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                                                                            Chapter 3:  Operation, Page 28 

 

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3.7 Trend 

A trend of the sulfur and density results can be displayed by pressing the TREND button on the Main Screen. 
The sulfur concentration is displayed as a solid trend line while the density is displayed as a dotted trend line. 
The time period that is displayed is dependent on the Count Time to provide optimum detail.  
 

 

 
If the Count Time is 59 seconds or less the Trend is updated every 5 seconds for the previous 5 minutes. 
 
If the Count Time is between 59 and 121 seconds, the Trend is updated every 30 seconds for the previous 30 
minutes. 
 
If the Count Time is 121 seconds or more, the Trend is updated every 60 seconds for the previous 60 minutes. 
 
The Trend is updated regardless of whether the analyzer is running or stopped. The vertical scale of the Trend 
is the same as the scale set for the 4-20mA outputs for sulfur and density. The units are always % for sulfur and 
gm/cc for density regardless of what units are selected for density on the Main Screen. 

 
 

3.8 Verification Utility 

The AMETEK ASOMA Model 682T-HP analyzer contains a utility for internal verification of the 
measurement system. This utility may be used to verify that the detector and X-ray tube yield the same results 
as when the system was last calibrated. The system achieves this by comparing the current measurements from 
two internal standards measured through the empty flow cell with historical results under the same conditions. 
The procedure is initiated by pushing the Capture button when the system is under Local control and the flow 
cell is empty. 
 
1.

 

Turn the Control switch on the door to the LOCAL position to stop any automatic analysis. Close the door 
of the analyzer if it is not already closed. This will maintain thermal stability in the electronics during the 
verification. 

 

 

 
2.

 

Turn the Valve Switch on the door to the CLOSED position to prevent any accidental flow from the 
process. If there are manual valves controlling flow to the analyzer, close these to prevent any accidental 
flow from the process. 

Summary of Contents for 682T-HP

Page 1: ...Model 682T HP Sulfur Analyzer ATEX Zone 2 pzc User Manual 9000 223 VE REV C...

Page 2: ...682T HP Sulfur Analyzer For ATEX Zone 2 Locations USER MANUAL June 2019 2019 by AMETEK Inc 150 Freeport Road Pittsburgh PA 15238 Ph 412 828 9040 Fax 403 826 0399 www ametekpi com R PROCESS INSTRUMENTS...

Page 3: ...1 5 Notice of Operation 9 2 INSTALLATION 10 2 1 Site Selection 10 2 3 Utility Requirements 11 2 3 1 Gas Supply Specifications 11 2 3 2 Electrical 11 2 3 3 Signal Connections 13 2 3 4 Process Connecti...

Page 4: ...ple Presentation 33 4 3 CAPTURE Procedure Using Pushbutton Control 34 4 3 1 Modifying Sample Data 36 4 3 2 Changing the Calibration Method 38 4 3 3 Saving the Calibration 38 4 3 4 Initializing CalSet...

Page 5: ...8 5 4 Leak Sensor 49 5 5 Inputs Outputs 50 5 6 AC Line Filter 51 5 7 Head Mounting Plate 51 5 8 XRT XRA Head and Detector 51 5 9 Fan 52 5 10 Sample Aperture Window 52 5 11 Flow Cell 52 5 12 Flow Cell...

Page 6: ...Corrections 79 6 14 Density Corrections 80 6 15 Port Setup 80 6 16 Transfer Data 81 6 17 Temperatures 83 7 ALARMS I O CONFIGURATION 85 7 1 General Alarm Error Messages 85 7 1 1 Leak in Cabinet 86 7 1...

Page 7: ...Aperture Window Replacement 96 10 1 3 Flow Cell Window Assembly 98 10 1 4 Replacing Parts 99 10 2 Controller Update 99 10 2 1 Updating the PLC Software 99 10 2 2 Updating the TP 177B Software 100 WARR...

Page 8: ...onents of the analyzer Section 6 Utilities Describes how to use standard software features of the analyzer Section 7 Alarms I O Configuration Describes the available alarms and explains how to configu...

Page 9: ...on System EPS also known as the Cabinet Purge is included with the analyzer to allow the system to be operated in a hazardous environment This system relies on an initial rapid cabinet purge and then...

Page 10: ...the process fluid shall not exceed 2 V V and the Upper Explosive Limit shall not exceed 80 3 The equipment shall be installed so the risk of mechanical impact on the display is low To avoid electrosta...

Page 11: ...r stainless steel tube with proprietary windows specially coated to eliminate erosion These windows positioned opposite each other and aligned with the source and detector are highly transmissive to X...

Page 12: ...r can be tied in to plant wide automation systems to provide real time strategic measurements Among the key features of the analyzer are a fully integrated Densitometer optional automatic density comp...

Page 13: ...lines terminals blending Sample stream temperatures up to 464 F 240 C with high temperature option Proprietary window in flowcell can withstand pressures In excess of 500 psig 35 bar Certified to indu...

Page 14: ...ll X ray Tube Head Detector Head and related electronics The signal from the Detector Head is fed to the Controller where it is corrected for density and applied in the calibration equation to yield t...

Page 15: ...oring the system uses various sensors and user definable limits The second function is to schedule and control the analysis sequence The third function is to handle communication with operators and ot...

Page 16: ...e density of the measured fluid NOTE The factory installed densitometer is an option However if the analyzer is ordered without the densitometer the customer must supply a 4 20 mA density signal to th...

Page 17: ...y 62 inches 158 cm high and 47 inches 120cm wide Be aware that the analyzer is designed to have the process stream connected to the top and bottom flanges standard connection is 1 600 ANSI RF Adequate...

Page 18: ...otective gas is connected to a 3 8 NPT entry at the purge controller Refer to the Customer Drawings Except for cylinder supplied gases the point at which the protective gas enters the supply duct s sh...

Page 19: ...should be consistently maintained to 90 nominal VAC on the low end and 110 nominal VAC on the high end The AC voltage input can be 230 VAC single phase 50 Hz 1600 watts maximum power MAINS supply cor...

Page 20: ...conduit hubs Refer to the Custoemr Drawings and Wiring Diagrams supplied with your analyzer for connection details Signal cables need to be connected to the analyzer through cable glands or conduit hu...

Page 21: ...ample probe may be necessary to ensure that a representative sample of the process flows through the analyzer The sample flow should be more than 4 liters per minute 1 gallon per minute through the an...

Page 22: ...should be green 6 Turn the Purge Control Valve On This will start the High Purge Flow and the Purging indicator should turn amber If the Purging indicator remains black the flow through the outlet val...

Page 23: ...Touch Panel When the Local Remote Control Switch is in the LOCAL position any signals from a remote location to run stop and change calibrations are ignored When the Local Remote Control Switch is in...

Page 24: ...on is pushed 5 The door switch is in REMOTE and the REMOTE RUN signal is inactive 6 The system was not running when last powered off unless condition 2 above is now true 7 The door switch changes from...

Page 25: ...Chapter 3 Operation Page 18 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2...

Page 26: ...d when the Update time has counted down to zero If Repeat Analysis is enabled the Update time will then reset to the Count time and start the countdown to the next result update Several parameters may...

Page 27: ...ol of the RUN and STOP and CalSet selection is performed remotely or locally If you want to control the system from the Touch Panel move the switch to the LOCAL position 4 Apply Power The Touch Panel...

Page 28: ...to Section 6 7 Setup 4 20mA Outputs for details 12 Set the Out of Bounds Limits Ensure that the upper and lower bound limits for the sulfur results are set appropriately Refer to Section 6 8 Setup Bo...

Page 29: ...sword is entered the password level is set to 0 until an appropriate password is entered again The following is compiled information from the Siemens TP 170B and TP 177B manuals Overview If operator c...

Page 30: ...the operating unit is not operated within the period of time configured logout time the current password level is automatically reset to 0 For the logoff time you can use values of 0 to 60 minutes The...

Page 31: ...UTIL Screen you may select the Count Time Pause and configure any other parameters displayed Access is allowed for Operator2 Level 2 or higher password For more details refer to Section 6 Utility Scr...

Page 32: ...Limited modifications can be made to items on the Main Screen You will need to log in with an appropriate password before changes are allowed The items you may change are the Product ID and the densit...

Page 33: ...used in calculating the result remain set in gm cc Access is allowed for Operator2 Level 2 or higher password The option for reference density shows the calculated density in gm cc based on the theor...

Page 34: ...screen with just the sulfur and density can be selected from a button on the main screen or set to automatically display when the Local Remote door switch is turned to Remote refer to section 6 5 Con...

Page 35: ...always for sulfur and gm cc for density regardless of what units are selected for density on the Main Screen 3 8 Verification Utility The AMETEK ASOMA Model 682T HP analyzer contains a utility for in...

Page 36: ...ity meter if included The system will warn that the density is low and X rays will be turned off This is desirable since the X rays would temporarily saturate the detector if they were transmitted thr...

Page 37: ...arm if the results are outside expected limits Note the verification procedure may be repeated as many times as desired by following steps 4 through 6 7 When you are satisfied with the verification re...

Page 38: ...cates that the X ray Tube is on and that it is NOT safe to swing the XRT XRA Head out An interlock is provided to shut off X rays if the XRT XRA Head is removed from the flow cell X ray Warning Light...

Page 39: ...applications To change calibrations make sure the Local Remote door switch is in the LOCAL position and logon with the appropriate password Select the CalSet from the drop down menu in the Main Scree...

Page 40: ...amples must be about 1 2 gallon 2 liters each to fill the Densitometer and the flow cell The Exponent method requires a minimum of 3 samples while the Hyperbolic and Alpha methods require a minimum of...

Page 41: ...you may follow the CAPTURE procedure while the process stream is flowing or trapped in the analyzer Pull a grab sample from the Manual Drain Valve while the analyzer is measuring and mark it for inde...

Page 42: ...and select the UTIL Screen to set the COUNT TIME 2 Press the Capture Button on the front door It is not necessary to stop the analyzer if it is already running automatic analysis The automatic analysi...

Page 43: ...ecords available for every CalSet View the records and note which ones you want to overwrite HINT Press the GIVEN CALC button for a quick view of all the enabled records since the last recalculation 4...

Page 44: ...11 Press the RECALC button The analyzer will calculate the best fit in about 40 seconds 12 Press the GIVEN CALC button to inspect the results of the calibration Refer to Section 4 4 Calibration Fit fo...

Page 45: ...previous sections after entering the calibration level password 4 3 4 Initializing CalSet Records You may initialize all the records in a particular CalSet by using the Transfer to All Records functio...

Page 46: ...tion 4 3 CAPTURE Procedure Using Pushbutton Control 5 When the Sample Table Screen is displayed find the Pull down menu near the top of the screen under the title Data Record Name There are 8 empty re...

Page 47: ...bout where the records will be initially stored either in the Capture Buffer or the Re Calc Records Captures performed using the pushbutton on the front door will always be placed in the Capture Buffe...

Page 48: ...nge of sulfur and there is not much variation in the sample density the Exponent method is recommended EXAMPLE OF A CALIBRATION FIT WITH AN EXPONENT DENSITY CORRECTION Element S Std Error of Estimate...

Page 49: ...ion in the samples to produce a valid Alpha coefficient If you have a set of samples with varying densities and sulfur to span the expected process conditions and the range of sulfur is small the Alph...

Page 50: ...it will not produce as good a fit as the Alpha method if the sample density varies by a large amount If you have a set of samples with a large sulfur range and similar densities the Hyperbolic method...

Page 51: ...standard error may mean one or more of the samples should not be included or a different method should be used Some typical problems that lead to calibration errors are 1 Insufficient range of sample...

Page 52: ...cted as the error involved in the counting statistics cannot be removed from the system Thus at best it can be expected that 68 of the measurements of a peak will come within this calculated one sigma...

Page 53: ...gma for the sample Since CPS is the count rate and not the total counts for the sample we must divide the CPS by the Count Time before taking a square root of the result For a 4 second Count Time CPS...

Page 54: ...urrent typ 2 05 1 23A at 120 230Vac Power factor typ 0 56 0 47 at 120 230Vac AC Inrush current typ 3A peak DC Input not allowed Efficiency typ 89 4 90 2 at 120 230Vac Losses typ 14 5 13 2W at 120 230V...

Page 55: ...10 mbar 4 wc Indicators Alarms Alarm Red Indicates Low Pressure Green Indicates Pressure OK Low Pressure Sensor Alarm setting 1 wc 2 5 mbar Purging Indicator turns Yellow when purge flow is detected...

Page 56: ...Chapter 5 Hardware Details Page 49 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2...

Page 57: ...ut signals are isolated with intrinsic safety barriers Refer to your drawing package for connection details 4 20mA outputs are connected to the I O signal terminal block or intrinsic safety barriers T...

Page 58: ...rated when the XRT XRA Head is not shielded by the Flow Cell and Detector Despite this interlock it is good practice to turn off power to the analyzer so there is no chance for X ray generation while...

Page 59: ...ns 5 10 Sample Aperture Window The sample aperture window also called the safety window is a sheet of 1 4 mil Polypropylene film covering the sample aperture on both the XRT Head and detector It must...

Page 60: ...tional The Densitometer or a Customer supplied analog density input is crucial to providing accurate results from the analyzer Please refer to the manual supplied with the Densitometer for operation d...

Page 61: ...ater may be supplied inside the enclosure Please refer to the manual supplied with the heater for operation details The heater is nominally set to control the cabinet temperature above 70 F 21 C 5 15...

Page 62: ...s for recalibrating the touch sensitivity of the panel are copied here for convenience 1 Cycle the power and when the Loader window comes up press the Control Panel button 2 When the Control Panel app...

Page 63: ...PLC 5 16 1 PLC Specifications CPU Order Number 6ES7 215 1BG400 0XB0 5 16 2 Battery Replacement The PLC is provided with a battery cartridge to extend the data retention time up to 200 days This batte...

Page 64: ...n the Manual Drain Valve while the process is flowing to grab a sample for independent analysis in which case care must be exercised so that the process fluid does not spill The Manual Sample Valve at...

Page 65: ...Several types of intrinsically safe switching amplifiers may be provided to safely connect signals from a hazardous location to the analyzer Please follow manufacturer s recommendations for connecting...

Page 66: ...Chapter 5 Hardware Details Page 59 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2...

Page 67: ...Chapter 5 Hardware Details Page 60 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2...

Page 68: ...Chapter 5 Hardware Details Page 61 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2 Digital outputs DP 0102...

Page 69: ...Chapter 5 Hardware Details Page 62 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2 Digital inputs DP 0094...

Page 70: ...Chapter 5 Hardware Details Page 63 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2...

Page 71: ...Chapter 5 Hardware Details Page 64 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2 RS485 isolator DP 0099...

Page 72: ...Chapter 5 Hardware Details Page 65 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2...

Page 73: ...1 1 ON SW2 1 OFF SW3 1 OFF 250 between A and B Hazardous Area SW1 2 ON SW2 2 OFF SW3 2 OFF RS485 Safe Area No Termination Resistor SW1 3 ON SW2 3 ON SW3 3 ON Unconnected Pin 6 SUB D Connector SW1 4 ON...

Page 74: ...W1 3 ON SW2 3 ON SW3 3 ON Unconnected Pin 6 SUB D Connector SW1 4 ON SW2 4 OFF SW3 4 OFF RS485 Hazardous Area 9600 Baud SW2 5 ON SW3 5 ON 11 total bits SW2 6 OFF SW3 6 ON SW2 7 OFF SW3 7 OFF SW2 8 OFF...

Page 75: ...Chapter 5 Hardware Details Page 68 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2...

Page 76: ...Chapter 5 Hardware Details Page 69 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2...

Page 77: ...ll require an appropriate password level 6 1 Valve Setup The analyzer can control an inlet and outlet valve to block off or allow flow from the connected process stream This control is enabled only if...

Page 78: ...the last calibration sample has been drained from the analyzer The Acquisition delay is the number of seconds the analyzer will delay before starting the first measurement when put into the RUN condit...

Page 79: ...ed after the START signal is received while the analyzer is in REMOTE operation This allows product some time to flow through the analyzer before the first analysis is started Subsequent analyses will...

Page 80: ...and Operator levels Press the PassWords button on the UTIL screen and log on with the Administrator Level 9 password Tap the password field you wish to modify and enter the new text on the alphanumer...

Page 81: ...e warning limits are all upper limits The warning limit cannot be set above the alarm limit Each of the monitored temperatures and their respective alarm limits are shown here Cabinet 45 C X ray Tube...

Page 82: ...s been off for more than 200 days or does not match the local time the PLC clock can be set from the UTIL screen by tapping the Set PLC CLK button Access is allowed for Operator6 Level 6 or higher pas...

Page 83: ...20mA output for density is identical regardless of which CalSet is active but the 4 20mA output for sulfur can be set independently for each CalSet To access the analog output range for each CalSet pr...

Page 84: ...tput a digital signal when the sulfur results exceed configured limits You may configure these limits through the UTIL screen by pressing the SETUP 4 20mA BOUNDS button Access is allowed for Operator6...

Page 85: ...cording to how much delay you want after each analysis before the start of the next analysis This time can be any value between 0 1 second and 320 seconds Access is allowed for Operator6 Level 6 or hi...

Page 86: ...0 303370787 1 2 1 3 1 14 1 3 1 2 1 17 User Offset 0 9 1 3 1 05 0 773033708 1 5 1 2 1 23 0 9 0 8 1 05 0 8 1 1 1 02 1 1 1 1 11 1 0 9 1 08 You may enter User Corrections for any CalSet by selecting the U...

Page 87: ...put but will not affect the calculated sulfur result If you are checking the mathematics of the calibration equation be sure to use the uncorrected density for your calculations The Data Records Captu...

Page 88: ...ilities A MMC needs to be installed to store the data Refer to section 10 2 3 Updating the TP 177B Software for instructions to install the MMC A card reader is required to read the data after the car...

Page 89: ...ed text file CSV file and can be found in the DAT folder or directory Example If the FILENAME is myDATA and the FILE NUMBER is 004 and you select CALSET0 and EXPORT REC 0 then all the calibration reco...

Page 90: ...T folder or directory If the file name and number specified is identical to a file name on the MMC while logging is enabled the system will automatically overwrite the existing file in the LOG folder...

Page 91: ...rature may be displayed from a customer supplied 4 20mA signal if desired The external temperature may be used instead of the Flow Cell temperature to calculate the reference density correction by pre...

Page 92: ...contact to open when power is on 1 Leak in cabinet 2 Cabinet X ray or Flow Cell temperature exceeds maximum 3 Zero Counts detected or Counts exceeding maximum 4 Purge Failure 5 System discrete input a...

Page 93: ...gh an increase in the Flow Cell or Cabinet temperatures may contribute to a Head temperature alarm Verify that the process stream is not over temperature Make sure that the area is safe to open the an...

Page 94: ...s above the minimum Check connections and try cycling power If nothing seems obvious contact AMETEK s service department for assistance 7 1 6 I O Error If the Touch Panel Display shows symbols instead...

Page 95: ...provided to indicate a Valid Result has been updated This signal will output voltage or close a contact for 3 seconds after a valid result has been sent to the analog outputs One digital signal may b...

Page 96: ...analysis during remote operation The two inputs allow binary selection of 3 pre configured Count Times If no inputs are set the Count Time will remain unchanged from the last valid Count Time Please...

Page 97: ...tures Page 90 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2 8 SPECIFICATIONS CERTIFICATION 8 1 Specifications When the optional heater is installed in the enclosure the following additio...

Page 98: ...ASOMA MODEL 682T HP General setup The AMETEK Model 682T HP can be considered to be a SLAVE device with default address 200 changeable from the local display PORT SETUP screen Transmission baud rate T...

Page 99: ...ounds 8 0x0100 O40001 Status Word RESERVED BIT reserved for future use 9 0x0200 O40001 Status Word RESERVED BIT reserved for future use 10 0x0400 O40001 Status Word RESERVED BIT reserved for future us...

Page 100: ...a n a O40009 040010 Floating Point G CC DENSITY USER CORRECTED n a n a O40011 040012 Floating Point SECONDS COUNT TIME n a n a O40013 040014 Floating Point C FLOW CELL n a n a O40015 040016 Floating...

Page 101: ...Receive parity error 7 Receive CRC error 8 Illegal function request function not supported 9 Illegal memory address in request 10 Slave function not enabled 9 2 Serial Output Option Serial output RS 4...

Page 102: ...left to right Product ID CPS Density Corrected Density Count Time C at the Flow Cell C inside the cabinet C at the X ray tube and the Date The data from each analysis update corresponds to the columns...

Page 103: ...an remove either the XRT head or the Detector by removing the 8 6 32 x 1 2 flat Phillips screws attaching the angle brackets on the top and bottom of the head or detector 10 1 2 Sample Aperture Window...

Page 104: ...nd standoff with a short threaded screw emerging from one end Carefully thread the tool into one of the two holes in the window holder ring Thread it in all the way Pull steadily on the tool straight...

Page 105: ...window should draw up tight and wrinkle free 5 Replace the window ring Use the window removal tool to carefully place the window ring back in the aperture Make sure that the O ring is not pinched up a...

Page 106: ...ram to S7 1200 series PLC with SD Card To insert a memory card open the top CPU door and insert the memory card in the slot A push push type connector allows for easy insertion and removal The memory...

Page 107: ...ansferred to internal load memory The CPU then goes to the start up mode RUN or STOP that you configured for the project Note You must remove the transfer card before setting the CPU to RUN mode 10 2...

Page 108: ...ck of the HMI Do not insert in the System slot The card should be oriented with the label to the right and the notch to the bottom when looking at the back of the HMI as pictured Push in until it latc...

Page 109: ...ge 102 M o d e l 6 8 2 T H P U S E R M A N U A L A T E X Z o n e 2 Select the row with the storage card when it appears in the window Press the Next button Previous backup files on the SD card if any...

Page 110: ...ame is normally the current date You can change this if desired or leave it alone Press the Create button Wait about 5 minutes Press OK when the Backup success window is displayed Press the X in the u...

Page 111: ...can remain in the Data slot or be removed if desired Restore Follow the initial steps of the Backup procedure except select the Restore tab instead of Backup Select the row with the storage card when...

Page 112: ...T E X Z o n e 2 Wait for transfer about 3 minutes Don t worry when the screen goes blank A normal boot up follows shortly after If you watch carefully you will catch the restore success message just b...

Page 113: ...cations Module 1 1000 757 JE HMI Touchscreen 1 1000 904 JE Battery 3V CR1025 1 1000 762 JE SIMATIC HMI Memory Card 1 1000 851 JE Memory Card 24 MB for Siemens 1215C PLC OTHER PROBLEMS If you have a pr...

Page 114: ...ch case within 7 days after discovery of the defect If Buyer does not provide such timely notification it shall not be entitled to reject Products including software firmware or Services and Seller sh...

Page 115: ...DENTS TO YOUR REGULATORY AGENCY Any failure of or damage to the shielding system requires you to suspend operation of the instrument until corrective action can be taken by a person licensed to perfor...

Page 116: ...adiation levels for instruments at typical energy levels A factory survey of your instrument is included with the shipping documents Keep this survey on file Remember that turning off the power immedi...

Page 117: ...ad 5 0 1 Left Side of Detector 6 0 1 Top Outside Enclosure 7 0 1 Right Outside Enclosure 8 0 1 Bottom Outside Enclosure 9 0 1 Left Outside Enclosure 10 0 1 Front Outside Enclosure 11 0 1 Rear Outside...

Page 118: ...company radiation safety officer or equivalent must certify that each employee has been trained in the safe operation of the instrument by reading and understanding the safety sections of the manuals...

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