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Table of Contents

AZURA V 2.1S User Manual, V6860, Version 2.2

Table of Contents

Note:

For your own safety, read the manual and always observe the warnings

and safety information on the device and in the manual.

Intended Use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Device Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Valves and Valve Drives . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Front View . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Rear View . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Valve Types . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

2-Position Valves . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Multiposition Valves . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Valve Drives . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Seals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Eluents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Scope of Delivery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Signal Words . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

Decontamination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

Symbols and Signs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

Contact Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

Transport . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

Operating Environment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

Space Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

Installation Site . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

Setup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

Unpacking . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

Checking the Scope of Delivery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

Mounting the Valve onto the Valve Drive . . . . . . . . . . . . . . . . . . . . . . . . 18

Setting the Valve Mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

Screwing the Adapter Plate onto the Valve Drive . . . . . . . . . . . . . . . . 19

Screwing the Valve onto the Valve Drive . . . . . . . . . . . . . . . . . . . . . . 20

Содержание Azura V 2.1S

Страница 1: ...Valve Drive V 2 1S User Manual V6860 HPLC...

Страница 2: ...Note The contents of this user manual apply for the BlueSha dow product Please submit a request on any article numbers for BlueShadow...

Страница 3: ...es 8 2 Position Valves 8 Multiposition Valves 9 Valve Drives 10 Seals 10 Eluents 11 Scope of Delivery 12 Safety 12 Signal Words 14 Decontamination 14 Symbols and Signs 15 Installation 15 Contact Data...

Страница 4: ...ystems Separately in a LAN 26 Connecting the Remote Connector 26 GROUND 27 HOME 27 BIN 0 3 28 Binary Code 28 Ground 29 Operation 29 Operating with the Keypad 29 Operation with Chromatography Software...

Страница 5: ...Information 47 Warranty Conditions 47 Transport Damage 47 Index 48 Declaration of Conformity 50 To whom it may concern In case you prefer a French language user manual for this product submit your req...

Страница 6: ...s have 6 ports and 3 channels 6P 3C multiposition valves have 1 channel always Operating Ranges Among others the device can be used for analytical or purification tasks Device Overview Various types o...

Страница 7: ...ce connections for external devices symbols warning signs and serial number External devices can be connected to the valve drive in three different ways via remote connector via LAN connector within a...

Страница 8: ...valves the input output port is not counted Valves are available in stainless steel or PEEK and with 1 8 or 1 16 connectors 2 Position Valves 2 position valves are used for injection column switching...

Страница 9: ...s e g the selection of elu ents columns or for fractionating of eluate Multiposition valves are employed for fractioning if the form and the size of the fraction containers should be freely selectable...

Страница 10: ...3C valves and 6P multi position valves operate on the same valve drive Note Submit any questions about the possible combinations between valves and valve drives to the Technical Support of KNAUER All...

Страница 11: ...h in the perti nent literature and is only a recommendation If there is any doubt contact the Technical Support Legend 1 biconical seal 2 Dynaseal 3 screw fitting with ferrule Fig 6 seals Material pH...

Страница 12: ...ratory technicians or have completed comparable vocational training The following knowledge is required Fundamental knowledge of liquid chromatography Knowledge regarding substances that are suitable...

Страница 13: ...by the accident insurance compa nies for laboratory work Filtration of substances under analysis Use of inline filters Once they have been used never re use capillaries in other areas of the HPLC syst...

Страница 14: ...tem in potentially explosive atmospheres without appropriate protective equipment For further information contact the Technical Support of KNAUER Decommissioning the Device Securely At any time take t...

Страница 15: ...ately and disposed of properly Symbols and Signs The following symbols and signs can be found on the device in the chromatog raphy software or in the user manual Installation This chapter describes al...

Страница 16: ...Clasp the device at its side panels and lift it out of the packaging Do not hold onto front cover or leak tray Operating Environment Only if the requirements for ambient conditions of the operating en...

Страница 17: ...om the mains Installation Site air humidity below 90 non condensing temperature range 4 40 C 39 2 104 F Setup Prior to setting up the device find a suitable place according to the require ments and re...

Страница 18: ...P multiposition valves Note While setting the valve mode switch the device off Switch on the device after the configuration so that the changes become effec tive Switch Assignment 3 Remove the foam in...

Страница 19: ...ermitted 16P multiposition valve 2 ON BIN 0 2 at 6P multi position valves BIN 0 3 BIN 0 3 OFF RS 232 manual Pos 1 I L RS 232 manual Pos 1 I L RS 232 manual Pos 1 I L 3 ON output OUT BIN 3 output OUT B...

Страница 20: ...Device defect Device damage due to blocked eluent flow Check that the number of valve ports is identical with the type of valve drive 6V 12V 16V Note The sample loop is not included with the delivery...

Страница 21: ...ng on one end and a long fitting on the other end Prerequisites The ends of the sample loop were cut straight at a right angle to the capillary axis The Dynaseals are at hand Process Figure 1 Switch t...

Страница 22: ...into port 2 and port 5 Fig 10scheme of an installed sample loop Process Figure 1 Insert one end of the sample loop into the screw fitting 1 2 Push the ferrule onto the capillary so that the broader si...

Страница 23: ...to the Computer This section describes how to set up an HPLC system in a local area network LAN and how a network administrator can integrate this LAN into your com pany network The description applie...

Страница 24: ...ows 7 For the network adapter the option Allow the com puter to turn off this device to save power in the Device Manager must be deactivated Process 1 In Windows 7 choose Start Control Panel Network a...

Страница 25: ...er is preset at the factory You will find a label at the bottom side of the router on which IP address user name and password are printed These infor mation help to open the router configuration Proce...

Страница 26: ...the device configuration of the chroma tography software We recommend to use the same port number for all devices in the same system Note The port is set to 10001 at the factory You must use the same...

Страница 27: ...tion without a current flow HOME If the valve is controlled by HOME it has priority over control via RS 232 or manual operation As long as the switch off signal is not canceled the valve cannot be sta...

Страница 28: ...tch of the device was set for the binary control Signal Explanation GROUND Ground connection for start and error signals HOME POS 1 Connection for short circuit for creating a switch signal Valve driv...

Страница 29: ...Operation You have several options to select one port with the valve drive with chromatography software with the keypad with the Pin Header see Connecting the Remote Connector on page 26 Note It is n...

Страница 30: ...olled with e g OpenLAB EZChrom edition ChromGater or ClarityChrom You find a detailed description on the chromatography software in the corre sponding user manual Switch On and Self Test Prerequisites...

Страница 31: ...s inherited If several valves are switched in series then all positions will be changed Note The valve position can be changed during operation The change takes effect immediately Next Steps Start the...

Страница 32: ...le at port 1 The sample runs into the sample loop port 2 and 5 and excessive sample is transported into the waste container through port 6 2 The valve is switched from load to inject 3 The pump port 4...

Страница 33: ...ransported to the column for separa tion Legend port 1 sample injection port 2 sample loop port 3 column port 4 pump port 5 sample loop port 6 waste Fig 20valve position load Legend port 1 sample inje...

Страница 34: ...nts on different columns Note Make sure there is no pressure when switching between the columns so that the columns are not damaged Functional Principle From the valve the sample is transported throug...

Страница 35: ...ecolumn The precolumn is used in chromatography for example in the following cases preseparation or separation of heavily retarding substances Functional Principle From the valve the column 1 is fille...

Страница 36: ...From the valve the precolumn 1 is filled with sample through the channel 2 3 From the channel 6 1 the quickly dissolved substances on the column 2 are separated while the heavily retarding substances...

Страница 37: ...KNAUER docu ment and includes the following definition of customer requirements and acceptance terms documentation on device specifications device functionality check at installation site Test Interva...

Страница 38: ...set for controlling Did the device receive an IP address 6 Turn off all devices router and computer Firstly turn on the router and sec ondly turn on the devices and the computer Has this been successf...

Страница 39: ...smooth surfaces of the device can be cleaned with a mild commercially available cleaning solution or with isopropanol Valve Assembly The valve contains a rotor in its housing With disk springs the ro...

Страница 40: ...te During disassembly make sure to mark the position of the rotor seal on the cylinder pins to make the assembly of the valve easier Legend 1 axial plate 2 axial needle bearing 3 compensation plate 4...

Страница 41: ...rotor seal 4become visible 4 Remove the rotor seal 5and deposit in the correct orientation Mark posi tion and installation position of the rotor seal 5 Hold the inner components and turn over the bott...

Страница 42: ...29multiposition valve position of the rotor seal 2 position valves Fig 302 position valve position of the rotor seal temperature range 4 40 C 39 2 104 F air humidity below 90 humidity non condensing...

Страница 43: ...drive with 6P 3C valve PEEK 1 8 AWA10AE valve drive with 6P multiposition valve PEEK 1 16 AWA10BB valve drive with 6P multiposition valve SS 1 8 AWA10BC valve drive with 6P multiposition valve PEEK 1...

Страница 44: ...tion valve 1 16 SS 50 bar with accessories A1379 16P multiposition valve 1 16 SS 100 bar with accessories A1379 1 Name Order No 6P 3C injection valve 1 16 SS with accessories A1357 6P 3C injection val...

Страница 45: ...6P multiposition valve 1 16 1 8 Vespel A0880 rotor seal 6P multiposition valve 1 16 0 3 mm bore size Ves pel A0880 1 rotor seal 6P multiposition valve 1 16 Tefzel A1586 rotor seal 6P multiposition va...

Страница 46: ...r belongs to category 8 and 9 which among others comprise laboratory equipment All distributors and importers are responsible for the disposal of old devices as defined by the WEEE directive End users...

Страница 47: ...to the manufacturer at the time the damage occurs wear parts fuses glass parts columns light sources cuvettes and other opti cal components damage caused by negligence or improper operation of the de...

Страница 48: ...er 23 control 2 position valve 8 binary 28 multiposition valve 9 D decontamination 14 delivery 12 DIP switch 10 18 disk spring 40 41 Dynaseal 10 E eluent list 11 G ground 29 I inject 33 installation a...

Страница 49: ...l 31 install 21 PEEK 21 scheme 22 stainless steel 22 seal 10 40 self test 30 setup 17 software 23 30 solvent flammability 13 line 13 self ignition point 14 tray 13 space requirements 16 spare parts 12...

Страница 50: ...ing standards Machinery Machinery Directive 2006 42 EC Cord Sets IEC 60799 1998 EMC EMC Directive 2004 108 EC IEC 61000 3 2 2009 IEC 61326 1 2011 Disposal RoHS Directive 2011 65 EU WEEE Directive 2002...

Страница 51: ...ed in Germany on environmentally friendly paper from sustainable forests AZURA are registered trademarks of KNAUER Wissenschaftliche Ger te GmbH Please find up to date manuals online www knauer net do...

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