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53

Appendix B

Material Safety Data Sheet: Isopropyl Alcohol

1 - PRODUCT IDENTIFICATION

Product Name.......................  Isopropyl Alcohol
Formula ................................ CH3CHOHCH3
Formula Wt ..........................  60.10
CAS No................................  67-63-0
NIOSH/RTECS No. .............  NT805000
Common Synonyms

.............

2-Propanol; Isopropanol; SEC-Propyl
Alcohol; IPA; Dimethylcarbinol

Product Codes ...................... U298, 5082, 9080
Effective............................... 09/03/86

Revision #02

Precautionary Labeling (Baker Saf-T-Data

TM

System)

Health...................................  1 Slight
Flammability ........................  3 Severe (Flammable)
Reactivity .............................  1 Slight
Contact .................................  1 Slight

Hazard Ratings are 0 to 4 (0 = No Hazard; 4 = Extreme Hazard).

Laboratory Protective Equipment:

Safety glasses; lab coat; vent hood; proper gloves; Class B extinguisher

Precautionary Label Statements:

Warning: Flammable
Causes Irritation.
Harmful if Swallowed or Inhaled.
Keep Away From Heat, Sparks, Flame.
Avoid Contact With Eyes, Skin, Clothing.
Avoid Breathing Vapor. Keep in Tightly Closed Container. Use With

Adequate Ventilation.

Wash Thoroughly After Handling.
In Case of Fire, use Alcohol Foam, Dry Chemical, Carbon Dioxide - Water

May Be Ineffective.

Flush Spill Area With Water Spray.
SAF-T-DATA

TM

Storage Color Code: Red (Flammable)

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Содержание 8525

Страница 1: ...Indoor Air Quality P TRAK Ultrafine Particle Counter Model 8525 TRAKPRO Data Analysis Software enclosed Operation and Service Manual 1980380 Revision K February 2009 ENERGY AND COMFORT ...

Страница 2: ......

Страница 3: ...y 2009 SHIP TO MAIL TO TSI Incorporated 500 Cardigan Road Shoreview MN 55126 3996 USA U S Technical Support 800 874 2811 651 490 2811 Fax 651 490 3824 E mail technical service tsi com E mail address answers tsi com Website http www tsi com INTERNATIONAL Technical Support 001 651 490 2811 Fax 001 651 490 3824 E mail technical service tsi com ENERGY AND COMFORT ...

Страница 4: ...ject to the LIMITATIONS stated herein NO OTHER EXPRESS OR IMPLIED WARRANTY OF FITNESS FOR PARTICULAR PURPOSE OR MERCHANTABILITY IS MADE TO THE EXTENT PERMITTED BY LAW THE EXCLUSIVE REMEDY OF THE USER OR BUYER AND THE LIMIT OF SELLER S LIABILITY FOR ANY AND ALL LOSSES INJURIES OR DAMAGES CONCERNING THE GOODS INCLUDING CLAIMS BASED ON CONTRACT NEGLIGENCE TORT STRICT LIABILITY OR OTHERWISE SHALL BE T...

Страница 5: ... Inlet Screen Assembly Sample Tube and Telescoping Probe to the Instrument 14 Instrument Software and Communications Setup 16 Setting up TRAKPRO Data Analysis Software 16 Connecting the P TRAK Particle Counter to the Computer 16 Setting up the Communications Port 16 Connecting the Optional Portable Printer 17 3 OPERATION 19 Overview 19 Turning the Instrument On 19 Tilting the Instrument 19 Daily Z...

Страница 6: ... Schedule 41 Daily Zero Check 41 Recharging the Alcohol Wick 42 Alcohol Cartridge 42 Changing the Alcohol Wick 42 Removing the Wick from the Cartridge 43 Re assembling the Alcohol Cartridge 44 Cleaning Inlet Screen Assembly 45 5 TROUBLESHOOTING 47 A SPECIFICATIONS 51 B MATERIAL SAFETY DATA SHEET ISOPROPYL ALCOHOL53 To obtain any of the listed Application Notes contact TSI at U S 800 874 2811 651 4...

Страница 7: ...PRODUCT IS IN COMPLETE COMPLIANCE WITH 21 CFR 1040 10 AND 1040 11 There are no user serviceable parts inside this instrument Performing services other than those described in this manual may result in exposure to harmful invisible laser radiation A warning label like the one shown below is affixed to the internal laser device DANGER INVISIBLE LASER RADIATION WHEN OPEN AVOID DIRECT EXPOSURE TO BEAM...

Страница 8: ...vi Safety Information ...

Страница 9: ...components Contact TSI immediately if anything is missing or damaged Figure 1 1 Model 8525 P TRAK Ultrafine Particle Counter With Inlet Probe Assembly Battery Pack and Batteries Quantity Item Description Part Model Reference 1 P TRAK Ultrafine Particle Counter N A 1 1 Probe assembly consisting of telescoping probe sample tube and inlet screen assembly 801622 801615 801616 2 1 Battery holder 801623...

Страница 10: ... with Storage Cap Alcohol Cartridge Alcohol Bottles and Shoulder Strap Quantity Item Description Part Model Reference 1 Alcohol fill capsule and storage cap 1083070 1 1 Alcohol cartridge 801624 2 16 30 ml alcohol bottles 1 shown 2918011 3 2 1 3 ...

Страница 11: ...sh Storage Bag with Spare Wicks Computer Cable Zero Filters and DB9 DB25 Adapter Quantity Item Description Part Model Reference 1 Mesh bag N A 1 2 Spare wick kit N A 2 1 Computer cable RJ45 DB9 800563 3 2 HEPA zero filter with adapter 801625 4 1 2 3 4 ...

Страница 12: ...eference 1 Calibration Certificate N A 1 1 Operation and Service Manual 1980380 2 1 TRAKPRO Software 1090014 3 Optional Accessories The following table lists optional accessories available for the P TRAK Ultrafine Particle Counter Quantity Item Description 1 AC adapter for P TRAK particle counter 115V only 1 Portable printer 1 2 3 ...

Страница 13: ...ement Parts The following items may be purchased as spare or replacement parts Item Description Part Number Alcohol wicks with screens Pkg of 10 8023 Tubing sample 4 x 1 8 Tygon 801615 Inlet screen assembly 801616 Alcohol 16 qty 30 ml bottles 2918011 ...

Страница 14: ......

Страница 15: ...ttery polarity as marked on the inside of the battery holder Remove the battery compartment door by pressing in and pulling out on the two locking tabs Next install the battery pack battery side down into the battery compartment as shown in Figure 2 1 putting the top of the pack the side with the two contacts extending from the body of the pack down first and snapping the rest of the pack in place...

Страница 16: ...dapter the batteries if installed will be bypassed The AC adapter will not charge the batteries The P TRAK particle counter has an internal non user accessible battery that is used for battery back up of logged data when the instrument is turned off Removing changing the alkaline batteries or disconnecting the AC adapter will not cause data to be lost This backup battery will last for years TSI wi...

Страница 17: ...ohol at a rate of about 1 ml per hour The alcohol is used to grow microscopic particles in the air into larger droplets that are easier to detect and count Refer to the TSI web site for details on how the P TRAK particle counter works www tsi com The isopropyl alcohol that is required to properly operate the P TRAK particle counter must be very high purity reagent grade alcohol Isopropyl alcohol t...

Страница 18: ...psule is located in the P TRAK carrying case The alcohol cartridge will also be either in the P TRAK cartridge cavity or in the alcohol fill capsule whichever one is not holding the storage cap The storage cap should be either sealing the alcohol fill capsule or inserted into the P TRAK cartridge cavity Filling the Alcohol Fill Capsule 1 Turn the P TRAK particle counter off 2 Open the alcohol fill...

Страница 19: ...o the capsule Figure 2 4 Alcohol Fill Capsule 4 Squeeze alcohol into the alcohol fill capsule until the liquid level is even with the scribed fill line near the base Figure 2 4 Recap the alcohol bottle 5 Make certain the alcohol cartridge is clean Insert the alcohol cartridge into the alcohol fill capsule by aligning the groove with the pin and turning 1 8 turn clockwise until it locks into place ...

Страница 20: ...into the capsule Stop when excess alcohol is no longer dripping It is not necessary to wait until the outside surface of the alcohol cartridge is dry 2 Insert the cartridge into the cartridge cavity on the P TRAK particle counter It should slide in easily with little effort Do not force it Align the tab on the alcohol cartridge with the corresponding tab on the P TRAK particle counter located just...

Страница 21: ...in the alcohol fill capsule The alcohol fill capsule is designed to be a safe transportation and storage container for alcohol The alcohol cartridge can be left soaking in alcohol indefinitely Also install the storage cap into the cartridge cavity to prevent dirt or lint from getting inside the P TRAK particle counter 3 Never transport or store the P TRAK particle counter with the alcohol cartridg...

Страница 22: ...ge particles and fibers from entering the instrument and plugging the internal fittings Do not operate the P TRAK particle counter without the inlet screen assembly in place To attach the sampling assembly 1 Make sure the quick connect fitting is in the unlocked position If the fitting is locked the sampling tube will not be able to be inserted into the instrument To unlock the fitting press up on...

Страница 23: ...nd safe keeping attach the telescoping probe to either side of the instrument Slide it in lengthwise along the instrument beginning at the back of the instrument the alcohol wick end until it stops do not force it See Figure 2 8 Figure 2 8 Slide Telescoping Probe onto Instrument Case ...

Страница 24: ...TRAK particle counter comes equipped with an RS 232 cable and a 25 pin to 9 pin serial cable adapter One end of the cable is a 25 pin D subminiature connector labeled COMPUTER the other end is an RJ 45 modular connector that connects with the P TRAK communications port Serial port connectors always have pins male on the computer side 1 Locate an available RS 232 serial port on your computer for ex...

Страница 25: ... looking for an attached P TRAK particle counter 6 Select OK to accept the setup or Cancel to discard the changes Connecting the Optional Portable Printer To connect the portable printer to the P TRAK particle counter do the following 1 Ensure that the P TRAK particle counter and printer are off 2 Locate the printer interface cable and connect the 9 pin end labeled PRINTER to the printer and the o...

Страница 26: ...Chapter 2 18 ...

Страница 27: ...store these readings in the instrument memory Data files may be downloaded to a computer for later analysis using TRAKPRO software Turning the Instrument On Press the ON OFF switch located at the back of the instrument and hold for 2 to 3 seconds to turn on the P TRAK particle counter The P TRAK particle counter immediately begins a warm up countdown sequence which takes about 60 seconds During th...

Страница 28: ...ary loss of performance To avoid this problem please observe the following cautions Do not tilt the instrument up into a vertical position to observe the display If the instrument is tilted for more than 4 seconds a tilt error message will be displayed the beeper will sound the displayed particle concentration will blank out and the pump will be stopped After restoring the instrument to level oper...

Страница 29: ...the instrument does not go to zero please refer to Chapter 5 Troubleshooting for more information The Daily Zero Check cannot be performed when the telescoping sample probe is attached to the instrument The telescoping joints will cause a small number of particles to be sampled and will invalidate the zero check 5 Remove the zero filter Attach the sample tube and telescoping sample probe as desire...

Страница 30: ...Description 1 Particle concentration in units of particles per cubic centimeter 2 Sample mode Used for capturing single data points 3 Setup mode Used for reviewing logged data single data points statistics Used for changing date time log interval backlight interval audio function Used for clearing memory 4 Log mode recording data files Displays current log mode 1 2 or 3 Used for changing mode and ...

Страница 31: ... fluctuate significantly When making a measurement therefore it is often desirable to dampen out these fluctuations with a short averaging period Recording and Saving a Single Data Point When you press with the Sample mode highlighted the P TRAK particle counter begins a countdown During these 10 seconds it is taking an average reading of the particle concentration At the end of the averaging peri...

Страница 32: ...on 01 If desired you may change the Location name up to a maximum of 15 alpha numeric characters When done editing press to exit and save The instrument will return to the Survey mode Setup Mode The Setup mode gives you access to a wide range of options for reviewing data examining statistics and changing operational parameters When SETUP is selected and is pressed the program opens the Setup menu...

Страница 33: ...memory A sample screen is shown below LOGGED TEST STATS TEST 3 START 08 23 11 02 2008 STOP 09 45 11 02 2008 MIN 3753 09 35 00 MAX 3753 09 35 05 AVG 4052 PRESS WHEN DONE Figure 3 6 Logged Test Statistics Ref Description 1 Test number not user adjustable 2 Start time and date 3 Stop time and date 4 Minimum value during test along with time at which minimum occurred 5 Maximum value during test along ...

Страница 34: ...ew the current logging interval used during LOG MODE 1 see Log Mode 2 and 3 section later in this chapter for more information about data logging It also allows you to adjust the log interval to a different value The menu screen is shown below LOG INTERVAL 01 00 MIN SEC Figure 3 8 Log Interval The default values for log intervals are set at 1 second 1 minute 5 minutes 15 minutes and 30 minutes Whe...

Страница 35: ...concentration When this feature is turned On you will hear an audio signal which will give you an indication of changing particle concentrations This feature may be particularly useful when you are attempting to detect highly localized sources of particulate in a low light condition A sample screen is shown below AUDIO OUTPUT 5600 PT CC OFF CAPTURE REFERENCE SET REFERENCE 3040 EXIT Figure 3 9 Audi...

Страница 36: ...rmat along with minutes and seconds It is very important for the P TRAK particle counter to have the time and date correctly set otherwise time and date stamping of recorded data will not be correct The time clock is set correctly at the factory for U S Central Standard Time If it requires adjustment it may be changed by selecting TIME DATE from the Setup menu The following screen is displayed TIM...

Страница 37: ...3 11 Time Date Programming with TRAKPRO Software 3 The system date and time from the computer can be transferred to the P TRAK particle counter using the arrows keys Alternately the date and time can be manually entered into the dialog box 4 Select Send to reprogram the P TRAK particle counter Backlight The BACKLIGHT option on the Setup menu allows you to adjust how long the display backlight stay...

Страница 38: ...lly erase the older data files It requires a deliberate step on your part to clear the memory Note Performing this step will erase all logged data files and or recorded single data points from the instrument memory There is no reversing this step once it is performed To clear the memory select the CLEAR MEMORY option on the Setup menu After pressing the following screen is displayed CLEAR MEMORY S...

Страница 39: ...rument memory If LOG MODE 1 was selected the following screen will be displayed 4048 PT CC MIN 4032 08 32 00 MAX 4950 09 27 00 98 MEM LOG MODE 1 TO STOP Figure 3 14 Log Mode 1 If LOG MODE 2 or 3 was selected the P TRAK particle counter may or may not begin logging immediately depending upon the setup parameters See Log Mode 2 and 3 in this chapter for more information Log Mode 2 and 3 The P TRAK p...

Страница 40: ...cted to the computer and turned on 2 Select Logging Setup from the Instrument Setup menu TRAKPRO software retrieves the current settings for Log Modes 2 and 3 from the P TRAK particle counter and displays them in the following dialog box Figure 3 15 P TRAK Particle Counter Logging Protocols 11 02 2008 11 03 2008 ...

Страница 41: ...o particle concentration Start Date Displays the start date for LOG 2 and LOG 3 modes Start Time Displays the start time for LOG 2 and LOG 3 modes Log interval Displays the log interval for LOG 2 and LOG 3 modes Test length Displays the test length for LOG 2 and LOG 3 modes Number of tests Displays the number of tests for LOG 2 and LOG 3 modes Selecting more than one test will cause the instrument...

Страница 42: ...the length for the sample If you enter a value the instrument automatically turns off when the last test is complete If you enter a blank the operator must manually stop the sample Number of tests Enter the number of tests to perform Time between tests If you have specified more than one Number of tests enter the time between tests If you enter 0 or blank the next test is started immediately after...

Страница 43: ...tocol for Log Mode 2 or 3 Log Mode 2 sample protocol features The sample protocol for Log Mode 2 is set to take unattended particle concentration readings for one day Logging takes place on 11 02 2008 The logging sample begins at 8 00 a m Logging continues for eight hours Log Mode 3 sample protocol features The sample protocol for Log Mode 3 is set up to take unattended particle concentration read...

Страница 44: ... settings for Log Modes 2 and 3 from the P TRAK particle counter and displays them as shown in the previous dialog 3 Enter the following for Log Mode 2 and 3 Setting LOG 2 LOG 3 Channels Particle Conc Particle Conc Start Date 11 02 2008 11 03 2008 Start Time 08 00 08 00 Log interval 01 00 05 00 Test length 00 08 00 00 08 00 Number of tests 1 4 Time between tests 00 00 00 00 16 00 4 Select Send The...

Страница 45: ...not set a start time the P TRAK particle counter will begin logging immediately after the is pressed This will happen no matter what is entered for the start date If you have set a test start time but no start date the P TRAK particle counter will begin at the specified time regardless of the date If you have set a start time and start date which are in the future the P TRAK pump and other interna...

Страница 46: ...ry for the single points and the logged tests filling up the memory for one type of data will have no affect on the other type The P TRAK particle counter can store approximately 470 single points It can also store approximately 1000 hours 41 days of logged tests when recording at 1 minute logging intervals the number of hours of logged tests may be more or less depending upon the logging interval...

Страница 47: ...ime before response time it takes for sample to be drawn through probe and tube Allows hands free operation attach probe to instrument case Sampling Through Inlet Screen and Sample Tube If you desire to pull a sample from a specific location or from a remote location but do not need the telescoping features of the probe it may be desirable to remove the probe and use the inlet screen and sample tu...

Страница 48: ... from clogging the sensitive internal components in the instrument If desired you may operate the P TRAK particle counter with only the inlet screen and no sampling tubing This configuration has the following features Advantages Disadvantages Cautions Most efficient least particle loss Not able to pinpoint aerosol sources Fastest response to particle concentration changes Well suited to area sampl...

Страница 49: ...r any required maintenance or service not described in this manual Maintenance Schedule Your Model 8525 P TRAK Ultrafine Particle Counter needs very little required maintenance The few items that are suggested however should be done regularly to ensure reliable operation Table 4 1 lists the factory recommended maintenance schedule Some maintenance items are suggested each time the P TRAK particle ...

Страница 50: ...d screen inside the alcohol cartridge may be changed in the field Two spare wicks and screens are included with the P TRAK particle counter Normally the wick will not need to be changed unless one of the following problems develops 1 Moisture accumulates in the wick and causes the Low Alcohol message to come on even when there is an adequate alcohol supply This may happen when the P TRAK particle ...

Страница 51: ...break it into two pieces The cartridge will snap apart exposing the end of the white Alcohol Wick See Figure 4 1 Figure 4 1 Snap Apart Cartridge After separating the two halves push the alcohol wick and screen out of the wick retainer cap from the opposite end with the wick removal tool wood dowel provided with each new alcohol wick Do not use a pencil point because bits of lead could break off Al...

Страница 52: ...cohol Cartridge Before re installing an alcohol wick you must make certain that all parts are clean Small bits of the wick or lint can cause serious problems if they get into the P TRAK particle counter Inspect the inside surfaces of the alcohol cartridge and the wick retainer cap Blow air into them if necessary to make certain that there are no dust particles present Blow air onto all surfaces of...

Страница 53: ...use and the conditions of use As a general rule of thumb whenever there is any noticeable contamination on the screen it should be cleaned To clean the inlet screen assembly do the following 1 Disconnect the inlet screen assembly from the instrument by depressing the quick connect fitting button and pulling the assembly away from the instrument 2 Unscrew the two halves of the assembly and remove t...

Страница 54: ......

Страница 55: ...mpting to perform zero with telescoping probe attached Alcohol cartridge is loose Bad HEPA filter uncommon Internal leak inside instrument very uncommon Let instrument run overnight using AC adapter with storage cap installed in P TRAK particle counter not alcohol wick This will dry out the optics and should restore proper operation Tighten assembly together hand tight only Install screen Securely...

Страница 56: ...idge Straighten tube remove obstruction Use factory supplied sample tube only Listen for pump operation Check pump flow with flowmeter should be approx 0 7 L min Operate in specified environment only Change alcohol wick inside alcohol cartridge Use only approved alcohol Return to factory for service Does not turn on Not pressing on off switch properly Batteries are dead AC adapter is not plugged i...

Страница 57: ...will normally correct itself Tilt condition may cause data logging or Sample Mode problems PUMP BLOCKED message Sample tube inlet is blocked Remove obstruction Press Enter to reset LO BATT message Low batteries AC adapter is malfunctioning or not plugged in Replace batteries Connect AC adapter LASER PROBLEM message Possible laser failure Return to factory for service ...

Страница 58: ......

Страница 59: ...to 1 000 hours of data at 1 minute intervals Storage of up to 141 separate tests Power Requirement Battery type Battery life AC adapter 6 AA Alkaline 6 hrs 70 F 21 C 9 V 1 6 A Alcohol Requirement Type Hours per charge 100 reagent grade isopropyl 8 hours at 70 F 21 C RS232 Output Baud rate 9600 8 N 1 Size 10 75 in x 5 5 in x 5 5 in 27 cm x 14 cm x 14 cm Carrying Case Size 21 in x 14 in x 8 3 in 53 ...

Страница 60: ...x A 52 Warranty Two years on workmanship and material Computer Requirements PC with Microsoft Windows 2000 or XP Windows compatible printer 5 MB hard disk space and available RS 232 serial port for downloading ...

Страница 61: ...ty 1 Slight Contact 1 Slight Hazard Ratings are 0 to 4 0 No Hazard 4 Extreme Hazard Laboratory Protective Equipment Safety glasses lab coat vent hood proper gloves Class B extinguisher Precautionary Label Statements Warning Flammable Causes Irritation Harmful if Swallowed or Inhaled Keep Away From Heat Sparks Flame Avoid Contact With Eyes Skin Clothing Avoid Breathing Vapor Keep in Tightly Closed ...

Страница 62: ...mmable Limits Upper 12 0 Lower 2 0 Fire Extinguishing Media Use alcohol foam dry chemical or carbon Dioxide water may be ineffective Special Fire Fighting Procedures Firefighters should wear proper protective equipment and self contained breathing apparatus with full facepiece operated in positive pressure mode Move containers from fire area if it can be done without risk Use water to keep fire ex...

Страница 63: ...ry edema Liquid may be irritating to skin and eyes Prolonged skin contact may result in dermatitis Eye contact may result in temporary corneal damage Ingestion may cause nausea vomiting headaches dizziness and gastrointestinal irritation Ingestion may cause central nervous system depression Target Organs Eyes skin respiratory system Medical Conditions Generally Aggravated By Exposure None identifi...

Страница 64: ...d or other non combustible absorbent material and place into container for later disposal Flush area with water J T Baker SOLUSORB solvent adsorbent is recommended for spills of this product Disposal Procedure Dispose in accordance with all applicable federal state and local environmental regulations EPA hazardous waste number D001 ignitable waste 8 PROTECTIVE EQUIPMENT Ventilation Use general or ...

Страница 65: ...ansferring liquid Keep container tightly closed Store in a cool dry well ventilated flammable liquid storage area 10 TRANSPORTATION DATA AND ADDITIONAL INFORMATION Domestic D O T Proper Shipping Name Isopropanol Hazard Class Flammable liquid UN NA UN1219 Labels Flammable liquid International I M O Proper Shipping Name Isopropanol Hazard Class 3 2 UN NA UN1219 Labels Flammable liquid ...

Страница 66: ...Appendix B 58 ...

Страница 67: ...3 491 95 21 90 E mail tsifrance tsi com Website www tsiinc fr Germany Tel 49 241 523030 E mail tsigmbh tsi com Website www tsiinc de India Tel 91 80 41132470 E mail tsi india tsi com China Tel 86 10 8260 1595 E mail tsibeijing tsi com Contact your local TSI Distributor or visit our website www tsi com for more detailed specifications P N 1980380 Rev K Copyright 2009 by TSI Incorporated Printed in ...

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