Endress+Hauser analytikjena PlasmaQuant 9100, Operating Manual, Page: 4 / 87

Table of contents PlasmaQuant 9100 (Elite)
4
4.4.3 Installing the argon humidifier ........................................................................................................................ 43
4.4.4 Installing the inline filter.................................................................................................................................. 44
5 Operation ........................................................................................................................................................................ 45
5.1 Switching on the emission spectrometer and igniting the plasma................................................................ 45
5.2 Switching off the emission spectrometer........................................................................................................ 46
5.3 Switching off the device via the plasma deactivation switch in an emergency ............................................ 47
5.4 Starting a measurement routine...................................................................................................................... 47
6 Troubleshooting.............................................................................................................................................................. 49
6.1 Fault messages in the software ....................................................................................................................... 49
6.2 Device faults and analytical problems ............................................................................................................. 52
7 Maintenance and care.................................................................................................................................................... 56
7.1 Maintenance overview ..................................................................................................................................... 57
7.2 Basic device maintenance ................................................................................................................................ 58
7.2.1 Cleaning the dismantleable torch.................................................................................................................... 58
7.2.2 Replacing the glass........................................................................................................................................... 60
7.2.3 Maintenance of the one-piece torch ............................................................................................................... 63
7.2.4 Cleaning the nebulizer...................................................................................................................................... 66
7.2.5 Cleaning the sample chamber and the plasma compartment ....................................................................... 67
7.2.6 Checking the gas system for leaks ................................................................................................................... 67
7.2.7 Replacing the argon hose................................................................................................................................. 68
7.2.8 Changing the plasma compartment windows ................................................................................................ 68
7.2.9 Replacing fuses ................................................................................................................................................. 71
7.2.10 Replacing the water filter................................................................................................................................. 71
7.2.11 Replacing the air filter ...................................................................................................................................... 72
7.3 Sampler maintenance ...................................................................................................................................... 72
7.3.1 Replacing the cannula and sample hose......................................................................................................... 72
7.3.2 Replacing the pump hoses of the purging pump............................................................................................ 74
7.3.3 Replacing fuses ................................................................................................................................................. 76
7.4 Maintenance of the recirculating chiller: Replacing the cooling water ......................................................... 76
8 Transport and storage .................................................................................................................................................... 78
8.1 Preparing the device for transport................................................................................................................... 78
8.2 Moving the device in the laboratory................................................................................................................ 78
8.3 Transport........................................................................................................................................................... 79
8.4 Storage .............................................................................................................................................................. 79
8.5 Recommissioning the device............................................................................................................................ 79
8.6 Installing the recirculating chiller .................................................................................................................... 80
9 Disposal ........................................................................................................................................................................... 81
10 Specifications .................................................................................................................................................................. 82
10.1 Technical data................................................................................................................................................... 82
10.1.1 Basic device technical data............................................................................................................................... 82
10.1.2 Control computer technical data...................................................................................................................... 84
10.1.3 Recirculating chiller technical data.................................................................................................................. 84
10.1.4 ASPQ 3300 sampler technical data ................................................................................................................ 85
10.1.5 Technical data for other accessories................................................................................................................ 85
10.2 Guidelines and standards................................................................................................................................. 86