170: ...Scientific Use the following procedure to replace the I O boards 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Swing arm open Figure 6 15 I O Replacement Arm 3 Pull board u...

Page 171: ...al 6 15 4 During install make sure to align cutout circular to keyway 5 Insert board downwards Figure 6 17 I O Replacement Install 6 Close arm Make sure expansion bracket aligns to the inside of the r...

Page 172: ...to replace the peripherals support board or system controller board 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Pull tab out two per board 3 Pull board out Figure 6 19 R...

Page 173: ...d flow board Equipment required Hex drive 7 16 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Unplug cables from the pressure and flow board Figure 6 20 Flow Pressure Board...

Page 174: ...Servicing DMC Pressure and Flow Board 6 18 49iQPS Instruction Manual Thermo Scientific Figure 6 21 Flow Pressure Board Screws 5 Replace board and reassemble in reverse order...

Page 175: ...Phillips drive 1 and 2 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Unplug pump cable from Step POL board J7 3 Twist opposite direction to unlock tube clamps Note Push in...

Page 176: ...p Replacement 6 20 49iQPS Instruction Manual Thermo Scientific Figure 6 22 Remove Pump Disconnect and Unfasten 7 Pull pump outwards Note When installing pump make sure the pump keyway opening goes ove...

Page 177: ...Pump Replacement Thermo Scientific 49iQPS Instruction Manual 6 21 Figure 6 23 Pump Removal Keyway 8 Remove two screws Figure 6 24 Pump replacing Unfasten Screws 9 Replace pump and reassemble in rever...

Page 178: ...y Equipment required Phillips drive 2 Hex drive 7 64 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Disconnect the plumbing 3 Using 2 Phillips drive unfasten captive hardwar...

Page 179: ...Replacement Thermo Scientific 49iQPS Instruction Manual 6 23 Figure 6 26 Capillary Plate Keyway 5 Using 7 64 hex drive remove four 6 32 socket cap head screws 6 Pull apart the capillary blocks Figure...

Page 180: ...ring pick tool 1 Using a metal o ring pick tool remove the o ring Note Be careful in not damaging the o ring walls during this process Refer to Figure 6 27 Use the following procedure to replace the...

Page 181: ...Supply Replacement Thermo Scientific 49iQPS Instruction Manual 6 25 Figure 6 28 Removing Power Supply 5 Pull power supply up 6 Replace power supply and reassemble in reverse order Figure 6 29 Replaci...

Page 182: ...Board Equipment required Torque screwdriver T15 or Slot screwdriver 3 16 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Unplug Step POL power cable J4 3 Unplug Step POL sig...

Page 183: ...6 Slide step board 1 upwards clearing the partition panel keyway 7 If replacing step board 1 make sure switch 1 and 2 are pointed away from ON Figure 6 32 If replacing optional step board 2 make sure...

Page 184: ...Servicing Step POL Board Replacement 6 28 49iQPS Instruction Manual Thermo Scientific Figure 6 32 Step POL Board 1 Switch Settings Figure 6 33 Optional Step POL Board 2 Switch Settings...

Page 185: ...wing procedure to service the Photometer DMC and replace the following as necessary Photometer lamp replacement Photometer DMC removal Photometer DMC board replacement Detector replacement Detector bo...

Page 186: ...e and replace the photometer lamp Equipment required Hex drive 3 32 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Disconnect lamp connector 3 Unhook lamp cable from cable h...

Page 187: ...hermo Scientific 49iQPS Instruction Manual 6 31 5 Peel insulation back enough to unfasten this screw 6 Using a 3 32 hex drive unfasten the 6 32 cap head screw Figure 6 37 Lamp Removal pt 3 7 Rebuild i...

Page 188: ...illips drive 2 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Unplug DMC cable top connector photometer DMC board to pressure flow board 3 Unplug DMC cable bottom connector...

Page 189: ...e to replace the board Equipment required Phillips drive 2 1 Unplug electrical detector 1 detector 2 thermistor and heater 2 Using a 2 Phillips drive unfasten five 6 32 pan head screws Figure 6 39 Pho...

Page 190: ...pre amplifier detector assembly Equipment required Hex drive 7 64 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Unplug electrical cable from detector 1 and detector 2 Figu...

Page 191: ...Servicing 49iQPS Photometer DMC Thermo Scientific 49iQPS Instruction Manual 6 35 Figure 6 41 Replacing the Detector 4 Replace detector and reassemble in reverse order...

Page 192: ...wer cord and remove the cover Figure 2 1 2 Unplug electrical cable from detector 1 and detector 2 3 Using a 3 32 hex drive unfasten four 4 40 cap head screws to remove the cover 4 Remove detector cove...

Page 193: ...he thermistor Equipment required Wrench 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Unplug the thermistor from the photometer DMC board 3 Using a wrench unfasten 1 4 hex...

Page 194: ...rn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Unplug electrical from Step POL board solenoid valve sample J8 and solenoid valve reference J6 3 Disconnect 2X plumbing 4 Using a...

Page 195: ...Replacement Thermo Scientific 49iQPS Instruction Manual 6 39 6 Turn assembly upside down 7 Unfasten kep nuts two per valve Figure 6 45 Removing the Solenoid Tray pt 2 8 Replace solenoids and reassembl...

Page 196: ...Lamp replacement Ozonator DMC board replacement Ozonator detector board replacement Ozonator replacement Ozonator DMC reassemble Use the following procedure to remove and replace the ozonator Equipmen...

Page 197: ...DMC Ozonator Thermo Scientific 49iQPS Instruction Manual 6 41 Figure 6 46 Ozone Removal pt 1 5 Slide ozonator assembly left Note Make sure ozonator plate clears the edge and stud Figure 6 47 Ozone Rem...

Page 198: ...42 49iQPS Instruction Manual Thermo Scientific 6 Slide ozonator assembly upwards Note Make sure ozonator plate clears the edge Figure 6 48 Ozone Removal pt 3 7 Pull away from the partition panel Figur...

Page 199: ...equired Ball end hex drive 3 32 1 Remove the ozonator DMC from the instrument Refer to DMC Ozonator Removal on page 6 40 2 Using a 3 32 ball end hex drive angle alignment of screws unfasten two 4 40 c...

Page 200: ...required Phillips drive 2 1 Remove the ozonator DMC from the instrument Refer to DMC Ozonator Removal on page 6 40 2 Unplug heater and lamp cable 3 Using a 2 Phillips drive unfasten five 6 32 pan head...

Page 201: ...ozonator Equipment required Phillips drive 2 1 Remove the ozonator DMC from the instrument Refer to DMC Ozonator Removal on page 6 40 2 Unplug heater and lamp cable Figure 6 52 Ozonator replace pt 1...

Page 202: ...Servicing DMC Ozonator 6 46 49iQPS Instruction Manual Thermo Scientific Figure 6 53 Replacing the Ozonator 5 Replace ozonator and reassemble in reverse order...

Page 203: ...nwards Note Make sure ozonator plate slides into bottom pocket Note Make sure ozonator plate goes over the partition panel keyway stud Figure 6 54 Installing the Ozonator DMC 2 Slide ozonator assembly...

Page 204: ...Servicing DMC Ozonator 6 48 49iQPS Instruction Manual Thermo Scientific Figure 6 55 Ozone DMC install pt 2...

Page 205: ...and remove the cover Figure 2 1 2 Disconnect 2x plumbing 3 Using a wrench unfasten regulator nut Remove as shown 4 Pull pressure regulator outwards Figure 6 56 Pressure Regulator Note Make sure regula...

Page 206: ...d Phillips drive 2 Wrench 1 Turn instrument OFF unplug power cord and remove the cover Figure 2 1 2 Using a wrench unfasten three nuts Remove the nuts front and back ferrules as shown from back panel...

Page 207: ...Servicing Optional Manifold Replacement Thermo Scientific 49iQPS Instruction Manual 6 51 Figure 6 58 Replacing the Manifold pt 3 5 Replace the manifold and assemble in reverse order...

Page 208: ......

Page 209: ...system components in the module framework including firmware electronics and I O function The 49iQPS system components include Photometer DMC with lamp Detector assembly Photometer lamp power supply...

Page 210: ...ity is varied by changing the current into the lamp The gas flow is held constant by a pressure regulator followed by a capillary The optional ozonator lamp power supply generates high voltage AC and...

Page 211: ...OWER FILTER SWITCH GND SYSTEM CONTROLLER BOARD A C FRONT USB PORT BOARD DISPLAY LEDS MFC 1 TOUCH SCREEN LCD DISPLAY 48V POWER SUPPLY DMC 1 DMC 2 24V POWER 2 POL 1 DATA POL 2 24V POL 1 24V POWER POWER...

Page 212: ...ientific 49 Photometer DMC Flow Pressure DMC Step Pol Ref Sol Backplane Measurement Case POL 1 DATA POL 1 24V POWER DMC 1 Pump Fan Fan 24V iQ Series 49 PS 49 Ozonator DMC Lamp Heater Lamp Heater Sampl...

Page 213: ...communication channels as described in Chapter 3 Operation The System Controller Board SCB contains the main processor power supplies and a sub processor and serves as the communication hub for the in...

Page 214: ...e through the instrument The Flow Pressure DMC is used measure instrument pressures that assure proper flow regulation and for sample pressure within the measurement bench for pressure corrections and...

Page 215: ...ystem operates on 1 second intervals Within those intervals data treatment like integration whether analog or digital and servo control are embedded in the module firmware The SCB receives the 1 secon...

Page 216: ......

Page 217: ...is available with the following options Several components are available for connecting external devices These connection options consist of three plug in boards Communication Board Analog I O Board D...

Page 218: ...ses a 9 pin serial connector with a bi directional serial interface that can be configured for either RS 232 or RS 485 communication Figure 8 2 RS 232 RS 485 Port Table 8 1 RS 232 RS 485 Port Terminal...

Page 219: ...t devices Figure 8 3 RS 485 External Accessory Port Table 8 2 RS 485 External Accessory Port Terminal Assignment Terminal Number Signal Name 1 EXT_RS485_RX_N 2 EXT_RS485_RX_P 3 5V Fused 0 4A 4 5V Fuse...

Page 220: ...ges 0 1 0 V 0 5 0 V 0 10 V 6 Isolated Analog Current Outputs Two Ranges 0mA 20mA 4mA 20mA Table 8 3 lists the analog voltage inputs are used to monitor four external 0 10V signals Figure 8 4 Analog Vo...

Page 221: ...ed through the software control registers to select Voltage Output ranges 0 1 V 0 5 V or 0 10 V as well as Current Output ranges 0 20 mA or 4 20 mA The maximum allowable load for each Current Output i...

Page 222: ...6 18 C V Return 6 The iQ series instruments provide for the ability to calibrate the analog outputs both voltage and current of the instruments The basic procedure for both voltage and current are th...

Page 223: ...tion follow the same procedure by selecting the 4 mA current calibration option Note This adjustment should only be performed by an instrument service technician 1 From the Home screen choose Settings...

Page 224: ...ease Decreases the output by coarse medium or fine amounts Increase Increase and Increase Increases the output by coarse medium or fine amounts Commit Accepts the changes to the analog output levels 5...

Page 225: ...follow the same procedure by selecting the 20 mA current calibration option Note This adjustment should only be performed by an instrument service technician 1 From the Home screen choose Settings Com...

Page 226: ...ease Decrease and Decrease Decreases the output by coarse medium or fine amounts Increase Increase and Increase Increases the output by coarse medium or fine amounts Commit Accepts the changes to the...

Page 227: ...al Relay Switches 20 pin connector 8 Valve Driver Outputs 16 pin connector The digital inputs are TTL 3 V or 5 V compatible and are pulled high within the instrument The active state can be user defin...

Page 228: ...ts Terminal Assignment Terminal Number Signal Name COMMON 1 Digital In 1 2 Digital In 2 3 Digital In 3 4 Digital In 4 5 Digital In 5 6 Digital In 6 7 Digital In 7 8 Digital In 8 9 Digital In 9 10 Digi...

Page 229: ...ng External Devices Thermo Scientific 49iQPS Instruction Manual 8 13 Table 8 6 lists the digital relay switches Maximum Voltage 300 VDC Maximum Current 500 mA Fuse 800 mA Figure 8 7 Digital Relay Swit...

Page 230: ...Digital Relay Switch Assignment Terminal Number Signal Name 1A Relay 1A 1B Relay 1B 2A Relay 2A 2B Relay 2B 3A Relay 3A 3B Relay 3B 4A Relay 4A 4B Relay 4B 5A Relay 5A 5B Relay 5B 6A Relay 6A 6B Rela...

Page 231: ...Instruction Manual 8 15 Table 8 7 lists the valve driver outputs Actual Output Voltage 22 24 VDC Maximum Current 300 mA Both positive and negative outputs are protected from over voltage and over curr...

Page 232: ...Name 1 Valve Drive 1 1 Valve Drive 1 2 Valve Drive 2 2 Valve Drive 2 3 Valve Drive 3 3 Valve Drive 3 4 Valve Drive 4 4 Valve Drive 4 5 Valve Drive 5 5 Valve Drive 5 6 Valve Drive 6 6 Valve Drive 6 7...

Page 233: ...O3 monitoring requirements This option includes the pump filter filter holder and Silastic tubing A 5 10 micron pore size two inch diameter PTFE element is available for the 49iQPS This filter should...

Page 234: ......

Page 235: ...ous personal injury if the warning is ignored A hazard is present or an unsafe practice can result in serious personal injury if the warning is ignored The hazard or unsafe practice could result in mi...

Page 236: ...arts may be new or refurbished at the election of Seller All replaced parts shall become the property of Seller Shipment to Buyer of repaired or replacement Products shall be made in accordance with t...

Page 237: ...S PRIOR WRITTEN APPROVAL OR ANY USE OF REPLACEMENT PARTS NOT SUPPLIED BY SELLER SHALL IMMEDIATELY VOID AND CANCEL ALL WARRANTIES WITH RESPECT TO THE AFFECTED PRODUCTS THE OBLIGATIONS CREATED BY THIS...

Page 238: ...hermo Fisher Scientific s compliance with these Directives the recyclers in your country and information on Thermo Fisher Scientific products which may assist the detection of substances subject to th...

Page 239: ...p Rebuilding 4 4 Figure 4 3 Absorption Cleaning Removing Nuts 4 6 Figure 4 4 Absorption Tube Removal 4 6 Figure 4 5 Absorption cleaning pt 3 clean tube 4 7 Figure 4 6 Absorption cleaning pt 4 clean wi...

Page 240: ...25 Figure 6 29 Replacing Power Supply 6 25 Figure 6 30 Unplug and Unfasten Step POL Board 6 26 Figure 6 31 Clear Partition Keyway Step POL Board 6 27 Figure 6 32 Step POL Board 1 Switch Settings 6 28...

Page 241: ...485 Port 8 2 Figure 8 3 RS 485 External Accessory Port 8 3 Figure 8 4 Analog Voltage Inputs 8 4 Figure 8 5 Analog Voltage and Current 8 5 Figure 8 6 Digital Inputs 8 11 Figure 8 7 Digital Relay Switch...

Page 242: ......

Page 243: ...ary Public License version 2 hence the version number 2 1 Preamble The licenses for most software are designed to take away your freedom to share and change it By contrast the GNU General Public Licen...

Page 244: ...t the original version so that the original author s reputation will not be affected by problems that might be introduced by others Finally software patents pose a constant threat to the existence of...

Page 245: ...the wherewithal to run that program using a modified version of the Library The precise terms and conditions for copying distribution and modification follow Pay close attention to the difference betw...

Page 246: ...brary You may charge a fee for the physical act of transferring a copy and you may at your option offer warranty protection in exchange for a fee 2 You may modify your copy or copies of the Library or...

Page 247: ...Library To do this you must alter all the notices that refer to this License so that they refer to the ordinary GNU General Public License version 2 instead of to this License If a newer version than...

Page 248: ...under Section 6 Otherwise if the work is a derivative of the Library you may distribute the object code for the work under the terms of Section 6 Any executables containing that work also fall under S...

Page 249: ...of the work that uses the Library must include any data and utility programs needed for reproducing the executable from it However as a special exception the materials to be distributed need not inclu...

Page 250: ...parties with this License 11 If as a consequence of a court judgment or allegation of patent infringement or for any other reason not limited to patent issues conditions are imposed on you whether by...

Page 251: ...of any later version published by the Free Software Foundation If the Library does not specify a license version number you may choose any version ever published by the Free Software Foundation 14 If...

Page 252: ...library It is safest to attach them to the start of each source file to most effectively convey the exclusion of warranty and each file should have at least the copyright line and a pointer to where...

Page 253: ...r terms of your choice provided that i the header files of the Library have not been modified and ii the incorporated material is limited to numerical parameters data structure layouts accessors macro...

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Page 255: ......

Page 256: ...282 0430 Fax 508 520 2800 orders aqi thermofisher com India C 327 TTC Industrial Area MIDC Pawane New Mumbai 400 705 India Ph 91 22 4157 8800 india thermofisher com China 8 F Bldg C of Global Trade C...

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