Thermo Scientific TSQ Altis, Руководство по оборудованию

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D
Setting Up Sample Introduction Techniques
Setting Up Injections Using the Autosampler
Thermo Scientific TSQ Altis, Quantis, and Fortis Hardware Manual 139
3. Use a Rheodyne fitting to connect one end of the Teflon tubing (3) to Port 3. Place the
other end in a waste container, not shown.
4. Use red PEEK tubing (5) to connect Port 5 (fingertight fitting) to bring in the LC pump
flow.
5. Connect the red PEEK tubing (6) from Port 6 to the API source.
• To connect to the H-ESI source go to in Chapter 14 .
• To connect to the APCI source go to “Connecting the Sample Flow to the APCI
Source,” in Chapter 14 .
Figure 72. Injector valve set up
Setting Up Injections Using the Autosampler
You can use the software to automatically inject a set of sample from the autosampler. In a
typical LC/MS experiment, solvent flow goes through an LC column to separate the
compounds of a mixture before they are directed into the API source.
1. Use red PEEK tubing, Figure 73 , and a Rheodyne fitting to connect Port 2 of the
divert/inject valve to one of the following:
• The outlet of the autosampler (not shown)
• The outlet of a column that is attached to the autosampler (not shown).
No. Description
1. Sample loop (across Port 1 and 4)
2. Sample input Port 2
3. Teflon tubing for waste Port 3
4. Sample loop (across Port 1 and 4)
5. Red PEEK from LC pump Port 5
6. Red PEEK to MS Port 6
3
2
1
5
4
6
3
2
1
6
5