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Troubleshooting
50081_Troubleshooting.fm
Page 141
Section 10
Troubleshooting
The following table is designed to help identify and solve various problems that may be
encountered while running the AutoCAT.
Problem
Category
Symptom
Probable Cause
Corrective Action
Electrical
Display does
not show up or
is too dark
No operating power
• Confirm that the power switch on the back of the instrument
has been turned ON.
• Confirm that the power cord is fully inserted into the back of
the instrument and that it is properly plugged into the wall
outlet.
• Confirm that there is power to the wall outlet.
• Verify the integrity of the fuses; change if necessary. See
Section 9.3 Replacing the Fuse
.
The screen contrast or
intensity is too low.
• While in the Methods menu, press the
0
to darken, and/or
7
to lighten until the desired screen intensity and contrast
is obtained.
Mechanical
Air bubbles
trapped in the
lines
Air bubbles have
inadvertently been
trapped while trying to
install the titrant or air is
being sucked into the
system where the tubing
is connected to the
instrument.
• Verify that the inlet tube for the titrant is secure and below the
surface of the titrant solution inside the titrant bottle.
• Verify that the all the tubing connections are tight. If the
threads of tubing connection are damaged or stripped, and
cannot be properly tightened, they must be replaced.
• Select Titrants>Burette functions>Flush. Lightly tap the
tubing while the instrument is flushing to purge air bubbles
from the system.
Titrant leaks
Titrant leaks can also
occur when the burette
seals become faulty.
Titrant leaks generally
indicate that a tubing
connector has not been
properly tightened.
• Tighten the leaking tube connection. If the tube connection
has been damaged, replace the tubing.
• Verify the integrity of the burette seals. If the burette seals are
leaking, replace the burette.
Titrant doesn’t
flow through
tubing
Loose tubing connection
• Verify that the inlet tube for the titrant is secure and below the
surface of the titrant solution inside the titrant bottle.
• Verify that the all the tubing connections are tight. If the
threads of tubing connection are damaged or stripped, and
cannot be properly tightened, they must be replaced.
Tubing is connected to the
wrong ports on the rotary
valve.
• Verify that the tubing sections are connected to the correct
ports on the rotary valve, respectively. Observe the icons.
See
Section 2.2 Instrument Assembly
Data
Collection
(w/o Auto-
scaling)
The titration is
very quick and
the resolution
of the titration
curve is too
low. The
titration curve
is too noisy.
The selected volume
increment is too large.
• Decrease the volume increment. The volume increment is
user adjustable during the titration procedure.
The titration is
very slow and
there are too
many points
before the end
point.
The volume increment is
too small.
• Increase the volume increment. The volume increment is
user adjustable during the titration procedure.
Summary of Contents for AutoCAT 9000
Page 2: ...50081_TTL fm...
Page 8: ...Page 6 50081_Safety fm...
Page 14: ...Page 12 50081_Introduction fm...
Page 24: ...Page 22 50081_OperationStop fm...
Page 34: ...Basic Operation Basic Operation Page 32 50081_Operation fm...
Page 44: ...Page 42 50081_SoftwareSetup fm...
Page 51: ...Calibration Procedures 50081_CalibrationStopper fm Page 49 Section 6 Calibration Procedures...
Page 52: ...Page 50 50081_CalibrationStopper fm...
Page 66: ...Page 64 50081_Sampling fm...
Page 67: ...Titration Procedures 50081_ProcedureStopper fm Page 65 Section 8 Titration Procedures...
Page 68: ...Page 66 50081_ProcedureStopper fm...
Page 138: ...Page 136 50081_ManualEndpoint fm...
Page 140: ...Page 138 50081_BDL fm...
Page 154: ...Page 152 50081_Titration fm...
Page 158: ...Page 156 50081_PrinterInstallation fm...
Page 160: ...Page 158 50081_ReplacementParts fm...
Page 170: ...Page 168 50081_GeneralInfoStop fm...
Page 176: ......