Analytik Jena contrAA 600, Руководство по эксплуатации

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Table of contents
2 Edition 01/2014 contrAA 600
7.7 Automatic samplers AS-F, AS-FD ............... 72
7.7.1 Washing the mixing cup of the AS-FD ........ 72
7.7.2 Replacing the canulas and guide on the
autosampler arm ......................................... 72
7.7.3 Replacing the intake tube ............................ 73
7.7.4 Replacing the tube set for diluent and
washing liquid .............................................. 73
7.7.5 Clean-up after cup overflow ......................... 73
8 Transporting the contrAA 600 ................74
9 Waste disposal .........................................75
10 Abbreviations / terms ..............................76
11 Index ..........................................................78
12 EC Declaration of Conformity .................80
Index of figures
Fig. 1 Warning signs on the contrAA 600 ........... 12
Fig. 2 Dimensions of the contrAA 600 - front view22
Fig. 3 Dimensions of the contrAA 600 - top view 23
Fig. 4 Installation layout of the contrAA 600 ....... 23
Fig. 5 Schematic comparison of the physical
measuring principle of LS AAS and HR-CS
AAS .......................................................... 24
Fig. 6 Beam path in the contrAA 600 ................. 25
Fig. 7 Xenon lamp without housing .................... 26
Fig. 8 Electrothermal atomizer – graphite tube
furnace ..................................................... 27
Fig. 9 Graphite tube furnace ............................... 28
Fig. 10 Inner and outer gas flows in the graphite
tube furnace ............................................. 29
Fig. 11 Graphite tube furnace ............................... 30
Fig. 12 Graphite tube variations ........................... 30
Fig. 13 Furnace jacket, adapters and inserts ....... 31
Fig. 14 Autosampler AS-GF ................................. 32
Fig. 15 Solid sampler............................................ 33
Fig. 16 Autosampler AS-FD with separate Fluidik
module ..................................................... 35
Fig. 17 Mains switch and bar for supply and control
connections on the right side of the
contrAA 600 ............................................. 36
Fig. 18 Bar for supply and control connections .... 37
Fig. 19 Rear view of the contrAA 600 with
connections for the supply of gas and
electricity as well as the fuse holders ....... 37
Fig. 20 Graphite tube atomizer in sample chamber39
Fig. 21 Connections at the graphite tube furnace . 39
Fig. 22 Elements in the sample chamber for the
graphite tube technique ............................ 40
Fig. 23"Main Settings" window for graphite tube
technique .................................................. 40
Fig. 24 "Furnace / control" window ...................... 41
Fig. 25 Graphite tube furnace opened with inserted
graphite tube ............................................. 42
Fig. 26 Installing the AS-GF .................................. 45
Fig. 27 Aligning the AS-GF with the furnace using
the set screw and adjusting screw 1 ......... 46
Fig. 28 AS-GF adjustment .................................... 47
Fig. 29 Attaching holding pin and crossbar to the
AS-GF support in the sample chamber ..... 49
Fig. 30 Position of the eccentric roll at the SSA 60049
Fig. 31 HydrEA system HS 60 modular ................ 50
Fig. 32 Rear of the autosampler AS-FD ................ 51
Fig. 33 Dosing unit at the Fluidik module of the AS-
FD ............................................................. 52
Fig. 34 Safety circuit switch for hardware ............. 57
Fig. 35 Xenon lamp housing ................................. 59
Fig. 36 Xenon lamp, installed ................................ 59
Fig. 37 Cooling water container under the graphite
tube furnace .............................................. 59
Fig. 38 Identical markings at the furnace windows
facing upward ........................................... 61
Fig. 39 Furnace tools ............................................ 62
Fig. 40 Window "Autosampler / Function tests" in
the ASpect CS software ............................ 68
Fig. 41 Dosing tube at the AS-GF ......................... 69
Fig. 42 Dosing unit at AS-GF and AS-FD ............. 71