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Normal operation

OPERATION MANUAL

Chapter 5

Water Cooler

Errors and omissions excepted.

V1.1.0en/13.12.12

40

5.1

Automatic operation

Hot or cold thermal fluid and surfaces
BURNS TO LIMBS

Avoid direct contact with thermal fluid and surfaces.
Wear your personnel protective equipment (e.g. temperature-resistant safety gloves, safety gog-
gles, safety footwear).

V22

5.1.1

Temperature control

[Display]

[LED display status]

[SET key]

[Arrow keys]

[Start/stop key]

5.1.1.1

Starting the temperature control process

The temperature control process can be started after filling and complete venting.

PROCEDURE

Press the

>Start/stop key<

when the temperature control unit is switched and in standby mode.

The temperature control process starts.

5.1.1.2

Ending the temperature control process

When the temperature control unit is switched off, the thermal fluid temperature is higher/lower
than room temperature
DAMAGE TO THE TEMPERATURE CONTROL UNIT AND THE GLASS APPARATUS/APPLICATION

Bring the thermal fluid up to room temperature using the temperature control unit.
Do not close shut-off valves in the thermal fluid circuit.

H13

The temperature control process can be ended at any time. Circulation is then switched off immedi-
ately.

PROCEDURE

Press the

>Start/stop key<

during circulation or temperature control modes.

The temperature control process stops.

CAUTION

The control panel:

Display and buttons

NOTE

.

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Summary of Contents for BioAcc-cool

Page 1: ...Cat No BioAcc cool Water Cooler Version 1 1 ...

Page 2: ...iagenode com info diagenode com Diagenode Inc USA NORTH AMERICA 400 Morris Avenue Suite 101 Denville NJ 07834 Tel 1 862 209 4680 Fax 1 862 209 4681 orders na diagenode com info na diagenode com For a complete listing of Diagenode s international distributors visit http www diagenode com pages distributors html For rest of the world please contact Diagenode sa ...

Page 3: ...OPERATION MANUAL V1 1 0en 13 12 12 Errors and omissions excepted Water Cooler 3 Water Cooler This operation manual is a translation of the original operation manual ...

Page 4: ...17 14 26 37 45 A Blue Red Drain Overflow Cooling water inlet only w Cooling water outlet only w Filling port Sight glass Overtemperature protec on only H Mains switch Controller Connector kit for Water Cooler 12 8 45 26 37 23 14 13 A 2 17 1 Figure 1 Connecting filling externally copen application ...

Page 5: ...AL V1 1 0en 13 12 12 Errors and omissions excepted Water Cooler 5 1 2 8 12 A Circula on flow Circula on return Drain Overflow Temperature control hose 12 8 A 2 1 Figure 2 Thermal fluid change check and internal clean ...

Page 6: ...OPERATION MANUAL Water Cooler Errors and omissions excepted V1 1 0en 13 12 12 6 ...

Page 7: ... 18 1 4 1 Air cooling 18 1 4 2 Water cooling 19 1 4 3 Consequence of inadequate energy dissipation 20 2 Commissioning 21 2 1 In plant transport 22 2 2 Unpacking 22 2 3 Ambient conditions 22 2 4 Installation conditions 24 2 5 Recommended temperature control and cooling water hoses 25 2 6 Wrench sizes and torques 25 2 7 Connecting an externally open application bath 26 2 8 Connecting to the power su...

Page 8: ...isplay error messages 44 7 2 Maintenance 45 7 2 1 Function check and visual inspection 45 7 2 2 Clean condenser fins air cooled temperature control unit 46 7 3 Thermal fluid inspection replacement and circuit cleaning 47 7 3 1 Thermal fluid inspection 47 7 3 1 1 Externally open application 47 7 3 2 Cleaning the thermal fluid circuit 47 7 4 Cleaning the surfaces 48 7 5 Inspect the mechanical seal 4...

Page 9: ...ood choice Thank you for your confidence in our products Read through this operation manual carefully prior to start up Strictly follow all notes and safety in structions Proceed with transport start up operation maintenance repairs storage and disposal in accor dance with this operation manual Subject to proper operation we offer a full warranty for your temperature control unit ...

Page 10: ...OPERATION MANUAL Water Cooler Errors and omissions excepted V1 1 0en 13 12 12 10 ...

Page 11: ...Temperature control unit with natural refrigerants NR 14 1 2 1 2 Temperature control units with 3 to 30 kg fluorinated greenhouse gases natural refrigerant 15 1 2 2 Requirements for operators 16 1 2 3 Obligations of the operators 16 1 3 General information 16 1 3 1 Description of the workstations 16 1 3 2 Safety devices to DIN 12876 16 1 3 3 Additional safety devices 17 1 3 3 1 Auto Start function...

Page 12: ...rra c behaviour EFFECT Ø Preven on Ø Resolve Ø Knowledge Severity of the residual risk Possible hazard source Possible eﬀects Preven on of errors Resolving problems Knowledge transfer Ø Step 1 Step 2 Step 3 Ø Ø Ø Step 4 PROCEDURE The procedure is explained here step by step The safety instructions in this operation are intended to protect you as the user operator and the plant from damage Safety i...

Page 13: ...d for any purposes other than temperature control in accordance with the operation manual The temperature control unit is manufactured for industrial use The temperature control unit main tains the temperature of certain applications including glass or metal reactors or other expedient items in laboratories and industry Flow through coolers and calibration baths must be used only in combination wi...

Page 14: ...work with numerous proven safe and highly sustainable technologies The relevant standards and regulations for temperature control units with natural re frigerants contain a number of stipulations the importance of complying with which is set out be low Also observe on page 12 the section Proper operation Huber temperature control units are constructed to be permanently sealed and are carefully che...

Page 15: ...between 6 and 12 months Shorter intervals can also be specified to meet tougher safety requirements Upon request we would be happy to propose a specialist company to carry out the calibration and maintenance work 1 2 1 2 Temperature control units with 3 to 30 kg fluorinated greenhouse gases natural refrigerant F Gas Directive EC No 842 2006 of the European Parliament and of the Council of 17 May 2...

Page 16: ... work station is determined by the customer s connected peripheries Accordingly it must be designed safe by the user The workstation design also depends on the applicable requirements of the Ger man occupational health and safety regulations BetrSichV and the risk analysis for the workstation 1 3 2 Safety devices to DIN 12876 Adjustable over temperature protection applicable for temperature contro...

Page 17: ...witched on the temperature control process is started only after manual input ON The temperature control unit is restored to the same status as it was before the power failure For example before the mains failure temperature is off according to this setting after the power is restored temperature control is off Automatic power outage mechanism If temperature control is active during a power outage...

Page 18: ...ooler Errors and omissions excepted V1 1 0en 13 12 12 18 1 4 Schematic illustration of the cooling variants 1 4 1 Air cooling Fresh air supply from the front Fresh air supply from below Fresh air supply from below or or Diagram Air cooling Air inlet ...

Page 19: ...Introduction Chapter 1 OPERATION MANUAL V1 1 0en 13 12 12 Errors and omissions excepted Water Cooler 19 1 4 2 Water cooling Diagram Water cooling Water connection ...

Page 20: ...igerant circuit Consequences of inadequate refrigerant quantity rising condensation temperature Not all the cool ing capacity from the refrigerant circuit is available at the evaporator This means reduced energy transmission from the thermal fluid circuit Thermal fluid circuit Consequence of inadequate energy dissipation from the thermal fluid The thermal fluid can only dissipate the energy from y...

Page 21: ...plant transport 22 2 2 Unpacking 22 2 3 Ambient conditions 22 2 4 Installation conditions 24 2 5 Recommended temperature control and cooling water hoses 25 2 6 Wrench sizes and torques 25 2 7 Connecting an externally open application bath 26 2 8 Connecting to the power supply 27 2 8 1 Connection using socket with protective earth PE 27 2 8 2 Connection via direct wiring 27 ...

Page 22: ...ature control unit Always contact your forwarding agent regarding the settlement of claims 2 3 Ambient conditions Unsuitable ambient conditions unsuitable installation SERIOUS INJURY CAUSED BY CRUSHING Observe the stipulations in section Ambient conditions and Installation conditions V03 Make sure there is adequate fresh air available at the site for the circulation pump and the compres sors The w...

Page 23: ...be located under a bench Can be located under a bench Front min 20 min 20 Right min 20 min 20 Left min 20 min 20 Rear min 20 min 20 Ambient temperature values are provided on the technical data sheet to ensure trouble free op eration compliance with the ambient conditions is mandatory Maximum relative humidity 80 to 32 C and to 40 C decreasing linearly to 50 Short distance to supply connections Th...

Page 24: ...torized lid Metallic soundproof box Start bu on Level meter Digital mer Power cord Power bu on Output selector switch Stop bu on Water bath Dis lled water Power cord Water Cooler Power cord Dis lled water Digital mer Water Cooler Power cord Motorized lid Tube holder Connector kit for Water Cooler Tubing s Transport upright Install upright stable and without tilt Use a non combustible sealed subsur...

Page 25: ...irect contact with thermal fluid and surfaces Wear your personnel protective equipment e g temperature resistant safety gloves safety gog gles safety footwear V22 To connect applications use only temperature control hoses that are compatible with the thermal fluid used When selecting temperature hoses also pay attention to the temperature range in which the hoses are to be used 2 6 Wrench sizes an...

Page 26: ...ction 2 is attached to the connection point B of the application Make sure that the connection points A and B of the application are higher than the connection Blue 1 and Red 2 of the temperature control unit PROCEDURE Remove the screw plugs from the Circulation flow 1 and Circulation return 2 connec tions Install the connector kit For more information see the user manual Connector kit for Water C...

Page 27: ... not use a power supply cable over 3 m long G02 Incorrect power supply connection DAMAGE TO THE TEMPERATURE CONTROL UNIT Your existing building power supply voltage and frequency must match the temperature control unit values on the rating plate H07 In case of uncertainties about an existing protective earth PE have the connection inspected by an electrician 2 8 2 Connection via direct wiring Conn...

Page 28: ...Commissioning OPERATION MANUAL Chapter 2 Water Cooler Errors and omissions excepted V1 1 0en 13 12 12 28 ...

Page 29: ...he temperature control unit 30 3 1 1 General functions 30 3 1 2 Other functions 30 3 2 Information on the thermal fluids 30 3 3 Testing planning 31 3 4 Display and control instruments 32 3 4 1 Display 32 3 4 2 LED display status 32 3 4 3 Arrow keys 32 3 4 4 SET key 32 3 4 5 Start Stop key 32 3 5 Menu navigation 33 3 6 Function examples 33 3 6 1 Display of the Setpoint 33 3 6 2 Setting change the s...

Page 30: ...et for the thermal fluid to be used must be read prior to use and its contents respected Observe the local regulations work instructions Wear your personnel protective equipment e g temperature resistant safety gloves safety gog gles safety footwear Risk of slipping on dirt on the floor and around the workplace V07 Non compliance with the compatibility between the thermal fluid and your temperatur...

Page 31: ...ature control results and damage Always use only the thermal fluids recommended by the manufacturer and only within the usable temperature and pressure range With a temperature control near to the boiling point of the thermal fluid the application should be at around the same height level or above the temperature control unit During filling the thermal fluid must be around room temperature level F...

Page 32: ... 3 4 2 LED display status These LEDs provide information about the current operating status 3 4 3 Arrow keys Depending on requirements these arrow keys are used to select or change a menu point or the setpoint up or down These Arrow keys are required to enter the menu 3 4 4 SET key The SET key is used to change the setpoint temperature Thus the current setpoint temperature can be displayed and cha...

Page 33: ...has been restored tem perature control is turned off Automatic power outage mechanism If temperature control is active during a power outage the process will automatically continue after the power outage 3 6 Function examples 3 6 1 Display of the Setpoint PROCEDURE Press the SET key and hold it down The setpoint is displayed Let the SET key go The internal temperature is displayed again 3 6 2 Sett...

Page 34: ...play to show the first menu item Press the Arrow key to display the menu point C40 Press the SET key and hold it down Press the SET key and the Arrow keys and simultaneously the display toggles be tween 0 auto start function is switched on to I auto start function is switched off After the desired setting is displayed release the SET key Simultaneously press the Arrow keys and for about 1 second O...

Page 35: ...ter contains the following sections 4 1 Setup mode 36 4 1 1 Turning on the temperature control unit 36 4 1 2 Setting the setpoint 36 4 2 Filling venting off gassing and draining 36 4 2 1 Externally open application 36 4 2 1 1 Filling and venting externally open application 36 4 2 1 2 Draining externally open applications 38 ...

Page 36: ...37 Press the SET key and hold it down The setpoint is displayed Set with the desired setpoint using the Arrow keys up the temperature increases down the temperature decreases Release the SET key The new setpoint is set 4 2 Filling venting off gassing and draining 4 2 1 Externally open application 4 2 1 1 Filling and venting externally open application Non compliance with the safety data sheet for ...

Page 37: ...If the unit is over filled excess thermal fluid flows out here Hose and container must be suitable for use with the thermal fluid and tem perature Add suitable thermal fluid to the bath The thermal fluid flows over the return line into the tem perature control unit and over the flow line to the bath This forces the air inside the tempera ture control unit outside The volume expansion of the therma...

Page 38: ...control unit and the drain hose into the container Wait until the external application and the temperature control unit are empty Open the connection Circulation flow 1 Open the connection Circulation return 2 Leave the temperature control unit open for a while for to allow it to dry out and the residue to drain Without screw caps with Drain valve 4 open Close the Drain valve 4 by turning clockwis...

Page 39: ...rors and omissions excepted Water Cooler 39 5 Normal operation This chapter contains the following sections 5 1 Automatic operation 40 5 1 1 Temperature control 40 5 1 1 1 Starting the temperature control process 40 5 1 1 2 Ending the temperature control process 40 ...

Page 40: ...ress the Start stop key when the temperature control unit is switched and in standby mode The temperature control process starts 5 1 1 2 Ending the temperature control process When the temperature control unit is switched off the thermal fluid temperature is higher lower than room temperature DAMAGE TO THE TEMPERATURE CONTROL UNIT AND THE GLASS APPARATUS APPLICATION Bring the thermal fluid up to r...

Page 41: ... 6 OPERATION MANUAL V1 1 0en 13 12 12 Errors and omissions excepted Water Cooler 41 6 Interfaces This chapter contains the following sections 6 1 Interface at the temperature control unit optional 42 6 1 1 Jack RS232 42 ...

Page 42: ...he temperature control unit optional 6 1 1 Jack RS232 A PC a SPS or a Process Control System PCS can be connected to this jack for remote control of the controller electronics Pin Signal Description Wiring RS232 2 RxD Receive Data 3 TxD Transmit Data 5 GND Signal GND Interfaces at the Minichiller top side Pin assignment ...

Page 43: ...enance 45 7 2 1 Function check and visual inspection 45 7 2 2 Clean condenser fins air cooled temperature control unit 46 7 3 Thermal fluid inspection replacement and circuit cleaning 47 7 3 1 Thermal fluid inspection 47 7 3 1 1 Externally open application 47 7 3 2 Cleaning the thermal fluid circuit 47 7 4 Cleaning the surfaces 48 7 5 Inspect the mechanical seal 48 7 6 Plug contacts 48 7 7 Deconta...

Page 44: ...ignal level alarm Thermoregulation is inactiv Pump off compressor off heating off Check level Reset only possible if level ok E2 flashing Inlet E1 indicates failure Pump is running and circulation is missing or pump is running and water pressure is missing Thermoregulation is inactiv Pump off compressor off heating off Reset only possible if disconnected from the power supply E3 flashing Even thou...

Page 45: ...ose connections prior to switching on the temperature control unit User and or operators A Inspection in accordance with the F Gas Directive In accordance with the F Gas Directive See page 15 section Temperature control units with 3 to 30 kg fluorinated greenhouse gases natural refrigerant User A Inspect power supply cable Prior to switching on the temperature control unit or on relocation Do not ...

Page 46: ...ation grille to create unhindered access to the condenser fins Clean the condenser fins using suitable cleaning appliances Make sure the condenser fins are not damaged or deformed as this will impair the air flow Re mount the ventilation grille after cleaning work Connect the temperature control unit to the power supply Switch on the temperature control unit PROCEDURE Ventilation grille on the und...

Page 47: ...o avoid boiling delays with future usage e g using a silicone oil at temperatures above approx 100 C the internal components of the temperature control unit must be dried out PROCEDURE Drain the temperature control unit and the externally open application as described on page 38 in section Draining externally open applications After draining residual thermal fluid can remain in the pump chamber an...

Page 48: ...tacts with the protective caps supplied Clean surfaces damp H22 A standard stainless steel cleaning agent is suitable for cleaning the stainless steel surfaces Carefully clean paint surfaces damp using the suds of a mild detergent 7 5 Inspect the mechanical seal No visual inspection of the collecting container DAMAGE INSIDE THE TEMPERATURE CONTROL UNIT CAUSED BY OVERFLOW FROM THE COLLECT ING CONTA...

Page 49: ... the materials used Consult the relevant safety data sheet A pre prepared return slip is available for download at www huber online com V19 You as the user are responsible for carrying out decontamination BEFORE third party personnel come into contact with the temperature control unit Decontamination must be carried out BEFORE the temperature control unit is returned for repair or inspection clear...

Page 50: ...Service maintenance OPERATION MANUAL Chapter 7 Water Cooler Errors and omissions excepted V1 1 0en 13 12 12 50 ...

Page 51: ...ng sections 8 1 Safety instructions and basic principles 52 8 2 Switch off 53 8 3 Packing 53 8 4 Shipping 53 8 5 Disposal 53 8 6 Telephone numbers and company address 54 8 6 1 Telephone number Customer Support 54 8 6 2 Telephone number Sales 54 8 6 3 Email adress Customer Support 54 8 6 4 Email adress Technical Support 54 8 7 Certificate of Compliance 54 ...

Page 52: ... respiratory tract The safety data sheet for the thermal fluid to be used must be read prior to use and its contents respected Observe the local regulations work instructions Wear your personnel protective equipment e g temperature resistant safety gloves safety gog gles safety footwear Risk of slipping on dirt on the floor and around the workplace V07 Hot or very cold thermal fluid SERIOUS BURNS ...

Page 53: ...ontrol unit upright on a pallet Protect attachments from damage during transport During transport place the temperature control unit on squared timber to protect the cas tors feet Secure with tensioning belts lashing straps rated for the weight concerned Additionally secure depending on model with plastic film cardboard and straps 8 5 Disposal Uncontrolled or incorrect opening of the refrigerant c...

Page 54: ...re control unit 8 6 1 Telephone number Customer Support Belgium Europe 32 4 364 20 50 USA North Ameriac 1 862 209 4680 8 6 2 Telephone number Sales Belgium Europe 32 4 364 20 50 USA North America 1 862 209 4680 8 6 3 Email adress Customer Support Belgium Europe custsupport diagenode com USA North America custsupport na diagenode com 8 6 4 Email adress Technical Support Belgium Europe techsupport d...

Page 55: ...Annex Chapter 9 OPERATION MANUAL V1 1 0en 13 12 12 Errors and omissions excepted Water Cooler 55 9 Annex Technical data sheet Replacement part list Connection diagram ...

Page 56: ... Fax 0781 57211 www huber online com Chiller with air cooled refrigerating unit and circulation pump Evaporator cooler tank and housing of stainless steel Pressure suction pump made of industrial plastic material Digital Temperature adjustment and digital temperature display Level indicator with sight glass Special Case Acetone and Polyglycol The plastic pump is not resistant against acetone and p...

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Page 58: ......

Page 59: ...PAGE 55 www diagenode com ...

Page 60: ...orders diagenode com orders na diagenode com www diagenode com ...

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