PerkinElmer Frontier IR User Manual Download Page 2

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Release History

Part Number

Release

Publication Date

L1050102

July 2013

Any comments about the documentation for this product should be addressed to:

User Assistance

PerkinElmer Ltd

Chalfont Road

Seer Green

Beaconsfield

Bucks HP9 2FX

United Kingdom

Or emailed to: [email protected]

Notices

The information contained in this document is subject to change without notice.

Except as specifically set forth in its terms and conditions of sale, PerkinElmer makes no

warranty of any kind with regard to this document, including, but not limited to, the

implied warranties of merchantability and fitness for a particular purpose.

PerkinElmer shall not be liable for errors contained herein for incidental consequential damages in

connection with furnishing, performance or use of this material.

Copyright Information

This document contains proprietary information that is protected by copyright.

All rights are reserved. No part of this publication may be reproduced in any form whatsoever or

translated into any language without the prior, written permission of PerkinElmer, Inc.

Produced in the United Kingdom

Trademarks

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are protected by law.

PerkinElmer is a registered trademark of PerkinElmer, Inc.

Spectrum, AssureID and Frontier are trademarks of PerkinElmer, Inc.

Summary of Contents for Frontier IR

Page 1: ...FRONTIER IR DUAL RANGE SYSTEMS User s Guide MOLECULAR SPECTROSCOPY...

Page 2: ...itness for a particular purpose PerkinElmer shall not be liable for errors contained herein for incidental consequential damages in connection with furnishing performance or use of this material Copyr...

Page 3: ...trols 26 The sample compartment 27 Internal accessories 28 External accessories 28 The Spotlight 400 Series Imaging System 29 Sample compartment windows 30 Power switch and communications ports 30 Acc...

Page 4: ...n Detail 64 Changing the Desiccant 65 Renewing the instrument desiccant 66 Installing rechargeable desiccant in the instrument 67 Renewing the desiccant in the spare window compartment 68 Purging the...

Page 5: ...Introduction...

Page 6: ...information on collecting viewing and processing spectra using Spectrum software refer to the help file that you can access from the Help menu or by clicking Help on a dialog The Help menu also inclu...

Page 7: ...F All eight digit numbers are PerkinElmer part numbers unless stated otherwise The term instrument refers to a Frontier IR spectrometer and any sampling accessory fitted Frontier IR Dual Range spectr...

Page 8: ...os En recuadros ste se proporciona informaci n sobre este tipo de circunstancias Caution Attention Nous utilisons le terme CAUTION ATTENTION pour signaler les situations susceptibles de provoquer de g...

Page 9: ...dros como ste se proporciona informaci n sobre este tipo de circunstancias Warning Danger Nous utilisons la formule WARNING DANGER pour avertir des situations pouvant occasionner des dommages corporel...

Page 10: ...10 Frontier IR Dual Range Systems User s Guide...

Page 11: ...Warnings and Safety Information...

Page 12: ...f the instrument DO keep the instrument dry Avoid spilling liquid into the instrument Clean all external spills immediately If anything that is spilled enters the main body of the instrument switch of...

Page 13: ...justment maintenance and repair of the opened operating instrument If any adjustment maintenance and repair of the opened operating instrument is necessary this must only be done by a skilled person w...

Page 14: ...lated area if nitrogen will be used as a purge gas or if liquid nitrogen will be used to cool a detector Oxygen depletion in an enclosed space does not trigger a gasping reflex and errors of judgment...

Page 15: ...on the instrument and there is any possibility that they have entered the interior by coming into contact with cover gaskets for example then the instrument must be switched off immediately and disco...

Page 16: ...nals may be live and the removal of covers other than those which can be removed by hand is likely to expose live parts Capacitors inside the instrument may still be charged even if the instrument has...

Page 17: ...d The laser is automatically shut down when the main cover of the instrument is raised The instrument complies with the following laser safety regulations 1 21 CFR Part 1040 10 and 1040 11 except for...

Page 18: ...m is normally given by the eye s aversion response including the blink reflex which limits exposure of the eye to less than 0 25 seconds Class 1 levels of laser radiation are not considered to be haza...

Page 19: ...ification label is on the front of the instrument Other labels are fixed to the Frontier IR spectrometers in the locations shown in Figure 1 and Figure 2 Figure 1 Labels rear of instrument NOTE The la...

Page 20: ...ier IR Dual Range Systems User s Guide NOTE There is a second copy of the CAUTION label inside the sample compartment cover Figure 2 Labels sample compartment Serial number part number and date of man...

Page 21: ...nt Caution hot surface Caution risk of electric shock Caution laser radiation hazard Caution risk of danger Refer to accompanying documents in all cases where this symbol is used to find out the natur...

Page 22: ...nd tested to meet the requirements of the EMC Directive 2004 108 EC FCC rules and regulations These products are classified as digital devices used exclusively as industrial commercial or medical test...

Page 23: ...An Overview of the Frontier IR Dual Range Spectrometers...

Page 24: ...n MCT mercury cadmium telluride detector is fitted KBr windows are fitted in the sample compartment For the NIR configuration The optical system enables you to collect data over a total range of 14700...

Page 25: ...Sample Compartment Windows on page 61 or Installing Replacing Beam Port and Sample Compartment Windows on page 85 for more information NOTE If you have a Frontier FT IR FT FIR spectrometer with an MCT...

Page 26: ...urce and a fire or explosion will result Only use clean dry oil free nitrogen or air to purge the instrument The optics are kinematically mounted to ensure accurate positioning and to make them rugged...

Page 27: ...ndard sampling accessories are mounted on a baseplate The standard baseplate includes a sample holder located by a knurled screw CAUTION The windows in the sample compartment and external beam ports a...

Page 28: ...External accessories The external beam port on the right side of the instrument is used for example with the optional External Near Infra Red Accessory External NIRA Spectrum software enables you to s...

Page 29: ...nal External Beam Pack If you did not purchase the External Beam Pack with your spectrometer it is available as a field fitted upgrade L1280248 CAUTION Do not attempt to remove the external accessory...

Page 30: ...IR FT FIR Sample Compartment Windows on page 61 A desiccated compartment is provided for storing spare windows NOTE For long term storage of spare windows we recommend that you use a desiccator Figur...

Page 31: ...ATR and External NIRA accessories There is a range of specialized sampling accessories available for the Frontier IR instruments as shown in Table 1 Table 1 Sampling accessories for the Frontier IR i...

Page 32: ...ernal LiTaO3 Detector External Yes Yes n a The NIR Tablet Autosampler accessory is supported by AssureID software and Spectrum software version 6 x It is not supported in Spectrum software version 10...

Page 33: ...Ask your PerkinElmer Customer Service Representative for details L1280252 Frontier FT IR FT NIR Narrow band MCT Detector Upgrade replaces standard MIR detector L1280253 Frontier FT IR FT NIR Medium ba...

Page 34: ...34 Frontier IR Dual Range Systems User s Guide...

Page 35: ...Unpacking and Installation...

Page 36: ...er The primary fuse is connected in the live line Environment To obtain the best performance from your instrument Place the instrument in an environment that is relatively dust free Make sure that the...

Page 37: ...shipping container Your instrument is packed inside the box in a silver bag that protects it from condensation The beamsplitters are packed as a kit in a separate protective box 1 First remove the ma...

Page 38: ...shipping container but not from the bag in which it was shipped CAUTION The spectrometer and beamsplitters must be allowed to reach the temperature of their surroundings This means leaving them in the...

Page 39: ...es pink but while the sectors marked 15 and 20 are still blue These numbers correspond to the approximate Relative Humidity in the instrument Refer to The Desiccant Indicator in Detail on page 61 for...

Page 40: ...o the network connection on your PC if you are using the crossover cable or network hub if you are using a standard Ethernet cable Connector details Description Connector Type Voltage Maximum Current...

Page 41: ...e instrument when it is switched on Connector details Icon Description Connector Type Voltages Maximum Currents 10101 Serial port Connects a PC to the instrument using an RS232 interface cable This co...

Page 42: ...e spectrometer to the electrical supply The power cable for the electrical supply plugs into the rear of the instrument It has a molded socket at one end If it is necessary to fit a plug on the power...

Page 43: ...electrical supply inlet Figure 14 of the instrument Figure 14 Electrical supply inlet 2 Switch on the power at the supply 3 Switch on the instrument at the switch above the supply inlet I is on and O...

Page 44: ...DVD and follow the instructions on the screen Details of the installation program are given in the Administrator s Guide The Instrument Install Wizard After installing your software you will need to...

Page 45: ...Using the Spectrometer with Spectrum...

Page 46: ...application OR Double click the shortcut icon on the desktop The Spectrum start up splash screen is displayed followed by a dialog that may require your login details 3 If required enter your User na...

Page 47: ...enter a unique Sample ID and Description for the sample If required you can also change the wavelength range of the spectrometer using the Mode drop down list See Changing the instrument range on pag...

Page 48: ...Select the Setup Instrument BeamPath tab The Mode field in the settings table shown here as MIR displays the current range NOTE The Mode option is also available in the Instrument Settings toolbar 3...

Page 49: ...n each item the appropriate row in the Settings Table is highlighted The accessory fitted in the sample compartment is identified by a graphic element in the beampath schematic If an external accessor...

Page 50: ...ith the beampath directed to the External NIRA circled Using the Spectrum on screen Help system Use the Spectrum Help system to find further information about using Spectrum software to control set up...

Page 51: ...ing the following issues Non linearity due to resolution The measured spectrum is temperature dependent Lineshape and calibration are affected by J stop and sample or accessory What does atmospheric s...

Page 52: ...52 Frontier IR Dual Range Systems User s Guide Figure 21 Atmospheric suppression...

Page 53: ...t performance over time and between instruments Traceability for all measurements Although FT IR spectrometers use a reference laser the wavenumber calibration and lineshape are affected by difference...

Page 54: ...nt instrument profile relative to an absolute standard the methane cell and an ideal lineshape function and applies a correction Figure 22 If you have an automated internal filter wheel this can provi...

Page 55: ...matically This information is used to identify the scans that are being collected and to accumulate sample scans This can decrease the overall scanning time required for those samples that require sca...

Page 56: ...d tab and if required adjust the threshold range using the slider bars To display more information about an individual test double click on its name in the list When you collect your spectrum the sele...

Page 57: ...Routine Maintenance...

Page 58: ...spilling liquid into the instrument Clean all external spills immediately If anything that is spilled enters the main body of the spectrometer switch off the power and contact a PerkinElmer Service E...

Page 59: ...sing the shaped handholds on its sides as shown in Figure 23 Two people are needed to lift it because its basic weight is approximately 36 kg Figure 23 Lifting a Frontier IR spectrometer CAUTION Do no...

Page 60: ...essary to set a different temperature range to ensure optimal performance 1 Browse to the C Program Files PerkinElmer ServiceIR or C Program Files x86 PerkinElmer ServiceIR directory and then double c...

Page 61: ...ample compartment and the PE D window is installed in the right side of the sample compartment 1 Open the sample compartment cover 2 Using the 3 mm screwdriver part number L9003317 supplied with the Q...

Page 62: ...mpartment wall by tightening the screws using the 3 mm screwdriver Figure 25 NOTE Do not over tighten the screws 7 Repeat steps 2 6 for the other sample compartment window 8 Close the sample compartme...

Page 63: ...ore you change to the MIR MCT detector in Spectrum software fit one of the attenuators supplied to the window to the right of the sample compartment to prevent the detector from overloading Figure 27...

Page 64: ...is fitted in the desiccated compartment Figure 34 on page 68 This is used for storing sample compartment windows when not in use Figure 28 The desiccant indicator when desiccant packs should be change...

Page 65: ...option on the Setup Instrument BeamPath tab in Spectrum software Figure 29 Figure 29 Setup Instrument BeamPath tab in Spectrum If an instrument desiccant change is overdue a warning will be displayed...

Page 66: ...ontains two packs of desiccant and three kits are required 1 Inspect the humidity indicator card in the plastic bags in which the spare desiccant packs are packed If the card indicates humidity in the...

Page 67: ...desiccant in the instrument There is also a rechargeable desiccant kit available part number L1250311 To install rechargeable desiccant packs follow the procedure in Renewing the instrument desiccant...

Page 68: ...PerkinElmer part number N0171159 A kit contains two packs of desiccant and one kit is required 1 Inspect the humidity indicator card in the plastic bags in which the spare desiccant packs are packed I...

Page 69: ...68 The desiccated compartment requires a single rechargeable desiccant pack that is sized to fit the desiccant container The rechargeable desiccant kit contains two rechargeable desiccant packs This...

Page 70: ...dry nitrogen or dry air stores 6 26 m3 at 1 4 104 kPa 220 ft3 at 2200 lbf in2 Make sure that the gas is free of oil water or dirt particles larger than 25 m 0 001 inch WARNING Do not site the instrume...

Page 71: ...nt to be purged Figure 36 If the connector will not push in press the clip at the bottom of the port and try again Figure 36 Connector fitted to purge port 4 Connect the free end of the tubing to the...

Page 72: ...tier IR Dual Range Systems User s Guide 7 Disconnect the fitting from the instrument by pushing the clip located at the bottom of the purging port Figure 37 Figure 37 Disconnect the locking clip Locki...

Page 73: ...50 V Time Lag fuses part number 04970839 from PerkinElmer You must only replace the fuse with one of this type and rating Do not use makeshift fuses and do not short circuit fuse holders WARNING Befor...

Page 74: ...r the power socket The fuse is in the right hand slot 2 Remove the old fuse and discard it 3 Fit the new fuse into the slot Figure 39 Figure 39 Fuse fitted drawer open 4 Close the drawer The new fuse...

Page 75: ...errors of judgment confusion or unconsciousness can occur in seconds and without warning WARNING Be sure to wait the specified time when filling the funnel and before replacing the plug This enables...

Page 76: ...uid nitrogen NOTE Make sure that the detector dewar is filled to the top with liquid nitrogen before selecting the detector Prevent radiation from reaching the detector by obstructing the beam path in...

Page 77: ...ain at its operating temperature for approximately eight hours NOTE Cooled detector dewars require pumping down after approximately 12 months operation When the boil off rate of liquid nitrogen become...

Page 78: ...78 Frontier IR Dual Range Systems User s Guide...

Page 79: ...Advanced Maintenance...

Page 80: ...laser radiation CAUTION Do not open the main cover if the humidity is 80 relative humidity for an instrument fitted with KBr optics The humidity sensitive optics will be damaged if subjected to a rel...

Page 81: ...rds you and sliding the accessory towards you Figure 43 Figure 43 Removing the sampling accessory 6 Undo the two locking bolts on the front of the instrument using the hexagonal wrench supplied insert...

Page 82: ...n and rotating it opposite to the direction indicated by the arrows in Figure 44 12 If required reinstall the sampling accessory by sliding it on the ledge and pushing it into the sample compartment u...

Page 83: ...llow sufficient time for the source to cool before attempting to remove it 1 Open the main cover of the instrument as detailed on page 80 and identify the source Figure 46 Figure 46 Source location fo...

Page 84: ...urce are white 3 By grasping the round metal source body NOT the wires remove the source from its housing by pulling noting its installed position 4 Install the new source in its housing by pushing in...

Page 85: ...you open the cover of the spectrometer This makes sure that you are safe from electrical shock and laser radiation 1 Open the main cover of the instrument as detailed on page 80 Using the hexagonal wr...

Page 86: ...ctor for the MIR range you will be supplied with an Attenuator kit part number L1160560 containing 1 T 4 T 6 T 14 T and 32 T attenuators The attenuators attach to the window magnetically You will requ...

Page 87: ...e WARNING Switch off the mains power supply to the spectrometer wait 60 seconds and disconnect the power cable before you open the cover of the spectrometer This makes sure that you are safe from elec...

Page 88: ...y Figure 53 and then gently ease the filter wheel off the shaft rotating the filter wheel as required to clear the filter wheel from the other instrument components Take care not to remove the spacer...

Page 89: ...and then remove the filter holder and foam spacer 8 Place the filter in the hole place the foam spacer on top of it and then fit the filter holder Figure 55 illustrates the assembly sequence Align th...

Page 90: ...der onto the baseplate with the knurled screw 11 Close and secure the main cover Refer to steps 11 to 15 on page 82 12 Select the filter you would like to use in the beam path from the Filter Wheel dr...

Page 91: ...ter This makes sure that you are safe from electrical shock and laser radiation WARNING Do not attempt to separate the Laser from the power supply The Laser retains an electrical charge even when the...

Page 92: ...instrument 3 Slacken the two screws securing the laser power supply 4 Unscrew and remove the cable clip that secures the thin black and red PSU laser cable at the rear of the instrument underneath the...

Page 93: ...ng label is facing directly upwards 9 Refit the laser retaining bracket and secure with the two securing screws 10 Secure the spring on the retaining pin 11 Reconnect the PSU laser cable to the board...

Page 94: ...94 Frontier IR Dual Range Systems User s Guide...

Page 95: ...Appendices...

Page 96: ...ing the clip and pulling the cover vertically to remove Figure 60 Figure 60 Removing the sample area cover 2 Remove the current sampling accessory by pulling the release handle under the baseplate of...

Page 97: ...he sample compartment until it engages with the connector Figure 62 Installing a sampling accessory Spectrum automatically recognizes which accessory is installed and displays the accessory informatio...

Page 98: ...he instrument display provides this sequence of messages Initializing Initializing Checking Program Integrity Checking Instrument Configuration Checking Source Checking Laser Checking Scan Checking Ca...

Page 99: ...m persists note any associated error messages and consult your PerkinElmer service representative Scan Failed If the problem persists note any associated error messages and consult your PerkinElmer se...

Page 100: ...alidate the MIR performance of your instrument use the optional MIR Performance Validation Kit part number L1250404 This kit contains an MIR polystyrene reference sample and an NG11 Schott Glass refer...

Page 101: ...pment Decontamination Procedure and complete the Certificate of Decontamination These documents are available on the PerkinElmer public website http las perkinelmer com OneSource decontamination htm A...

Page 102: ...ment is the most effective means of protecting the customer s environment The requirements for waste collection reuse recycling and recovery programs are set by the regulatory authority at your locati...

Page 103: ...26 E Electrical supply inlet 43 EMC Compliance 22 EC Directive 22 FCC rules 22 External accessories 28 F FCC rules and regulations 22 Filter wheel Filter 89 Filter holder 89 Foam spacer 89 Installing...

Page 104: ...Summary 12 Use of flammable solvents and samples 15 Use of nitrogen 14 Safety interlock 25 Sample area cover Release clip 96 Removing 96 Sample compartment 27 Sampling accessories Diffuse Reflectance...

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