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instrument's zero line will affect your measurements if they you do not correct 
for these. You should refer to ASTM method E903 for further details. 

See Appendix B for more info on the acquisition, storing, and retrieval of baseline 
files 
 

Storage tab under Setup 

The Auto Store tab allows you to specify if you want to be prompted to store the 

collected data. You can store the data in a Batch or Data file at the start or end of 
a collect. There are 3 different options for automatically storing your data 

Storage Off:  

Select this if you do not wish to be automatically prompted to save 

collected data. To manually store your unsaved data after the run is complete, 
choose 

Save Data As

 from the File Menu. You can save your data as a Batch or 

Data file. In the Scan application, data is automatically stored as a Data file. See 
the Note below. 

Storage On (Prompt At Start): 

Select this to display the Windows Save As dialog 

box at the start of the collect where you can enter the Batch file name for your 
data.

 

Storage On (Prompt At End): 

Select this to display the Windows Save As dialog 

box at the end of a collect where you can enter the Batch file name for your data.

 

 

Note

 

In the Scan application, Prompt at Start and Prompt at End save information as a 
*.DSW file unless there are multi or cycle scans being performed. In these cases, 
information is saved in a Batch file. 

 
Commands Menu  

Commands in this application can be accessed both from the menu items at the top of 

the main window and from the application buttons on the right hand side of the screen. 
Alternatively, you can use function key shortcuts for some of the commands. These 
appear next to the item in the Commands menu.  

Start: 

Select this to start a Scan run using the currently set up parameters. 

Function key is F9. 

 

Stop: 

Select this to stop a Scan run. If you have selected Storage On in the Auto 

Store tab of the Setup dialog box, all data collected is automatically stored in the 
file specified in the Batch name field of the Windows Save As dialog box before 

or after the run commenced. Function key is F12. 

 

Connect: 

The Connect command becomes available when more than one 

software application is running at any one time. The application that is in use 

will be online and will have control of the Cary. All other applications will be 
offline and display the Connect command. If you wish to swap to a different 

Summary of Contents for Cary 5000

Page 1: ...n on computer 2 Check lens and mirror are correct for your measurement a Install Small Sample Kit mirror M3 SSK or regular M3 mirror if needed b If using SSK install correct lens L2 3 Make sure cover...

Page 2: ...e Turn on the instrument 0 I switch on the lower left side of the front of the instrument In the Scan program watch the lower left corner to see the status of the instrument When the traffic light is...

Page 3: ...mounts in front of the sample see Figure 4 There are three lenses that can be used again for the three positons marked as T C or R Each time the sample configuration is changed the optics need to be...

Page 4: ...T C and R for the three positions of the integrating sphere Also the large mirror M3 is switched out for a one with a different curvature this mirror is always kept in the T position regardless of the...

Page 5: ...on located in the upper left hand corner defines the scan parameters The following useful tabs can be found under Setup Cary tab Here you can set the units of the x and y axes nm cm 1 etc and A T R et...

Page 6: ...be applied to a sample where the abscissa range of the sample exceeds that of the baseline If you change your abscissa range to one outside that of the baseline the Cary will display an error message...

Page 7: ...x at the end of a collect where you can enter the Batch file name for your data Note In the Scan application Prompt at Start and Prompt at End save information as a DSW file unless there are multi or...

Page 8: ...multiple graphs in the Graphics area You can double click on the Graphics area to toggle the display through graph and report to graph only The graph functions can also be accessed by clicking one of...

Page 9: ...ich Text Format file How to Export Collected Data If you want to export data from a Cary WinUV application into a third party application then save your data as an ASCII CSV file To do this 1 Click Fi...

Page 10: ...eck box is not checked 8 In the File name field type in the file name for your new batch file 9 Click Save to create the new batch file The current method will be stored with the batch files All the d...

Page 11: ...SBW will change automatically to maintain the required signal level If you are collecting data in double beam mode across the UV Vis and NIR regions with Fixed SBW set as the Measurement Mode then you...

Page 12: ...nes for another Scan run you simply open the file using either the File Open Data command or click the Baseline button in the Baseline tab of the Setup dialog box Note If you decide that you do not wa...

Page 13: ...gle bounce relative SRA accessories should not use this correction Select a Baseline Zero correction instead This correction is performed with the raw transmission data and due to the double bounce on...

Page 14: ...owever sometimes you may notice that the text has turned to gray and is in italics This indicates that the Cary is currently idling outside the abscissa range of the baseline file but that the current...

Page 15: ...ferences and Graph Preferences options 1 Graph menu options Print XY point Select this to print the cursor s current X and Y coordinates in the report area This option is only available when right cli...

Page 16: ...to Arrange Graphs Select Auto Arrange Graphs to view and arrange all graphs simultaneously Copy Graph Select this to copy the Graphics area onto the Windows Clipboard Paste to Graph Select this to pas...

Page 17: ...in traces You can resize the Name of Trace and File name fields by selecting and dragging the splitter bar between the fields File Name This field displays the file name and path of the trace If the n...

Page 18: ...il the font is changed again Trace Style This field allows you to define the way that your trace will appear on screen Points Each individual data point collected by the Cary is shown on the graph Poi...

Page 19: ...e right side of each graph box A single click on a sample name or example line within the legend will make it the focused or red scan Information about the trace will be displayed below the X axis Dou...

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