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Chapter 5 Ion Measurement (F-53,55)

5.3 Measurement Using Standard Addition Method

74

HORIBA

5.3.3 Measuring Ion Concentration in Sample Addition 1 Mode

This mode is used to obtain the ion concen-
tration of the target ion species by adding a
small amount of the sample to the standard
solution for the ion species to measure once,
thus increasing the ion concentration of the
target component, and then measuring the
change in electric potential which occurs at
that time.

1.

In the ION SETUP screen, press

↑

or

↓

key and select the MEA-

SUREMENT option.

2.

Press

←

or

→

key, select the

INCREMENTAL option and press
F4 (RETURN).

The ION Measurement screen
appears.

3.

Press

↑

or

↓

key and select the

SAMPLE ADD option.

4.

Press

←

or

→

key and select (1)

SINGLE.

5.

Press F4 (RETURN).

The SAMPLE ADDITION 1 screen
appears.

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Содержание F-52

Страница 1: ...For more information please contact us ExpotechUSA 10700 Rockley Road Houston Texas 77099 USA 281 496 0900 voice 281 496 0400 fax E mail sales expotechusa com Website www ExpotechUSA com...

Страница 2: ......

Страница 3: ...over the following Any trouble or damage attributable to actions or conditions specifically mentioned to be avoided in the operation manuals Any trouble or damage attributable to use of the meter in w...

Страница 4: ...asurement categories and FCC Warning This equipment has been tested and found to comply withthe limits for a Class A digital device pursuant to part 15 of the FCC Rules These limits are designed to pr...

Страница 5: ...to cause fire or accidents Do not disassemble or modify the meter Heat or fire may occur to cause fire or accidents CAUTION Do not use the serial communication or AC adapter in the place that may pos...

Страница 6: ...s injury CAUTION This indicates a potentially hazardous situation which if not avoided may result in minor or moderate injury It may also be used to alert unsafe practices This mark indicates the oper...

Страница 7: ...tion by the fingers not by the hard object like metal stick or rod To disconnect the electrode cable or interface cable pull them out with holding the connector part Do not pull the cable part it may...

Страница 8: ...Function 17 Chapter 2 BASIC OPERATIONS 19 2 1 Measurement Flow 19 2 2 Measurement Mode Transition for Each Model 20 2 3 Turn on the Power 24 2 3 1 At User Control OFF initial setting 24 2 3 2 At User...

Страница 9: ...5 2 1 Calibration Using Ion Standard Solution 62 5 2 2 Ion Measuring 65 5 3 Measurement Using Standard Addition Method 67 5 3 1 Measuring Ion Concentration in Standard Addition 1 Mode 68 5 3 2 Measur...

Страница 10: ...MENT F 54 55 109 8 1 Screen Operation 109 8 2 Setting Configuration 110 Chapter 9 DATA MEMORY 113 9 1 Setting Memory Type 113 9 2 Performing Data Memory 115 9 3 Calling up Memory Data 116 9 3 1 Displa...

Страница 11: ...r operation 144 11 5 2 Attachment Removal of compact flash card 144 11 5 3 Compact flash operation 145 11 5 4 Data acquisition to PC 146 11 5 5 User control function 147 11 6 Network Setting F 55 148...

Страница 12: ...3 15 1 3 Conductivity electrode maintenance 199 15 2 Troubleshooting 200 15 2 1 Error message chart 200 15 2 2 More troubleshooting 208 Chapter 16 Reference 215 16 1 pH measurement 216 16 2 Measuring...

Страница 13: ...TABLE OF CONTENTS X HORIBA...

Страница 14: ...lectrodes the battery replacement and the cautionary items 1 1 Package contents The package contents of the meter F 5X is as follows No electrode is included in the package Product Model F 52 F 53 F 5...

Страница 15: ...Displays and records cali bration and measurement dates DATE AND TIME SETUP All models Page 138 Display Screen Displays the measured val ues in a graph Effective for confirming the stability of indic...

Страница 16: ...RY All models Page 142 Copies the data to the com pact flash card COMPACT FLASH SETUP DATA COPY SETUP F 53 54 55 Page 144 Com mon opera tion Mutes the operation sound SYSTEM SETUP SOUND OFF All models...

Страница 17: ...dels Page 41 Page 42 Sets the standard solution for the pH calibration pH SETUP F1 CAL SETUP pH CALIBRATION SETUP BUFFER All models Page 44 Sets the calibration point pH SETUP F1 CAL SETUP pH CALIBRAT...

Страница 18: ...F 53 55 Page 84 Saves the electrode model type and lot in memorizing each data ION SETUP ELECTRODE MODEL ION SETUP ELECTRODE LOT F 53 55 Page 84 Page 84 Registers ion valency for linearity method meas...

Страница 19: ...T F 54 55 Page 97 Page 98 User Control function Starts up with the Operator name registered SECURITY SETUP USER MANAGEMENT ON All models Page 122 Controls the password validity SECURITY SETUP PASSWORD...

Страница 20: ...Page 106 Page 110 Data output via RS 232C After the serial cable connec tion turn on the power and either startup the PC soft ware or send commands by the Hypertermial All models Page 154 Formats the...

Страница 21: ...iption of Each Part Main Unit 1 For only F 53 54 and 55 2 For only F 55 Operation key Indication Battery cover bottom Electrode stand Serial communication terminal Analog output terminal Electrode ter...

Страница 22: ...ction key is available ON OFF key Switches the operator Turns ON or OFF the power ESC key Cancels the operation or the setting MEAS key Starts the measurement when returning to the MEASUREMENT mode MO...

Страница 23: ...temperature measured by the connected elec trode HOLD icon Without the icon instantaneous value Blinking in judging HOLD Lit HOLD External output connection icons Compact flash Displayed when the com...

Страница 24: ...and to the base by the fixing screw At the shipment the stand is already attached 3 Attach the stopper and the electrode clamp to the stand by this order At the shipment the stopper and the electrode...

Страница 25: ...s Measurement electrode G Referential electrode R In using the electrodes of pH ORP and or of Ion for those other than the referential electrode combination type connect the referential electrodes Do...

Страница 26: ...hands 2 Hold the metal part of the electrode connector and push it according to the slit by rotating clockwise Pinched injury 3 Cover the connector with the con nector cover on the straight Never rot...

Страница 27: ...ter specifications 1 Connect the adapter to the AC adapter connector located on the side part of the main unit Supply voltage range 100 200 V AC Frequency range 50 60 Hz Current rating Max 370 mA Clas...

Страница 28: ...y 1 Open the battery cover at the bottom of the meter and replace the battery 2 Adjust the clock The battery life is approximately three 3 years The battery life depends on the using conditions The bu...

Страница 29: ...the compact flash card refer to 11 5 Compact Flash Setting F 53 54 55 p 144 Ethernet output F 55 To disconnect the cable hold the connector part with a screwdriver and remove the connector cap Do not...

Страница 30: ...red data stored in the meter by the third person Therefore such setting changes as follows by the third person without authority are not available date change data memory deletion or security related...

Страница 31: ...Chapter 1 Overview 1 9 Security Function 18 HORIBA...

Страница 32: ...t to ON first reset the previous operator name to allow the other operator to use the meter To reset the operator name either press ON OFF key to make the screen to SLEEP mode or turn off the power SE...

Страница 33: ...20 HORIBA 2 2 Measurement Mode Transition for Each Model Pressing the MODE key in the Measurement screen will switch the measurement item In this section the measurement flow for each model is explai...

Страница 34: ...52 53 54 55 21 F 53 measurement mode F4 SELECT CH CH1 pH Measurement CH2 pH Measurement mV Measurement mV Measurement ION Measurement selecting AFTERCAL ION Measurement selecting AFTERCAL SETUP screen...

Страница 35: ...ASIC OPERATIONS 2 2 Measurement Mode Transition for Each Model 22 HORIBA F 54 measurement mode F4 SELECT CH CH1 COND Measurement CH2 pH Measurement mV Measurement SALT Measurement RESIST Measurement S...

Страница 36: ...nsition for Each Model F 52 53 54 55 23 F 55 measurement mode F4 SELECT CH CH1 COND Measurement CH2 pH Measurement mV Measurement SALT Measurement ION Measurement Selecting AFTERCAL RESIST Measurement...

Страница 37: ...BA 2 3 Turn on the Power Soon after the power OFF approx 4 seconds ON OFF key may be invalid 2 3 1 At User Control OFF initial setting 1 Press the ON OFF key The startup screen appears and then the SE...

Страница 38: ...pears and then the SELECT OPERATOR screen appears 2 Press or key to select the operator When the Operator is not registered register the operator newly 3 Press F4 RETURN The INPUT PASSWORD screen appe...

Страница 39: ...ck Turning the power ON displays the SETUP screen 1 Press or key to select DATE AND TIME SETUP Press the ENTER key The DATE AND TIME SETUP screen appears 2 Press or key to select the set item year dat...

Страница 40: ...age Detailed press the Detailed page mark and press the ENTER key The display jumps to the page When an error occurs the counteraction is displayed and the error indication is deleted from the screen...

Страница 41: ...Chapter 2 BASIC OPERATIONS 2 5 Navigation Function 28 HORIBA...

Страница 42: ...s Potassium Chloride in high concentration 3 33 mol L KCl When the internal solution contacts the hands or skin immediately wash it away with water If the solution gets into the eyes first wash it awa...

Страница 43: ...en pH Measurement Screen 30 HORIBA 3 2 Open pH Measurement Screen 1 Press the MODE key in any of the Measurement screens to go to the pH Measurement screen The displayed screen shows pH mea surement s...

Страница 44: ...ndard solution should be used for calibration When the measurement sample is known to be acid perform two point calibra tion pH7 and pH4 When it is known to be alkaline perform two point calibration p...

Страница 45: ...ring the calibration the filler port should be kept open The fill port configuration depends on the electrode type 5 Immerse the electrode in the bea ker with standard solution of pH7 For accurate mea...

Страница 46: ...display instantaneous value Press the ESC key The blinking interval of HOLD display is not always constant Calibration of the 2nd point After calibration of the 1st point perform calibration of the 2n...

Страница 47: ...een Maximum five points of calibration can be performed even though the number of set point is less than five The screen display shows the calibration to be performed from the solution of pH7 but any...

Страница 48: ...layed after calibra tion of the 2nd point is completed According to the displayed operation guide confirm the repeatability The electrode status is displayed To judge the electrode status refer to 3 4...

Страница 49: ...range after the repeated calibration this status display disappears Electrode status display Display Description The electrode sensitivity has deteriorated Wash the electrode Electrode sensitivity 90...

Страница 50: ...ion value stabilizes HOLD display is lit and the indication value is held This means the measure ment is completed To stop the measurement when the HOLD display is blinking press the ESC key to return...

Страница 51: ...tting The pH measurement setting is available for each CH on the F53 only Open the pH measurement SETUP screen 1 In the pH Measurement screen press F1 pH SETUP The pH SETUP screen appears When no sett...

Страница 52: ...is converted The input temperature value is used to perform temperature compensation Temperature compensation page 216 Switch temperature compensation 1 In the pH SETUP screen press or key to go to TE...

Страница 53: ...ON When ON is selected input the tem perature conversion factor Input temperature conversion factor 1 Press the ENTER key The cursor moves to the conversion factor setting part 2 Press the ENTER key a...

Страница 54: ...or key and move the cursor to ELECTRODE MODEL field 2 Press the ENTER key The ELECTRODE MODEL screen appears 3 Press and or keys to move the cursor to the electrode model to be set 4 Press the ENTER k...

Страница 55: ...or data memory will contain the electrode Lot information Setting procedure 1 In the pH SETUP screen move the cursor to the ELECTRODE LOT field by or key 2 Press the ENTER key The ELECTRODE LOT scree...

Страница 56: ...key to select OFF or ON In selecting ON pressing the ENTER key moves the cursor to the upper limit value setting field Pressing the ENTER again changes the display color of the set part enabling to i...

Страница 57: ...creen appears Pressing F1 key in the pH SETUP screen also shows the pH CALIBRATION SETUP screen To perform calibration with the standard solution other than NIST or USA specifications select Custom op...

Страница 58: ...pH value of the standard solution Pressing or key stops the value fluctuation enabling the dis play to be input mode 4 Press the CAL key and start the calibration of 1st point When the calibration is...

Страница 59: ...L POINTS field 2 Press ENTER key The display color of the set part changes Set the calibration point by or key Setting range 1 to 5 points 3 Press the ENTER key to determine the setting The display co...

Страница 60: ...en press or key to go to the CAL INTERVAL field 2 Press or key to select ON 3 Press the ENTER key The cursor moves to the interval day setting field 4 Press the ENTER key again The display color of th...

Страница 61: ...alibration by pH7 and pH4 is as follows pH7 Calibration of 1st point pH4 Calibration of 2nd point pH7 Repeatability check with the calibrated value by 1st point The result is displayed as follows Prel...

Страница 62: ...nd pH4 the measurement of the solution of pH7 is given five times and the repeatability is confirmed SIMULATOR mode Optional pH checker X 51 checks the meter only electrode check is not included JIS a...

Страница 63: ...H9 180 pH9 180 pH9 180 Cautionary points Wash the electrode with pure water before each measurement Keep the temperature gap during the measurement within 0 2 The measurement values during the periodi...

Страница 64: ...epeatability The repeatability shows the difference between maximum and minimum of the indi cation given by three times of measurements using the standard solution of pH9 See the values and above Line...

Страница 65: ...ectrode stand and a stirrer Press HOLD after the measured values completely stabilizes Pressing ESC key when the HOLD indication is lit makes the HOLD indication disappear and shows the instantaneous...

Страница 66: ...e with pure water before each measurement The measured values during periodical check are displayed according to the val ues after the calibration is cleared When the calibration range error occurs ei...

Страница 67: ...ng to the operation guide perform functional check as calibration by the standard solutions of pH7 pH4 in the following order Calibration by standard solutions pH6 865 pH4 008 Linearity check pH0 000...

Страница 68: ...tial Within regulated value 3 mV Sensitivity 99 to 101 of regulated value Linearity Indication error at each input Regulated value 0 010 pH 1digit High impedance Indication error at each input Regulat...

Страница 69: ...t data for one time calibration is dis played With a printer connected Print is displayed at the field of F4 Pressing F4 PRINT prints out the displayed information Check data display 1 In the CHECK sc...

Страница 70: ...s CAL key The displayed title of the screen changes from mV Measurement to Relative mV Measurement The indicated value is compensated as off set potential and the screen displays the instantaneous val...

Страница 71: ...F1 mV SETUP to go to mV SETUP screen 2 Press or key and select LIMIT ON 3 Press the ENTER key The screen moves to the upper limit value setting field 4 Press the ENTER key again The display color of...

Страница 72: ...r 4 mV ORP MEASUREMENT 4 2 Functions in mV Measurement F 52 53 54 55 59 To skip alarm function 1 Select OFF in the above step 2 2 Press F4 RETURN to reflect the setting The screen returns to the Measu...

Страница 73: ...Chapter 4 mV ORP MEASUREMENT 4 3 Meter Check 60 HORIBA 4 3 Meter Check There is no checking mode in mV ORP measurement For meter check use pH checker mode...

Страница 74: ...ation of an unidentified solution by preparing a calibration curve which shows the relation between mV and concentration The standard addi tion method is used to obtain the concentration of the target...

Страница 75: ...o perform 2CH simultaneous measurement for the same solution it may take approximately 10 seconds until the indication stabilizes 5 2 1 Calibration Using Ion Standard Solution CH 1 calibration 1 In an...

Страница 76: ...s indication mark showing the first point calibration appears The calibration of the second point 1 Input the value of the standard solution for the second point by or key and select the unit by or ke...

Страница 77: ...value and measured value is displayed When the repeatability check is successfully completed the electrode status OK appears on the screen Function key at Ion calibration CHECK To perform periodical c...

Страница 78: ...Open the internal solution filler port During the calibration the filler port should be kept open The filler port structure depends on the elec trode 3 Immerse the electrode in the sample to at least...

Страница 79: ...tarts blinking and when the indication stabilizes the HOLD indication lights up The indi cation value is held and the measure ment is completed The measured value may be in the HOLD state such as in t...

Страница 80: ...e Sample addition method For the sample addition method a small amount of sample is added to the standard solution for the ion species to measure to increase the amount of the target component concent...

Страница 81: ...etical value Nernst coefficient or if a decrease in the concentration after addition is specified then accurate measurement results may not be obtained 5 3 1 Measuring Ion Concentration in Standard Ad...

Страница 82: ...solution It is desirable that when the standard solution is added to the sample solu tion the concentration of the ion species under measurement increase by 1 to 10 times in the sample solution It is...

Страница 83: ...up Pressing the ESC key clears the HOLD status 3 Add the standard solution to the sample solution 4 Press the MEAS key The AutoHold measurement starts When the indication stabilizes the HOLD indicatio...

Страница 84: ...t the known addition method 5 Press or key and select the 2 DOUBLE option 6 Press F4 RETURN The BUFFER ADD2 screen appears Setting the Measurement condition Input such parameters as sample volume conc...

Страница 85: ...solution It is therefore necessary to consider the concentration and added amount of the standard solution well If the concentration of the added standard solution is too low if the volume of the adde...

Страница 86: ...on 2 to the sample solution Pressing the ESC key clears the HOLD status 6 Press the MEAS key The AutoHold measurement starts When the indication stabilizes the HOLD indication lights up After cal cula...

Страница 87: ...n for the ion species to measure once thus increasing the ion concentration of the target component and then measuring the change in electric potential which occurs at that time 1 In the ION SETUP scr...

Страница 88: ...ing is completed press F4 START For more accurate measurement Normally the added amount of the sample should be from 0 1 to 10 volume of the stan dard solution It is desirable that when the standard b...

Страница 89: ...n lights up 3 Add the sample to the standard solution Pressing the ESC key clears the HOLD status 4 Press the MEAS key The AutoHold measurement starts When the indication stabilizes the HOLD indicatio...

Страница 90: ...d solution for the ion species to measure twice thus increasing the ion concentration of the target component and then measuring the change in electric potential at that time 1 In the ION SETUP screen...

Страница 91: ...alue The Ion valency depends on each ion input the appropriate valency for the ion to be mea sured Setting range Types and Features of Applicable Electrodes page 235 For more accurate measurement Norm...

Страница 92: ...y The AutoHold measurement starts When the indication stabilizes the HOLD indication lights up Pressing the ESC key clears the HOLD status 3 Add the Sample 1 to the standard solution 4 Press the MEAS...

Страница 93: ...ts When the indication stabilizes the HOLD indication starts blinking When the measurement is completed the concentration of the sample solu tion will display in the screen To continue the measurement...

Страница 94: ...press F1 ION SETUP The ION SETUP screen appears When there is no need to change the conditions press either the ESC key or the MEAS key The screen returns to the ION Measurement screen Measurement 1...

Страница 95: ...entered The temperature is compensated using the entered temperature value 1 In the ION SETUP screen press or key and select the TEMP COMPENSATION option Select either AUTO or MANUAL by press ing or...

Страница 96: ...en select the ION SELECTION option 2 Press or key and select MANUAL Selecting MANUAL 1 Press the ENTER key The display color of the input part of ION SELECTION changes enabling the input 2 Press or ke...

Страница 97: ...ting Setting the other model freely Press F2 OTHER to enable the model name input by alphabetical and numerical characters Up to 9 characters are available Press F4 RETURN returns the screen to ION SE...

Страница 98: ...n Measurement F 53 55 5 4 Changing Measurement SETUP Conditions F 52 53 54 55 85 3 Press F4 RETURN to return to the ION SETUP screen 4 Press F4 RETURN to reflect the setting and returns to the Measure...

Страница 99: ...n The display color of the setting part changes enabling the input by pressing or key Setting range 0 0 g L to 999 g L 0 00 mol L to 999 mol L Press or key to change the auxiliary unit 3 When the sett...

Страница 100: ...appears 2 Output the sample data from the checker 3 Press the CAL key When the indication stabilizes the HOLD indication changes from the blinking state to the lit state 4 Output the next sample data...

Страница 101: ...ion Linearity check regulated indication error by each input 3 0 1digit of the full scale Temperature regulated error by each input 0 4 When the judgment of CHECK is displayed assure the connection an...

Страница 102: ...eck display 1 In the CAL screen press F3 CAL DATA The CALBRATION DATA screen appears When the printer is connected the function display of F4 shows PRINT Pressing F4 PRINT prints the check data Check...

Страница 103: ...Chapter 5 Ion Measurement F 53 55 5 5 Check Display 90 HORIBA...

Страница 104: ...ment Screen for Conductivity 1 Press the MODE key in any Mea surement screen and go to COND Measurement screen The displayed screen shows the instantaneous measured value of conductivity In the Measur...

Страница 105: ...y and set the cell constant displayed on the elec trode The unit indication of the cell constant depends on the electrode Convert the unit to the one for the meter before input 100 m 1 1 cm 1 1000 m 1...

Страница 106: ...y the step described in the previous section pressing the MEAS key should show the instantaneous measurement value 1 In the COND Measurement screen press the MEAS key The AutoHold measurement starts W...

Страница 107: ...en 6 4 1 Unit selection 1 In the COND SETUP screen press or key to select the UNIT and press or key to select S m or S cm 2 Press F4 RETURN The setting is reflected and the dis play returns to the Mea...

Страница 108: ...t the temper ature value to the system The compensation uses the input temperature value 1 In the COND SETUP screen press or key and select the TEMP COMPENSATION option and press or key and select AUT...

Страница 109: ...by a thermostatic chamber 1 In the COND SETUP screen press or key to select the TEMP COEFICIENT option and press or key to select OFF ON or PURE WATER In setting to PURE WATER refer to Pure water tem...

Страница 110: ...ve the cursor to the ELETRODE MODEL option Pressing F2 will switch the ELECTRODE MODEL screen with the input screen 4 Determine the setting by the ENTER key 5 Press F4 RETURN The set value is register...

Страница 111: ...ry can con tain the electrode Lot information 1 In the COND SETUP screen move the cursor to the electrode Lot change the field by or key 2 Press the ENTER key The ELECTRODE LOT screen appears 3 Select...

Страница 112: ...f the setting part changes enabling to input the values by pressing or key Setting range 0 3 S m to 199 9 S m 0 3 S cm to 199 9 S cm Set the auxiliary unit by or key 2 Press the ENTER key The setting...

Страница 113: ...to AUTO 1 In the COND Measurement mode press the CAL key The SETUP screen for the cell con stant appears 2 Press the MODE key The COND CALIBRATION screen appears 3 Press F2 CHECK The periodical check...

Страница 114: ...s not related with the inspection When all the confirmation is done the result is displayed Span check result Criteria 0 5 1digit of the full scale At input of 19 00 S m 1 5 1digit of the full scale L...

Страница 115: ...ture check result Indication error by each input regulated value 0 4 When the judgment of CHECK is displayed assure the connection and repeat the check When the error repeatedly occurs ask further ins...

Страница 116: ...T prints the check data Calibration data display The latest calibration data can be displayed 1 In the CAL screen press F3 CAL DATA The calibration data is displayed When the printer is connected the...

Страница 117: ...ds input only when it is not set In this case set the cell constant by referring to 6 2 Cell Constant Setting page 92 7 1 Operation of Salinity Measurement In any Measurement screen for CH2 press the...

Страница 118: ...lowing step 1 Immerse the electrode in the stan dard sea water 2 In the SALT Measurement screen press the CAL key The SALT CALIBRATION screen appears 3 Press or key to set the con centration of standa...

Страница 119: ...n or outputs them from the external output terminals The values out of the limit value are displayed in the different color on the screen Set the alarm ON or OFF by the following step 1 Press or key t...

Страница 120: ...changes 4 Press key to select the lower limit option 5 Press the ENTER key again The display color of the set part changes and pressing or key enables the value input Setting range 0 00 to 4 00 6 Pre...

Страница 121: ...Chapter 7 SALINITY MEASUREMENT F 54 55 7 4 Check 108 HORIBA 7 4 Check There is no check mode for the salinity mea surement Check the meter by SYSTEM CHECK for COND...

Страница 122: ...when it is not set See 6 2 Cell Constant Setting page 92 The unit setting of resistivity should be determined by unit setting of conductivity See Page 94 Conductivity unit S m Resistivity unit m Cond...

Страница 123: ...y to select the RESISTANT LIMIT option and press or key to select ON or OFF 3 Press F4 RETURN The setting is reflected and the Mea surement screen is displayed Setting alarm conditions By selecting ON...

Страница 124: ...es can be input by pressing or key Setting range 0 0 m to 199 9 M m Switch the auxiliary unit by pressing or key 7 Press the ENTER key The setting is determined and the display color of the set part c...

Страница 125: ...Chapter 8 RESISTIVITY MEASUREMENT F 54 55 8 2 Setting Configuration 112 HORIBA...

Страница 126: ...the power ON After the startup screen the SETUP screen appears Pressing ESC key in the Measurement screen also shows the SETUP screen 2 Pressing or key select SYS TEM SETUP option and press ENTER key...

Страница 127: ...or of the set part changes press or key to input the values Setting range 1 to 999 sec 4 Press the ENTER key The setting is determined and the color of the set part changes 5 Press the F4 RETURN The s...

Страница 128: ...be memorized during instantaneous value dis play or when the AutoHold measurement is completed while HOLD display is lit 1 Press F3 DATA IN The data at this time is memorized The sample ID input scree...

Страница 129: ...ta is displayed In performing pH repeatability check the electrode status displayed in the measurement data is the one judged by the preliminary inspection 3 Press the ESC key to return to the data ca...

Страница 130: ...asurement item 1 Press or key and select ITEM 2 Press F4 SEARCH key The search result is displayed Search by Operator name 1 Press or key and select Operator 2 Press F4 SEARCH The search result is dis...

Страница 131: ...r 9 DATA MEMORY 9 3 Calling up Memory Data 118 HORIBA 4 Press F4 SEARCH The searched result is displayed To delete the memorized data perform data memory deletion by referring to CLEAR DATA MEMORY pag...

Страница 132: ...security related setting change The meter can be used without operator registration In that case this section can be skipped When the operator is not selected by selecting OFF in SELECT OPERATOR the o...

Страница 133: ...CURITY SETUP screen 120 HORIBA 10 1 SECURITY SETUP screen 1 Press ESC key on the Measure ment screen The SETUP screen appears 2 Press or key and select the SECURITY SETUP option 3 Press the ENTER key...

Страница 134: ...on Common operation 1 In the SETUP menu press or key to select SECURITY SETUP 2 Press the ENTER key The SECURITY SETUP screen appears 3 Press or key to select option 4 Set or perform each option accor...

Страница 135: ...erator has been registered the SELECT OPERATOR menu appears When the User Control is ON Administrator should be careful not to forget the password Multiple Administrators should record passwords in ca...

Страница 136: ...0 3 4 Password Limit By setting the Password Limit ON input of erroneous passwords more than the set times until the normal startup locks out the system To make the setting valid 1 With the PASSWORD R...

Страница 137: ...g unit is minute Setting range 1 to 999 minutes 3 Press the ENTER key The setting has been made 10 3 6 Reset the lockout This section explains how to reset the lockout This operation is only available...

Страница 138: ...is regarded as the Administrator The configuration for the Administrator and Operator can be also set after the registration 1 In the OPERATOR REGISTRA TION screen press F2 NEW OPERATOR The NEW OPERA...

Страница 139: ...ost the stored data is not available Changing the password The password can be changed on the OPER ATOR REGISTRATION screen 1 Press or key and select the operator which password is to be changed 2 Pre...

Страница 140: ...or in the sys tem Deleting the Administrator with the User Control option ON will make the User Control status unable to change 1 Press or key and select the operator to be deleted from the registrati...

Страница 141: ...ed as Administrator becomes the normal Operator and the Operator registered as normal becomes Administrator 1 Press or key and select the Operator which authority is to be changed 2 Press the ENTER ke...

Страница 142: ...ETUP screen From the Measurement screen 1 In the Instantaneous Measurement screen press the ESC key The SETUP screen appears From power ON This is effective only when the USER MAN AGEMENT is OFF 1 Tur...

Страница 143: ...ectable by operators other than the Adminis trator when the User Control is ON MAINTENANCE Setting configuration for the meter functional check Not selectable by operators other than the Adminis trato...

Страница 144: ...ss or key and select SYSTEM SETUP option The SYSTEM SETUP screen appears 11 2 1 Display pattern change The display pattern of the Measurement screen can be set 1 In the SYSTEM SETUP screen press or ke...

Страница 145: ...The graph is cleared when the oper ations such as pressing MODE or SETUP keys are made The horizon tal axis on the graph screen is Instantaneous time sec The data is displayed as a graph in measuring...

Страница 146: ...h as calibration data is displayed on the sub screen for DIGITAL display 1 In the SYSTEM SETUP screen press or key and select 2CH DISPLAY option 2 Press or key and select OFF or ON 3 Press F4 RETURN T...

Страница 147: ...COND Potential change in 10 seconds within 1digit Temperature change in 10 seconds within 2 0 Salinity Potential change in 10 seconds within 0 03 Temperature change in 10 seconds within 2 0 NOR MAL p...

Страница 148: ...and the dis play returns to the SETUP screen In selecting TIME When the mode option TIME is selected in the step 2 above set the time until the measure ment value is held by the following step 1 Press...

Страница 149: ...ing Data Memory of the func tion keys at any time Selecting ON stores multiple data at set time intervals 9 1 Setting Memory Type page 113 11 2 5 Setting printout format The printout format can be sel...

Страница 150: ...n 2 Press or key and select either ENGLISH or JAPANESE 3 Press F4 RETURN The setting is reflected and the dis play returns to the SETUP screen 11 2 7 Sound setting The meter electrical sound can be se...

Страница 151: ...s or key and select the DATE AND TIME SETUP option 2 Press the ENTER key The DATE AND TIME SETUP screen appears 3 Press or key and select the appropriate year date and time 4 Press or key and give the...

Страница 152: ...NTER key The MAINTENANCE screen appears 3 Press or key and select the option to be set or executed 4 Set or perform the option accord ing to each configuration 5 Repeat step 3 and step 4 above and com...

Страница 153: ...the initial setting 1 Press the ENTER key The setting is now available 2 Press or key and set the color tone The color tone of the screen changes 3 Press the ENTER key The setting is made Character T...

Страница 154: ...pears 2 Press or key and select the item and press ENTER key to determine the selection 3 Check the output by a voltmeter 4 Press or key and adjust the output voltage indicated on the voltmeter to the...

Страница 155: ...is made Pressing any key returns the display from power saving state to normal state CLEAR DATA MEMORY This function deletes all the measurement results stored in the system memory 1 Press the ENTER...

Страница 156: ...zed 3 Read the temperature indication correctly by a thermometer 4 Press the ENTER key The setting is now ready to be made 5 Press or key and set the value to the read temperature from the thermom ete...

Страница 157: ...eration Cautionary items The compact flash cards used in this meter should be either 8MB or 16MB A micro drive with hard disk format is not available Always use the products that HORIBA sells or a HOR...

Страница 158: ...essary options 6 Press the F4 RETURN The setting is reflected and the SETUP screen appears Setting Executing each item DATA COPY SETUP Setting ON will memorize the data in the compact flash card when...

Страница 159: ...ted Formatting will delete all the data previously stored 1 Press ENTER key 2 Press F4 CONFIRM The formatting starts Since the formatting uses a part of memory the empty capacity displayed will be sma...

Страница 160: ...ailable by the operator name registered in the compact flash card The compact flash card can be commonly used on multiple meters Startup by the compact flash card allows the following convenience No p...

Страница 161: ...er network system Cautionary items for Internet address setting In using IP address a private address can be used in the environment unconnected to the external Internet specified by RFC1918 The envir...

Страница 162: ...t is recommended to use the standard setting Gateway address When the network configuration includes a server or rooter as gateway the address of that server or rooter is called the gateway address Wh...

Страница 163: ...pears 3 Press or key and select the operator 4 Press F4 RETURN The password input screen appears 5 Press or key to select the numerical values and press ENTER 6 When the password is input press F4 RET...

Страница 164: ...d required in 21 CFR Part 11 FDA United State Food and Drug Administration is available To perform this optional software supporting FDA 21 CFR Part 11 as well as the specific database software with t...

Страница 165: ...Chapter 11 METER SETTING 11 8 FDA Part 11 Function Audit Trail F 55 152 HORIBA...

Страница 166: ...PC using an exclusive communication cable be sure to turn off the power beforehand Connecting the meter and the PC with the power ON may damage the meter Do not use any cable except for the exclusive...

Страница 167: ...s CPH CMV CIO CCO COH CSA and measure ment start command CMS are effective only when the main screen and the specified channel are matched If the present measurement mode and the channel are not match...

Страница 168: ...R Electrode status 0 Good 1 Electrode check 2 Electrode NG 3 No calibration data 4 Good 0 5 Good 1 6 Good 2 7 Electrode exchange preparation 9 Abnormal temperature Check pH meter Time On setting yyyy...

Страница 169: ...ld OFF or in calibration either calibration value is forcefully obtained in calibration or holds the measured value in measure ment In the interval memory the error response malfunction returns pH mea...

Страница 170: ...bration can be per formed exceeding the calibration points However after calibration of five points is complete the error message Incor rect operation is responded for the suc ceeding command Start io...

Страница 171: ...f Serial Command 158 HORIBA With a model that has two input channels the calibration command is effective only on the main channel Cancel inter val memory C CN Effective only during the interval mem o...

Страница 172: ...ode Parameter CR LF Command for Command Parameter Description of parameter Note Header Comma nd code AutoHold setting S PH x y zzz x channel number y AutoHold condi tion zzz pH AutoHold time Channel n...

Страница 173: ...is no calibra tion data RPC x 0 3 zzzzzzzzzzzz Operator name x channel number a number of cali brated points b Electrode status c Temperature com pensation dddddd Asymmetry potential e Check flag befo...

Страница 174: ...Response when there is no calibra tion data RIC x 0 0 3 zzzzzzzzzzzz Operator name x channel number aa ion type b number of cali brated points c Electrode status d Temperature com pensation eeeeee As...

Страница 175: ...bbbbbb cc e f g ii yyyy yy yy yy yy yy ppppp ppp q r s ttttt uuuu uuu v aaaaaaaaaaaa Operator name bbbbbbbbbbbb ID No cc Measuring composition e channel f Condition 0 MEAS 1 CAL 2 Check before use 3 I...

Страница 176: ...q r s ttttt uuuu u v xxx Memory No aaaaaaaaaaaa Operator name bbbbbbbbbbbb ID No cc Measuring compo sition e Channel f Condition 0 MEAS 1 CAL g HOLD 0 Instanta neous value 1 Hold 2 Measurement ii ion...

Страница 177: ...yy Calibration date ppppp Cell constant numeral qqqq Cell constant digit number r Unit for cell constant sssss temperature Salinity cali bration his tory request R SC x x channel number RSC zzzzzzzzzz...

Страница 178: ...nnel number y Request mode zzzzzzzz Error con tents bit basis 0x00000002 Battery voltage drop model 0x00000004 Electrode instability other than model 0 00000008 Abnormal asymmetry potential pH 0 00000...

Страница 179: ...is displayed in the external output connection display section in the pH Measurement screen Communication sample As a reference here is the communication using the Windows hyperterminal 1 Open the Hyp...

Страница 180: ...contents transmitted via HyperTerminal by enabling the Echo typed characters locally E option 4 Input the commands If you input a command the corresponding response data is sent back Command input sh...

Страница 181: ...and temperature data and the open drain output for the alarm set can be obtained The analog alarm output cable is optional F 52 Terminal No Connection cable Output 1 For CH1 Shield CH1 Ground Red CH1...

Страница 182: ...H1 Shield CH1 Ground Red CH1 Temperature White CH1 measure ment data 2 For CH2 Shield CH2 Ground Red CH2 Temperature White CH2 measure ment data 3 For alarm Shield Alarm ground Red CH1 alarm White CH2...

Страница 183: ...04 800 10 0 to 99 9 mg L mmol L 400 to 0 mV Measurement value 4 103 400 100 to 999 mg L mmol L 0 to 400 mV Measurement value 4 102 1 00 to 9 99 g L mol L 400 to 800 mV Measurement value 4 100 400 10 0...

Страница 184: ...e 2500 500 2 00 to 19 99 mS cm 0 to 500 mV Measurement value 2 5 104 0 200 to 1 999 mS cm 500 to 0 mV Measurement value 2 5 105 500 20 0 to 199 9 3 S cm 1000 to 500 mV Measurement value 2 5 106 1000 2...

Страница 185: ...1 999 k m 0 to 500 mV Measurement value 2 5 10 1 20 0 to 199 9 5 m 500 to 0 mV Measurement value 2 5 2 5 500 2 00 to 19 99 6 m 1000 to 500 mV Measurement value 2 5 25 1000 0 50 to 1 999 m 1500 to 1000...

Страница 186: ...Chapter 13 ANALOG OUTPUT 13 3 Alarm Output F 52 53 54 55 173 13 3 Alarm Output The alarm output is open drain output 15V less than 20 mA When the alarm is triggered the output is ON...

Страница 187: ...Chapter 13 ANALOG OUTPUT 13 3 Alarm Output 174 HORIBA...

Страница 188: ...h the FEED and CHARGE switches held down Startup the printer SETUP mode to change to the above setting Refer to the instruction manual for the printer 14 1 1Printer output timing The printer prints at...

Страница 189: ...ain when this happens The model and the manufacturer may be changed according to improvement and or change of the printer specification or features Font size of the printout data may be changed withou...

Страница 190: ...intout Electrode state OK CHECK ERROR Sensitivity display Standard solution value is displayed No calibration 1 point calibration None 2 point calibration 1st item 3 point calibration 2nd item 4 point...

Страница 191: ...calibration 4th item When the data in the one con firmed with AutoHold Stable is shown Nothing is displayed for the instan taneous value measurement Std solution and potential Up to 5 point CAL BRIEF...

Страница 192: ...n the one con firmed with AutoHold Stable is shown Nothing is displayed for the instantaneous value measure ment DIsplayed only with CAL data BRIEF printout Operator name max 12 letters Temperature co...

Страница 193: ...with the format same with the one in 14 4 1 When the ENTER key is pressed in the Measurement mode page 177 Example in the pH Measurement mode 14 4 3 Printout from DATA OUT screen The same format with...

Страница 194: ...point calibra tion None 2 point calibration 1st item 3 point calibration 2nd item 4 point calibration 3rd item 5 point calibration 4th item Std solution and potential Up to 5 point CAL Electrode stat...

Страница 195: ...2 point calibration 1st item 3 point calibration 2nd item 4 point calibration 3rd item 5 point calibration 4th item Std solution and poten tial Up to 5 point CAL Electrode status OK Calibration is per...

Страница 196: ...Printout F 52 53 54 55 183 Printout in COND CAL mode Printout in SALT CAL mode Electrode status OK Calibration is performed EXACT printout BRIEF printout Electrode status OK Calibration is performed...

Страница 197: ...Chapter 14 PRINTER 14 4 Sample Printout 184 HORIBA 14 4 5 Printout in CHECK mode pH CHECK JIS mode Electrode status OK CHECK ERROR EXACT printout BRIEF printout...

Страница 198: ...Chapter 14 PRINTER 14 4 Sample Printout F 52 53 54 55 185 pH CHECK NIST mode Electrode status OK CHECK EXACT printout BRIEF printout...

Страница 199: ...Chapter 14 PRINTER 14 4 Sample Printout 186 HORIBA pH CHECK SIMULATOR mode Meter status OK CHECK EXACT printout BRIEF printout...

Страница 200: ...Chapter 14 PRINTER 14 4 Sample Printout F 52 53 54 55 187 ION CHECK SIMULATOR mode Meter status OK CHECK EXACT printout BRIEF printout...

Страница 201: ...Chapter 14 PRINTER 14 4 Sample Printout 188 HORIBA COND CHECK SIMULATOR mode Meter status OK CHECK EXACT printout BRIEF printout...

Страница 202: ...pears be sure to take appropriate action 15 1 Maintenance 15 1 1 pH ORP electrode maintenance Maintain the electrodes by referring to the following information or to the operation manuals for the elec...

Страница 203: ...tive cap from the electrode 3 Open the internal solution filler port then use a plunger to remove the standard solution 4 Fill the electrode with new internal solution 300 until it nears the filler po...

Страница 204: ...he protective cap has dried wash the inside of the protective cap with pure de ionized water After shaking out the water fill the cap with enough pure de ionized water to soak the sponge If the soluti...

Страница 205: ...trode is so dirty that it cannot be cleaned by rinsing with pure de ionized water wash the electrode using the method below that is most appro priate General dirt oily grime Wipe the dirt grime off us...

Страница 206: ...e ion electrodes listed in the above table begins on next page Ion to be measured Ion type Slope Measurement range Elect rode mod el Comp atible tip model standard solution Potassium K 1 58 mV 0 04 to...

Страница 207: ...rode No conditioning F ion electrode NO3 ion electrode 1 mol L potassium nitrate solution 100 g L KNO3 Approx 1 h K ion electrode 0 1 mol L potassium chloride solution 75 g L KCl Approx 12 h Ca2 ion e...

Страница 208: ...ctrode outer tube 1 Open the internal solution filler port by removing the rubber stopper then turn the electrode upside down and use a syringe to remove the standard solution 2 Use the syringe to fil...

Страница 209: ...are during disassembly Items necessary when replacing internal solution inner tube are a syringe 330 gel stan dard solution and the standard solution specified for the particular electrode Filling the...

Страница 210: ...ash them with pure de ion ized water 3 Insert body 1 into body 2 Make sure that the O ring is securely sealed 4 Return the spring to the top of body 1 5 Hold the rubber sleeve in place by hand then tw...

Страница 211: ...able Connector cover Electrode connector O ring Silicon tube Rubber seal for internal solution filler port internal cylinder Body 1 Rubber cap Rubber seal for internal solution filler port external cy...

Страница 212: ...of time store it after performing the fol lowing procedure Also perform maintenance on the electrode every three to six months 1 Remove the electrode from the pH meter 2 Use pure water to wash away a...

Страница 213: ...the electrode is 45 mV or more 05 Span calibration ERROR pH pH The electrode sensitivity is either 105 or more or 85 or less than the theoretical sensitiv ity 06 Excess calibration points Calibration...

Страница 214: ...en to the internal memory ERR No 02 The battery voltage is low Explanation The battery has insufficient voltage Cause How to solve problem Software is not writ ten at starting Seek repairs at your nea...

Страница 215: ...ure change Press the MEAS key again while HOLD is either flashing or steadily lit in the display to measure the sample using instantaneous value measurement The electrode is dirty Wash the electrode T...

Страница 216: ...e The electrode is not connected correctly Connect the electrode correctly Electrode is not sub merged deeply enough to cover reference junction Immerse the electrode in the sample to at least 3 cm be...

Страница 217: ...problem 6th point calibration was executed Regulate the calibration up to 5 points This error message is released by setting the pH meter to measurement mode Cause How to solve problem There is a pro...

Страница 218: ...ow then turn the power to the meter back ON ERR No 10 Data memory over Definition The number of data items has exceeded the limit of the memory Cause How to solve problem The printer paper is jammed R...

Страница 219: ...No 14 CF not inserted Definition The compact flash card is not correctly inserted Cause How to solve problem COND electrode is at the end of the useful life Replace the electrode Improper standard sol...

Страница 220: ...rnet timeout Definition Abnormality occurs in Ethernet during communication Cause How to solve problem Faulty Ethernet con nection or setting Check the connection and setting of the net work Check the...

Страница 221: ...of the AC adaptor The pH meter is defective Contact with the nearest sales representative Cause How to solve problem The responsive membrane is dry or dirty Wash the responsive membrane The responsive...

Страница 222: ...How to solve problem The liquid junction is not immersed in the sample solution Immerse the electrode in the sample solution up until the liquid junction This is caused by the effects of the sam ple...

Страница 223: ...re is absolutely no response Cause How to solve problem The electrode con nector is not attached correctly Turn the power OFF then turn it back ON again The electrode is defective The responsive mem b...

Страница 224: ...per wire or bent paper clip to short the meter by touching both the center pin and some metal part in the electrode connector If the flaching measured value disappears when this done the meter is noma...

Страница 225: ...or more at room temperature replace the electrode Poor connection of temperature connec tor Firmly insert the temperature connector There is a problem with the setting for the temperature dis play ca...

Страница 226: ...OFF was pressed Make the operator selection again Cause How to solve problem The user manage ment is still ON Newly register settings and make the operator setting or make the Administrator turn OFF...

Страница 227: ...Chapter 15 Maintenance and troubleshooting 15 2 Troubleshooting 214 HORIBA...

Страница 228: ...hapter provides a simple compilation of information for people who would like to know more details about the functions of the main unit of the pH meter and other measurement prin ciples Also consumabl...

Страница 229: ...ns is equal In this state of equilibrium the potential at the contact surface between the two solutions is called the liquid junction potential A large liquid junction potential means very inaccurate...

Страница 230: ...le Therefore the pH electromo tive force changes according to the change in temperature and this change in the electromotive force becomes an input to the pH meter Then it is called the temperature co...

Страница 231: ...tion pH 6 86 standard solution Neutral phosphate 0 025 mol L potassium dihydrogen phosphate 0 025 mol L sodium dihydrogen phosphate aqueous solution pH 9 18 standard solution Borate 0 01 mol L tetra s...

Страница 232: ...ibration Use the pH 7 standard solution or a standard solution that approximates the pH value of the solution that is to be inspected When it is known beforehand whether the test solution is acidic or...

Страница 233: ...ng equation E Electric potential E Coefficient R Gas coefficient T Absolute temperature n Electron count F Faraday constant a Activity Fig 1 ORP measuring system For example for a solution in which tr...

Страница 234: ...ue of the same solution may appear to be different HORIBA uses Ag AgCl with 3 33 mol L KCl as the standard solution for reference elec trodes According to general technical literature standard hydroge...

Страница 235: ...easure the mV value 3 If the electrode and the meter itself are working correctly numerical values within 15 mV or less of those listed in Table 1 should be obtained 4 If measurements that fall within...

Страница 236: ...tandard substance the measured values may not sta bilize or the results of measurement might not be repeatable If this is the case use the meter after immersing the electrodes in the solution again an...

Страница 237: ...ic solution and then retained on polyvinyl chloride to make it oily for use as mem brane K Ca2 NO3 ClO4 Cl NH4 Dissolved gas sensitive electrode Perforated gas permeable membrane is combined with a pH...

Страница 238: ...ding the potential E of the ion electrode inside the solution being measured will enable the ion concentration to be determined When actual measurement is performed the ion electrode measures the ion...

Страница 239: ...omplex dissociating agent commercially avail able TISAB solution for the fluoride ion electrode to the sample solution to dissociate the complexes into fluoride ions before measurement Measurable rang...

Страница 240: ...ained at a certain level Generally this is attained by adding indifferent base which does not react with the target ions nor influence the electric potential under measurement the type and added amoun...

Страница 241: ...mV for bivalent ions This requires making the temperature of the standard solution as equal as possible to that of the solution under mea surement when preparing a calibration curve When you actually...

Страница 242: ...stance The ion electrode is excellent in its selectivity for the target ions but it may sometimes respond to other ions If those ions coexist with the target ions they interfere with or influ ence the...

Страница 243: ...main component in its responsive membrane Cl Br I CN etc Standard solution To measure the ion concentration of a solution previously calibrate the ion meter by using a conditioned standard solution wh...

Страница 244: ...in their concentrations because of their evapora tion or inclusion of impurities Storing ion electrode The most important point in the maintenance of the ion electrode is that the electrode is kept cl...

Страница 245: ...uid junction part of reference electrode clogged Are the readings of standard solutions stable Are they free from any noise resulting form stirring 1 Open the rubber stopper at the inlet for internal...

Страница 246: ...SI the liquid junction part of the reference electrode free from clogging Measurement Use masking agent against interfering ions if it is found appropriate The measured ions might have caused precipi...

Страница 247: ...o 11 350 mg L Cl 59 mV 0 to 50 NO3 F HCO3 SO4 2 PO4 2 more than 1000 SCN 0 3 MnO4 0 1 Br 0 03 S2O3 2 S2 I Ag Hg2 Not applicable At 10 3 mol L Cl 2565A 10T 1 mol L KNO3 100 g L Potas sium nitrate 8003...

Страница 248: ...0 NH4 K 1000 Ni2 Mg2 Zn2 100 Cd2 10 Cr3 1 Fe3 0 01 2565A 10T 1 mol L KNO3 100 g L Potas sium nitrate 8009 10C Thiocy anate SCN 0 6 to 35000 mg L SCN 1 to 10 5 mol L SCN pH 2 to 12 5 8 mg L SCN 59 mV 0...

Страница 249: ...e NO3 0 62 to 62000 mg L NO3 1 to 10 6 mol L NO3 pH 3 to 7 62 mg L NO3 55 mV 0 to 50 SO4 2 more than 1000 CH3COO 300 F 200 Cl 40 NO2 3 I 0 1 ClO4 0 02 At 10 3 mol L NO3 2565A 10T 1 mol L KCl 75 g L po...

Страница 250: ...ll the electrodes Model and ion type Applica ble chip elec trode type quantity 1 Measurable range 2 pH allowable range 1 3 Electric potential slope 2 interfering ions and allowable limit for their coe...

Страница 251: ...ases as the allowable coex istence limit becomes larger or the concentration of the measured ion becomes higher 4 The internal liquid types are not limited to the solutions listed in the table You may...

Страница 252: ...en cool it in a desiccator Measure out the above listed amount of potassium chloride into a beaker and dissolve it in distilled water Then pour into one liter volumetric flask and add distilled water...

Страница 253: ...e potassium chloride standard solution constant at 25 0 5 2 Press the CALkey in the COND instant value measurement screen to open the CAL screen 3 Press the MODE key in the cell constant input screen...

Страница 254: ...stance R expressed in is in inverse proportion to the area A expressed in m of the pole plates as is the case with metal and other conductors and is proportional to the distance l expressed in m betwe...

Страница 255: ...n temperature as the standard and calling that the standard temper ature the temperature coefficient expresses how much change expressed in occurs in conductivity when the temperature of the solution...

Страница 256: ...0 0867 2 38 KCl 18 5 6 90 2 01 4 01 0 1095 2 50 10 13 59 1 88 8 03 0 1038 2 62 15 20 20 1 79 16 15 0 0632 3 01 20 26 77 1 68 HF 18 1 5 1 98 7 20 21 28 10 1 66 4 8 5 93 6 66 KBr 15 5 4 65 2 06 24 5 28...

Страница 257: ...intended seawater based on the nor mal seawater converting it according to its measured conductivity and temperature Therefore note that all the substances detected as conductivity is indicated as sal...

Страница 258: ...ring range 0 0 to 100 0 Resolution 0 1 Repeatability 0 1 1digit ION Measuring principl Ion electrode Measuring range 0 00 g L to 999 g L mol L Resolution Valid numbers 3 digits Repeatability 0 5 1 dig...

Страница 259: ...0 5 1 digit of full scale Input CH number 1CH 2CH Output RS 232C Printer output Analog output Compact flash Ethernet output Data mem ory Memory number 300 pcs Interval memory Dis play Display Color g...

Страница 260: ...Salin ity Salt concentration calibration Ambient temperature 0 to 45 Power AC adaptor 100 to 240 V 50 60 Hz Power consumption Approx 8 4 W Mass of main unit Approx 1 1 kg Dimensions 79 H 179 W 230 D m...

Страница 261: ...COEFFICIENT OFF OFF ON COEF 0 100pH to 0 100pH Temperature 0 0 to 100 0 pH SETUP ELECTRODE MODEL No indication Selection formula from attached material or freed input 9 characters pH SETUP ELECTRODE...

Страница 262: ...E SETUP RESISTANCE LIMIT OFF OFF ON 0 0 m to 199 9M m SYSTEM SETUP DISPLAY DIGITAL DIGITAL GRAPH ANALOG SYSTEM SETUP 2CH DISPLAY ON ON OFF SYSTEM SETUP AUTO HOLD NORMAL EXACT NORMAL BRIEF TIME 2 to 99...

Страница 263: ...ETUP SUBNET MASK 255 255 255 0 0 to 255 0 to 255 0 to 255 0 to 255 SECURITY SETUP USER MANAGE MENT OFF OFF ON SECURITY SETUP VALID TERM OF PASSWORD OFF OFF ON 1 999 days SECURITY SETUP PASSWORD LENGTH...

Страница 264: ...ITIZEN printer CBM 910 24RJ100 A 16 7 3 Cable for SEIKO printer DPU H245AS A03A Meter main unit MINI DIN8M PC D SUB 9PIN 2 CTS 7 RTS 3 TXD 2 RXD 4 GND 5 GND 5 RXD 3 TXD Meter main unit MINI DIN8M Prin...

Страница 265: ...astic body electrode for immersion measurement F 50 series standard electrode 9611 10D 9096001800 Glass body electrode reinforced responsive glass employed Laboratory use elec trode for slurry sam ple...

Страница 266: ...c tive electrode 5002 10C 9003016600 Conbination selective electrode Part name Model Part number Remarks Chloride ion chip 7660 9003015000 For 6560 10C Fluoride ion chip 7661 9003015100 For 6561 10C N...

Страница 267: ...dard type Cell constant 100 m 1 3553 10D 9056001000 For high conductivity Cell constant 1000 m 1 Flow type conductiv ity electrode 3561 10D 9056001100 For low conductivity Cell constant 10 m 1 3562 10...

Страница 268: ...ion 150 4 9003002700 Powdered pH7 standard solution 150 7 9003002800 Powdered pH9 standard solution 150 9 9003002900 Part name Model Part number Remarks Standard solution for ORP check 160 51 90030031...

Страница 269: ...n paper printer Printer For Japan 9096003500 Purchase a printer cable when purchasing the printer For US 9096003600 For Europe 9096003700 Printer cable 9096003800 Roll paper 20 winding set 9096003900...

Страница 270: ...For more information please contact us ExpotechUSA 10700 Rockley Road Houston Texas 77099 USA 281 496 0900 voice 281 496 0400 fax E mail sales expotechusa com Website www ExpotechUSA com...

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