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6
Bath Use
CAUTION:
Read this section entitled BATH USE before placing the bath
in service.
The information in this section is for general information only. It is not de-
signed to be the basis for calibration laboratory procedures. Each laboratory
needs to write their specific procedures. Some of the information in this text
may not apply to the specific bath you have purchased.
6.1
General
Be sure to select the correct fluid for the temperature range of the calibration.
Bath fluids should be selected to operate safely with adequate thermal proper-
ties to meet the application requirements. Also, be aware that fluids expand
when heated and could overflow the bath if not watched. Refer to General Op-
eration, Section 9, for information specific to fluid selection and to the MSDS
sheet specific to the fluid selected. Generally, baths are set to one temperature
and used to calibrate probes only at that single temperature. This means that the
type of bath fluid does not have to change. Additionally, the bath can be left en-
ergized reducing the stress on the system.
The bath generates extreme temperatures. Precautions must be taken to prevent
personal injury or damage to objects. Probes may be extremely hot or cold
when removed from the bath. Cautiously handle probes to prevent personal in-
jury. Carefully place probes on a heat/cold resistant surface or rack until they
are at room temperature. It is advisable to wipe the probe with a clean soft cloth
or paper towel before inserting it into another bath. This prevents the mixing of
fluids from one bath to another. If the probe has been calibrated in liquid salt,
carefully wash the probe in warm water and dry completely before transferring
it to another fluid. Always be sure that the probe is completely dry before in-
serting it into a hot fluid. Some of the high temperature fluids react violently to
water or other liquid mediums. Be aware that cleaning the probe can be danger-
ous if the probe has not cooled to room temperature. Additionally, high temper-
ature fluids may ignite the paper towels if the probe has not been cooled.
For optimum accuracy and stability, allow the bath adequate stabilization time
after reaching the set-point temperature.
6.2
Triple Point of Water Cell Maintenance
6.2.1
Bath Preparation
The bath fluid to maintain the TPW cell must be able to operate near 0
°
C with-
out freezing. Water alone can freeze. Water with about 10% ethanol is a good
fluid for this application. It retains most of the excellent temperature control
properties of water while reducing the freezing point to a useable level. The
21
6 Bath Use
General
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