8 Performing a Measurement
56
D52IB001EN-G
8.4.5 Mounting and use of the Antechamber
for TTK 600
In order to use the antechamber for TTK 600, the
normal lid of the instrument has to be removed. In
order to transfer a sample without interaction with air
from a glove box to TTK 600, the following steps are
necessary:
Before the sample is loaded to the antechamber,
connect the Pt100 blind plug (2) that was delivered
together with the antechamber to the Pt100 plug
connector (1).
1 Pt100 plug connector
2 Pt100 blind plug
This is necessary to change the control behavior of
CCU 100 from the Pt100 to the thermocouple inside
the heater.
Fig. 58: Antechamber TTK 600
1 Sample holder for antechamber
2 Closing mechanism
3 Sample holder loader
4 Gas tight compartment
5 Vacuum flange
6 Torx screw for sample holder fixation
7 Mounting screws
1. Place the antechamber as depicted in Fig. 58
(A) in the glove box. In order to do so a separate
mount is contained in the delivery of the ante-
chamber (see appendix 12).
2. Fill the sample into the sample holder (1).
3. Pull back the sample loader (3).
4. Close the gas tight compartment (4) by pushing
in the closing mechanism (2) like shown in
Fig. 58 (B).
5. Extract the antechamber from the glove box and
mount it on TTK 600. The mounting is done in
exactly the same way as for the standard lid of
the instrument by using the two mounting
screws (7).
6. Connect the gas vacuum connector to the vac-
uum flange (5) of the antechamber.
7. Remove residual air from TTK 600 by purging
gas and/or evacuating.
8. In the final step of air removal bring TTK 600
back to ambient pressure by purging with inert
gas.
2
1
1
2
A
4
3
6
5
B
7
C
Summary of Contents for TTK 600
Page 2: ......
Page 74: ...Appendix B Sample Chamber Dimensions 74 D52IB001EN G Appendix B Sample Chamber Dimensions ...
Page 75: ...Appendix C Declaration of Conformity D52IB001EN G 75 Appendix C Declaration of Conformity ...
Page 77: ...Appendix D Spare Parts and Accessories D52IB001EN G 77 176383 COOLING MODE SWITCHING VALVE ...