ME12044A
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Contents
1.
OVERVIEW.................................................................................................................................. 1
2. PRINCIPLE OF MEASUREMENT ............................................................................................ 2
3.
CONFIGURATION...................................................................................................................... 3
4.
SPECIFICATIONS....................................................................................................................... 5
4.1 Goniometer Section...................................................................................................................5
4.2
Counter and Electronic Circuit Section .......................................................................................5
5. INSTALLATION.......................................................................................................................... 6
5.1 Preparations for Adjustment ......................................................................................................6
5.2
Adjustment of Optical Axes.......................................................................................................8
5.2.1 Setup of the divergence slit (DS) .....................................................................................8
5.2.2
Model with a direct-beam monitor ...................................................................................8
5.2.3
Model without a direct-beam monitor ...............................................................................9
6.
MEASUREMENT ...................................................................................................................... 10
6.1
Preparations for Measurement.................................................................................................10
6.2
Adjustment of the Monochromator ...........................................................................................10
6.3 Adjustment of the Detector .....................................................................................................10
6.4
Measurement .........................................................................................................................10
6.5
Example of Measurement........................................................................................................11
6.5.1
Installing the analyzing crystal.......................................................................................11
6.5.2 Moving the goniometer .................................................................................................11
6.5.3
Setting the detector provisionally....................................................................................12
6.5.4
Setting the slits .............................................................................................................12
6.5.5
Adjusting the monochromator ........................................................................................13
6.5.6
Adjusting the detector ...................................................................................................16
6.5.7
Measurement...............................................................................................................18
6.6
Switching the Measurement Mode ...........................................................................................19
7.
WARRANTY .............................................................................................................................. 22
8. WARNINGS................................................................................................................................ 23
9. MAINTENANCE AND SAFETY............................................................................................... 24
10.
TROUBLESHOOTING ............................................................................................................. 25
11.
WHEN A SIX-SAMPLE CHANGER IS IN USE (OPTIONAL ITEM).................................... 26
11.1
General..................................................................................................................................26
11.2
Configuration..........................................................................................................................26
11.3
Operating Method...................................................................................................................27
11.3.1
Mounting the sample holders .........................................................................................27
11.3.2
Mounting the turret.......................................................................................................27
11.3.3
Installing the sample changer in the equipment and connecting it ......................................27
11.4
Software Operation.................................................................................................................28
11.4.1
Setup...........................................................................................................................28
11.4.2
Operation.....................................................................................................................28
11.4.3
Measurement conditions ...............................................................................................29
11.4.4
Set-reset Mode Measurement .......................................................................................30
