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ADC 2

4.4. Developing and preconditioning solvent

The inlet reservoirs for developing (mobile phase) and precondi-
tioning solvents are located on top of the ADC2. The left inlet is
used for developing solvent and the right inlet for precondition-
ing solvent. The volume of developing solvent should be 10ml,
the preconditioning volume 25ml.

Developing Preconditioning
solvent (10ml)

solvent (25ml)

Fig.11: Inlet reservoirs

Manual, August 2005

Page 15

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Содержание ADC 2

Страница 1: ...s dried with air and finally stays safely protected in the chamber until removed by the user If used in Stand Alone mode all method parameters are en tered via the keypad Ten complete development prog...

Страница 2: ...cords without ground contact Instrument data Mains voltage 100 240 V Frequency 50 60 Hz Power consumption 20 W Some internal parts of the instrument are under AC power un authorized manipulations can...

Страница 3: ...hed off and secured in a way that prevents it from being switched on ac cidentally Shipping the instrument is permitted only in the original con tainer Improper handling or packing can cause damage to...

Страница 4: ...nk to winCATS B 022 8350 E Manual English 1 4 Options Part Description 022 8360 Humidity Control Module 115 8363 Foil holder old New magnet holder 022 8373 125 1026 Ethernet cable 3m gray 125 1027 105...

Страница 5: ...is complete 9 Remove the instrument carefully from the package and place it on a table Attention Do not pull out the instrument by holding it at the blue top cover hold the instrument at the bottom wh...

Страница 6: ...Option additional for tubes 250mm Height 520mm Weight 18 5kg Operating temperature The temperature should be within a range of 18 to 30 degrees centigrade and free from significant varia tions Humidit...

Страница 7: ...e the instrument near equipment that generates intense magnetic fields such as electric welding equipment high frequency furnaces pole transformers etc Protect the instrument from excessive dust Conne...

Страница 8: ...ion to the PC The CAMAG ADC2 is shipped with a 9 pin RS 232 interface cable for connection to the PC If you wish to use the instrument controlled by winCATS 9 Connect the cable to the instrument and t...

Страница 9: ...ins an exhaust tube witch can be slipped onto the black air outlet fig 4 permitting exhaust solvent vapor to be directed into a fume hood or other vent Fig 4 Mounting the exhaust tube to the air outle...

Страница 10: ...hapter 6 8 3 2 Checking system functions Switch on the instrument The ADC2 will now show the installed firmware version and perform the following checks and tasks 1 Initializing the drying module 2 In...

Страница 11: ...a plate into the plate holder the TLC layer side must be facing the user the text LAYER Fig 5 Insert TLC plate in plate holder Fig 6 Plate clamped in Plate holder Important After being clamped the HPT...

Страница 12: ...underneath the respective down holders fig 7 Fig 7 Mounting a foil into a foil holder 4 2 Drying module and plate lift To attach the plate or foil holder into the drying module approach the holder to...

Страница 13: ...s touching the two stoppers at the back otherwise chromatography cannot be started The CAMAG label of the Chamber should normally face the user strongly inhomogeneous glass walls may thus require turn...

Страница 14: ...make sure it has been in serted in the right position i e the fold of the pad is contacting the bottom of the Twin Trough Chamber while the shorter side is lying on the bulge of the chamber fig 10 Fig...

Страница 15: ...lvents are located on top of the ADC2 The left inlet is used for developing solvent and the right inlet for precondition ing solvent The volume of developing solvent should be 10ml the preconditioning...

Страница 16: ...ssing another key these measurements will be cleared ENTER Confirms the current parameter switches to the selected dialog or re starts the last selected method in manual function END Interrupts the cu...

Страница 17: ...s interrupted but all parameters remain in memory RUN Shows the selection of stored methods 9 Use the arrow keys 5 or 6 to select a method to start 9 Press ENTER to start the selected method or DIALOG...

Страница 18: ...9 Press the ENTER key to start the displayed method The last method is re started if ENTER is pressed in the SYSTEM READY mode 5 2 Procedure for local input of parameters 9 Press the RUN key The most...

Страница 19: ...ou can select the locally stored method to delete 9 Press the key combination RUN END press and hold RUN then press END and confirm deleting with ENTER Flow diagrams for these dialogs are depicted in...

Страница 20: ...or closing the door moving the lever down or proper po sitioning of the Twin Trough Cham ber INIT DRIVE Initialization of specified drive GO TO POSITION Lift or spindle drive are moved to specified po...

Страница 21: ...TEM READY Boxes with two lines on both sides include another diagram shown in the next pages RUN END Method stack Repeat last method Select manual functions Show temperature rel humidity YES NO YES EN...

Страница 22: ...he instrument display shows System ready THIS METHOD METHOD XX ENTER DIALOG RUN END Increment decrement method Start selected method END Delete selected method YES YES YES YES YES YES NO UP DOWN Back...

Страница 23: ...when the instrument display shows the name of the method to be edited in the method stack dialog ENTER END Increment decrement di alog type YES YES NO NO NO Enter selected dialog type Data changes YES...

Страница 24: ...display shows the name of the parameter type to be edited in the Dialog mode GLOBALS PARAMETERS SAVE METHOD ENTER PLATE TYPE ENTER CONTROL HUMIDITY TIME TANK SATURATION TIME PLATE PCOND TIME MIG DIST...

Страница 25: ...the instrument display shows System ready THIS FUNCTION MANUAL FUNCTION ENTER DIALOG END Select function Start selected function YES YES YES YES NO NO NO Back to Normal operation mode NO Increment or...

Страница 26: ...key wile switching on the instrument DIALOG POWER ON SHOW FIRMWARE VERSION All keys except ENTER SELECT BAUDRATE SELECT LANGUAGE SELECT LCD CONTRAST ENTER RESET ENTER RESET ENTER RESET ENTER RESET PR...

Страница 27: ...able or there are temperature prob lems e g due to sun light 39 Tolerances of TLC plate or TT Chamber too big 40 The TT Chamber has been moved during develop ment 41 The drying compartment lid has bee...

Страница 28: ...D contrast To enter the Setup dialog 9 Hold down the DIALOG key and press the RESET key 9 Release the RESET key then release the DIALOG key The display will now show ADC2 Vx xx xx Setup Mode where x x...

Страница 29: ...ent selection and move on to the LCD contrast selection 9 Press the RESET key to quit the setup dialog 7 2 3 Set the LCD contrast Start the user dialog according to the procedure above The display now...

Страница 30: ...in socket with help of a small screwdriver Press it on both sides of the holder into the recess Now you can pull out the fuse holder 9 Replace the fuse s The label 250 V 1 0 AT slow blow is valid over...

Страница 31: ...module drive Stepper motor 1600 steps rev 160 steps 0 1mm Positioning with acceleration ramp Lift drive Stepper motor 1600 steps rev 5 steps 0 1mm Positioning with acceleration ramp Dimensions Width 3...

Страница 32: ...s or coastal climates can be compared to those performed in dry winters or in highland climates 1 General saturated salt solution The desired humidity is adjusted in the ADC2 by means of a saturated s...

Страница 33: ...ues from R mpp Lexikon Chemie 9 Aufl 2 The solubility values are from K ster Friedrich W Rechentafeln f r die chemi sche Analytik Berlin New York de Gruyter 103 bearb Aufl 1985 Remarks It should be ad...

Страница 34: ...9 The ventilation valve module is mounted on a holding plate that has to be placed in the position over the four screws and tightened Next the two hoses already fixed on the ven tilation valve module...

Страница 35: ...h The connection of the gas wash bottle to the ventilation valve module is made with two pre assembled hoses 9 Connect the center hose black socket to the black horizontal socket of ventilation valve...

Страница 36: ...are for exhaust and air supply The exhaust tube has to be slipped onto the black socket fig 15 2 2 3 4 Fig 15 2 Humidity module 1 center hose 2 top cover 3 outside hose 4 exhaust hose Warning Never i...

Страница 37: ...lt so lution see page 35 fig 14 3 3 Sodium chloride rel humidity at 20 C 75 Add 360g NaCl into the gas wash bottle Add 500 mL distilled water and heat it up to 40 50 C under stirring Set the final vol...

Страница 38: ...to the adiabatic process and the energy balance during aggregate state changes A good example is shown in the graphics below 28 30 32 34 36 38 40 42 44 46 48 0 1 2 3 4 5 RH Minutes RH C Fig 16 Measur...

Страница 39: ...C plate by weighting It has been shown that within 2 5 minutes a stable equilibrium is reached for the humidifying as well as the drying process 75 rH 10 minutes Used plate material Merck HPTLC plates...

Страница 40: ...ADC 2 Manual August 2005 Page 40...

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