Bruker M1 MISTRAL, User Manual

Page: 5 / 122

Table of Figures
M1 ORA/MISTRAL
5
Table of Figures
Fig. 1 Safety equipment on the front panel of the M1 ORA/MISTRAL .............................. 16
Fig. 2 Schematic visualization of the X-ray fluorescence process in an atom .................. 18
Fig. 3 Schematic working principle of a silicon drift detector (SDD) .................................. 21
Fig. 4 Origin of a X-ray fluorescence spectrum ................................................................. 22
Fig. 5 Fitting process with two Gaussian shaped profiles ................................................. 23
Fig. 6 Definition of the full width at half maximum (FWHM) .............................................. 24
Fig. 7 Typical XRF spectra of glass, precious metal alloy and steel ................................. 24
Fig. 8 M1 ORA with computer ........................................................................................... 29
Fig. 9 M1 MISTRAL with computer .................................................................................... 29
Fig. 10 Main components of the M1 ORA/MISTRAL ........................................................... 30
Fig. 11 Room planning for the installation of the M1 ORA/MISTRAL ................................. 33
Fig. 12 „Run as administrator“ option for program installation ............................................ 35
Fig. 13 Select setup language. ............................................................................................ 36
Fig. 14 Select type of installation ......................................................................................... 36
Fig. 15 Select folder for installation ..................................................................................... 37
Fig. 16 Select data folder ..................................................................................................... 37
Fig. 17 Select components for installation ........................................................................... 38
Fig. 18 Installation of the video driver software ................................................................... 38
Fig. 19 Installation of Acrobat Reader ................................................................................. 39
Fig. 20 Installation of XML Notepad .................................................................................... 39
Fig. 21 Restart of the computer and creation of a new XSpect Pro database .................... 40
Fig. 22 Windows Device manager after connecting the M1 ORA/MISTRAL ...................... 41
Fig. 23 Properties dialog for the M1 ORA/MISTRAL before installing the correct driver .... 41
Fig. 24 Setting the driver path manually for the unknown devices ...................................... 42
Fig. 25 Windows security warning during driver installation ................................................ 42
Fig. 26 Finishing the successful instrument driver installation ............................................ 42
Fig. 27 Status display during initialization of the XSpect Pro program ................................ 46
Fig. 28 Switching on the high voltage .................................................................................. 46
Fig. 29 Main screen of the XSpect Pro program ................................................................. 47
Fig. 30 Additional information dialog ................................................................................... 49
Fig. 31 Stage control for the manual Z stage ...................................................................... 50
Fig. 32 Stage control for the motorized Z stage .................................................................. 50
Fig. 33 Stage control for the motorized X-Y-Z stage ........................................................... 51
Fig. 34 Cross hair parameters dialog .................................................................................. 52
Fig. 35 Video settings dialog ............................................................................................... 53
Fig. 36 Save dialog .............................................................................................................. 53
Fig. 37 Main screen of the System spectra workspace ....................................................... 54
Fig. 38 Recording reference spectra ................................................................................... 55
Fig. 39 Recording pure element spectra ............................................................................. 56
Fig. 40 Recording primary spectra ...................................................................................... 57
Fig. 41 Recording standard sample spectra ........................................................................ 58
Fig. 42 Measurement workspace ........................................................................................ 59
Fig. 43 Selection of an existing measurement method ....................................................... 61
Fig. 44 Pre-examination tab ................................................................................................ 62
Fig. 45 Measurement workspace - Results tab ................................................................... 63
Fig. 46 Measurement workspace - Table tab ...................................................................... 63
Fig. 47 Measurement workspace - Trend tab ...................................................................... 64
Fig. 48 Measurement workspace – Spectrum tab ............................................................... 65
Fig. 49 Touch screen user interface .................................................................................... 68
Fig. 50 Stage program screen ............................................................................................. 69
Fig. 51 Selection or creation of a stage program ................................................................ 70
Fig. 52 Graphic display of the stage program ..................................................................... 71
Fig. 53 Table of measurement positions ............................................................................. 72
Fig. 54 Create/edit a stage program .................................................................................... 73
Fig. 55 Status display during initialization of the XData program ........................................ 75
Fig. 56 Start-up screen of the XData program .................................................................... 76
Fig. 57 Standards workspace .............................................................................................. 77