Büchi Labortechnik AG
Table of contents
Operation Manual Pure Chromatography Instruments
v
6
Operation............................................................................................................................ 33
6.1
Control panel ....................................................................................................................... 33
6.1.1 Layout of control panel ............................................................................................. 33
6.1.2 Enter value................................................................................................................ 34
6.1.3 Menu bar................................................................................................................... 35
6.1.4 Conditions panel ....................................................................................................... 37
6.1.5 Collection panel ........................................................................................................ 38
6.1.6 Gradient panel .......................................................................................................... 39
6.1.7 Run panel ................................................................................................................. 40
6.1.8 Solvent selection panel............................................................................................. 41
6.1.9 Detector selection panel ........................................................................................... 41
6.1.10 Slope detection panel ............................................................................................... 42
6.2
Editing a method.................................................................................................................. 42
6.2.1 Selecting a cartridge (Flash mode)........................................................................... 42
6.2.2 Selecting a column (Prep mode) .............................................................................. 44
6.2.3 Selecting a solvent.................................................................................................... 45
6.2.4 Editing the gradient................................................................................................... 45
6.2.5 Editing detector selection.......................................................................................... 48
6.2.6 Editing the wavelength for the UV detector .............................................................. 48
6.2.7 Editing the fraction collection criteria ........................................................................ 49
6.2.8 Editing the fraction collection time ............................................................................ 50
6.2.9 Editing the vapor sensor sensitivity .......................................................................... 52
6.2.10 Saving a method....................................................................................................... 52
6.3
Editing a solvent .................................................................................................................. 53
6.3.1 Adding a new solvent................................................................................................ 53
6.3.2 Deleting a solvent ..................................................................................................... 54
6.4
Tasks during a separation ................................................................................................... 54
6.4.1 Introducing a sample into the prep system ............................................................... 54
6.4.2 Injecting a sample into the flash system ................................................................... 55
6.4.3 Installing and removing a cartridge........................................................................... 57
6.4.4 Installing and removing a column ............................................................................. 58
6.4.5 Inserting the fraction collection tray .......................................................................... 60
6.4.6 Selecting an existing method.................................................................................... 61
6.4.7 Selecting values on the dialog box Sample Loading ................................................ 61
6.5
Performing a Flash separation using a method................................................................... 61
6.5.1 Preparing the instrument .......................................................................................... 61
6.5.2 Selecting the flash mode (Pure C-850 only) ............................................................. 62
6.5.3 Starting Flash separation using a method ................................................................ 62
6.5.4 Changings during a separation................................................................................. 62
6.5.5 Ending a Flash separation ........................................................................................ 63
6.5.6 Shutting down the instrument ................................................................................... 63
6.6
Performing a Flash separation manually ............................................................................. 63
6.6.1 Preparing the instrument .......................................................................................... 63
6.6.2 Selecting the flash mode (Pure C-850 only) ............................................................. 64
6.6.3 Starting Flash separation manually .......................................................................... 64
6.6.4 Changings during a separation................................................................................. 65
6.6.5 Ending a Flash separation ........................................................................................ 65
6.6.6 Shutting down the instrument ................................................................................... 65
6.7
Performing a Prep separation using a method .................................................................... 66
6.7.1 Preparing the instrument .......................................................................................... 66
6.7.2 Selecting the prep mode (Pure C-850 only) ............................................................. 66
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Содержание Pure C-810
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