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Thermo Scientific Orion Star LogR™ Meter User Guide

32

mV, Relative mV and ORP Technique

mV, Relative mV and ORP Measurement

Note:  

Turn on the automatic datalog feature to send measurements to the meter 

datalog at the frequency specified in each measurement mode.  Refer to the Data 
Archiving and Retrieval section for details. If the automatic datalog feature is off, 
connect the meter to a printer or computer to record the measurements. 

1.  Rinse the electrode with distilled or deionized water.  Shake off any excess 

water and blot the electrode dry with lint-free tissue.

2.  Place the electrode into the sample.

 

a.    If the meter is in the continuous measurement mode, it will start reading 

immediately and continuously update the display.  The 

mV

 or 

RmV 

icon will 

flash until the reading is stable.  Once the reading is stable, log and print 
the measurement by pressing 

.  If the stirrer is enabled, press 

 to 

start the stirrer.  Press 

 again to turn off the stirrer before removing the 

electrode and stirrer from the sample.

 

b.   If the meter is in the AUTO-READ measurement mode, press 

 to start 

the reading.  The 

AR 

icon will flash until the reading is stable.  Once the 

reading is stable, the meter will log and print the measurement and freeze 
the display.  If the stirrer is enabled, the stirrer will turn on when 

 is 

pressed and turn off when the reading is stable.

 

c.   If the meter is in the timed measurement mode, it will start reading 

immediately and continuously update the display.  The meter will log and 
print the measurement at the frequency specified in the setup menu.  If the 
stirrer is enabled, press 

 to start the stirrer.  Press 

 again to turn off 

the stirrer before removing the electrode and stirrer from the sample.

3.  Remove the electrode from the sample, rinse it with distilled or deionized water, 

blot it dry, place it in the next sample and repeat step 2.

4.   Once all of the samples have been measured, rinse the electrode with distilled 

or deionized water and blot it dry. Consult the electrode user guide for proper 
storage techniques.

Summary of Contents for Orion Star LogR Meter

Page 1: ...Orion Star LogR Meter User Guide...

Page 2: ...c ISEasy KAP LabConnect LogR Low Maintenance Triode Minimum Stir Requirement MSR NISS One Touch One Touch Calibration One Touch Measurement Optimum Results Orion Star Pentrode pHuture MMS pHuture Pent...

Page 3: ...Table 12 General Menu Settings 14 Time and Date Settings 16 AUTO READ Continuous or Timed Measurement Settings 17 Temperature Reading and Compensation Settings 19 Selecting the Measurement Parameter 2...

Page 4: ...Meter Self Test 44 Meter Error Codes 45 General Troubleshooting 47 Chapter Xlll Meter Specifications Meter Specifications 50 Ordering Information 53 Appendix A Meter Setup Menu Features pH Setup Menu...

Page 5: ...H measurement capability includes a mV relative mV ORP function Built to meet the demands of busy multiple user laboratory or plant environments all Orion Star LogR series meters are microprocessor co...

Page 6: ...ontrol Control for the stirrer probe Cat No 096019 sold separately which eliminates the need for additional stir plates and stir bars SMART STABILITY and SMART AVERAGING Remove the guesswork by automa...

Page 7: ...2 icons indicate which pH buffers were saved after a pH calibration is performed The setup icon only appears when the meter is in setup mode The icon indicates an error condition and when it is displa...

Page 8: ...ng and Compensation Setting is currently active the resistance across the pH electrode bulb can be shown on the second line Press to move the arrow icon to between the first and second lines and press...

Page 9: ...User Guide Chapter III Keypad General Description The keypad layout is the same for the Orion Star LogR pH and pH ISE meters Stirrer On Off Measure Save Print View Log Power Line Select Digits Setup C...

Page 10: ...ibration modes Starts the calibration for the selected line in the measurement mode If the arrow icon points to the top line and the displayed units are pH pressing the key will start a pH calibration...

Page 11: ...100 to 240 VAC 0 5 A 50 60 Hz Based on your wall outlet select one of the four plug plates provided 110 V 220 V 240V and slide it into the grooves on the adapter A click will be heard when the plug i...

Page 12: ...ays be connected to a power source via the universal power supply 1 Confirm that the meter is off and gently place the meter upside down on a clean lint free cloth to prevent scratching the LCD 2 Remo...

Page 13: ...Benchtop meters have a reference input that is used to connect a separate reference electrode Reference electrodes require an separate appropriate sensing electrode for measurements Use the 8 pin min...

Page 14: ...ll stay on until is pressed To turn off the meter press and hold for about three seconds Meter Maintenance For routine meter maintenance dust and wipe the meter with a damp cloth If necessary a warm w...

Page 15: ...ne 6 To scroll through a list of options on the bottom line press until the desired option is displayed To enter a numeric value for an option on the bottom line press to adjust each digit and to move...

Page 16: ...s dUE LOGr 0 to 9999 LogR calibration alarm value in hours 0 is off 0 yes rEAd tyPE AUt0 tImE C0nt Measurement read type as AUTO READ timed or continuous AUt0 yes rEAd tInE 00 05 to 99 59 Timed measur...

Page 17: ...ation points 3 no AUt0 0rP n0 YES ORP calibration option appears if 0 was selected for PH n0 no AUt0 ISE 0 2 3 ISE calibration points appears if 0 was selected for PH 2 no 1 AUt0 ISE1 Concentration va...

Page 18: ...p the real time clock only OFF option or use the batteries for complete meter operation On option If meter is changed from On to OFF with no power adapter connected the meter will power off in 60 seco...

Page 19: ...t of options on the bottom line press until the desired option is displayed To enter a numeric value for an option on the bottom line press to adjust each digit and to move to the next digit 7 Press t...

Page 20: ...on to the middle line 4 Press to scroll through for the current hour setting for the current minute setting for the date format setting for the current month setting for the current day setting and fo...

Page 21: ...gnificantly decrease battery life In the timed mode the meter is constantly taking measurements and updating the display The meter logs and prints the measurement at the selected time interval 1 In th...

Page 22: ...Star LogR Meter User Guide 18 Meter Setup 7 Press to accept the selection and move the arrow icon to the top line 8 Repeat steps 3 through 7 to change another measurement setting or press to return t...

Page 23: ...gR pH ISE meter Cat No 3115000 The ATC setting uses the automatic temperature compensation ATC probe To use the temperature value entered under the General Menu Setting select the manual setting 1 In...

Page 24: ...The measurement lines and icons for the Star LogR meter are shown below pH mV and RmV capabilities are in all Orion Star LogR meters ISE capabilities are for Orion Star LogR pH ISE meters Cat No 3115...

Page 25: ...l be used 1 To enable the GLP function a In the measurement mode press b Press until is displayed on top line c Press to move the arrow icon to the middle line and press until is displayed d Press to...

Page 26: ...menu until is displayed on the top line 3 Press to accept the selection and move the arrow icon to the middle line 4 Press to scroll through for pH measurement resolution and for the automatic buffer...

Page 27: ...ual calibration When the pH icon stops flashing the meter will display the actual pH value read by the electrode Press until the first digit to be changed is flashing press to change the value of the...

Page 28: ...before removing the electrode and stirrer from the sample b If the meter is in the AUTO READ measurement mode press to start the reading The AR icon will flash until the reading is stable Once the re...

Page 29: ...he temperature display on the top left of the screen To view the temperature for the pH measurement line 1 In the measurement mode press to select the top display line The arrow icon will point to the...

Page 30: ...d Refer to the Appendix B for additional information Choose a temperature calibration range that is at least 5 C apart depending on your expected operating range Evenly bracket your expected sample te...

Page 31: ...tting should be LogR shown as LOgr on the third display line If this is not the case refer to the section titled Temperature Reading and Compensation Settings The first screen when starting the temper...

Page 32: ...ith distilled water Place the electrode into the solution Stir moderately Press 5 CAL 1 will display When the reading stabilizes the arrow icon and first digit will flash to display actual LogR temper...

Page 33: ...lly adjusted 1 Connect an ATC probe to the meter and change the temperature input to ATC in the setup menu 2 In the measurement mode press to choose the top measurement line and press until the temper...

Page 34: ...d Relative mV and ORP Calibration 1 Prepare the electrode according to the electrode user guide 2 In the measurement mode press until the arrow icon points to the top line press until the RmV icon is...

Page 35: ...lue of the standard To change the value to negative or positive number press until none of the digits are blinking and the arrow icon is blinking and then press to change the sign of the mV value 5 Pr...

Page 36: ...er Press again to turn off the stirrer before removing the electrode and stirrer from the sample b If the meter is in the AUTO READ measurement mode press to start the reading The AR icon will flash u...

Page 37: ...endix A for a description of the special setup menu features 1 In the measurement mode press 2 Press to scroll through the setup menu until is displayed on the top line 3 Press to accept the selection...

Page 38: ...eionized water shake any excess water off blot it dry and place the electrode into the least concentrated standard 4 Wait for ISE icon to stop flashing Press until the first digit to be changed is fla...

Page 39: ...35 Thermo Scientific Orion Star LogR Meter User Guide ISE Technique b For a two or more point calibration the meter will automatically proceed to the measurement mode after the slope is displayed...

Page 40: ...n off the stirrer before removing the electrode and stirrer from the sample b If the meter is in the AUTO READ measurement mode press to start the reading The AR icon will flash until the reading is s...

Page 41: ...anged to display pH pH millivolts mV relative millivolts RmV concentration ISE temperature no icon or a blank line ATC Probe Calibration Technique The temperature calibration mode of the Orion Star Lo...

Page 42: ...er point Automatic Datalog Feature The automatic datalog feature that can be turned on or off To enable the automatic recording of data into the datalog 1 In the measurement mode press 2 Press until i...

Page 43: ...ter or computer to clear the error message If the datalog deletion setting is set to the meter will overwrite the oldest datalog point when all 1000 datalog points are filled and will not delete the d...

Page 44: ...n and the time date and year the log was recorded will be on the top middle and bottom display lines respectively Press to scroll through the log 4 Press The meter will display the data or calibration...

Page 45: ...uter interface cable Cat No 1010053 2 Click on the start button on the lower left side of the computer screen Select All Programs Accessories Communications and HyperTerminal 3 When the HyperTerminal...

Page 46: ...ISE Meters Conforms with the following directives and standards 2004 108 EC Electromagnetic Compatibility EMC Directive EN 61326 1 2006 Electrical equipment for measurement control and laboratory use...

Page 47: ...of the Canadian Department of Communications ICES 003 Le pr sent appareil num rique n met pas de bruits radio lectriques d passant les limites applicables aux appareils num riques de la class A et B...

Page 48: ...not lit and press 5 The display will read Press every key on the keypad one at a time in any order If the keys are not pressed within five seconds of one another the display will read which indicates...

Page 49: ...another 034 BNC Input Failure Disconnect all the electrodes from the meter connect the BNC shorting cap to the meter and repeat the self test 038 Datalog Full Download the datalog to a printer or com...

Page 50: ...trode user guide Re calibrate the electrode with fresh standards 309 Bad ISE Slope Clean the electrode according to the electrode user guide Re calibrate the electrode with freshly prepared standards...

Page 51: ...lem When I press the meter displays Solution The meter is printing and cannot enter the calibration mode until the printing is done This should rarely occur if the meter is set to a 9600 baud rate If...

Page 52: ...in the setup menu is set to low Change the concentration range to high The ISE resolution is set to 3 digits in the setup menu Change the ISE resolution to 2 digits for faster stabilization of the re...

Page 53: ...starting the temperature calibration shows the setting Problem The resistance display shows Solution The resistance input is over 6000 Mohms This resistance value is normal for a new electrode not yet...

Page 54: ...nsing Storage Temperature 20 to 60 C Storage Relative Humidity 5 to 85 non condensing Pollution Degree 2 Overvoltage Category II Altitude Up to 2000 meters Weight 0 91 kg Size 9 4 cm H x 17 0 cm W x 2...

Page 55: ...ntal Operating Conditions Operating Ambient Temperature 0 to 50 C Operating Relative Humidity 0 to 90 non condensing Storage Temperature 20 to 75 C Storage Relative Humidity 0 to 90 non condensing Pol...

Page 56: ...figures Relative Accuracy 0 2 mV or 0 05 whichever is greater Displayed Units M mg L ppb or no units Calibration Features Linear point to point selectable non linear automatic blank correction and low...

Page 57: ...olution and one pint each of pH buffer 4 7 and 10 3115101 Orion Star LogR pH ISE benchtop meter with stainless steel ATC probe 927007MD PerpHecT ROSS Sure Flow electrode 8272BN and electrode stand 090...

Page 58: ...with epoxy body 9172BNWP Sure Flow combination pH electrode with glass body 927005MD ATC probe with epoxy body 927007MD ATC probe with stainless steel body 9512HPBNWP High performance ammonia combina...

Page 59: ...0 30 to 30 10 01 207 to 147 4 01 207 to 147 9 18 99 to 159 12 46 293 to 353 6 86 38 to 22 ISE Setup Menu Features Concentration Range The Orion Star LogR pH ISE meters can be set for a high or low ISE...

Page 60: ...in low level standards and samples Since the automatic blank correction feature requires the use of a set of non linear equations that can only be calculated numerically the user cannot analytically v...

Page 61: ...on using the electrical resistance of the glass sensing bulb as the temperature probe The logarithm of the resistance of the bulb varies almost linearly with the reciprocal of the absolute temperatur...

Page 62: ...e 20 C C Average Temp Compensation Error 0 to 25 C pH units Average Temp Compensation Error above 20 C pH units 8202BN 0 36 0 10 0 004 0 001 8203BN 0 13 0 02 0 002 0 000 8235BN 0 04 0 14 0 000 0 002 8...

Page 63: ...e Temp Compensation Error 0 to 25 C pH units Average Temp Compensation Error above 20 C pH units 8202BN 0 04 0 03 0 000 0 000 8203BN 0 04 0 01 0 000 0 000 8235BN 0 07 0 06 0 001 0 001 8256BN 0 04 0 06...

Page 64: ...sistance To view the electrode resistance the third line of the display indicating the temperature reading and compensation setting should show If or is shown refer to the user guide chapter 5 Tempera...

Page 65: ...esistance In most cases the initial value is not a definitive test of electrode condition except in extreme cases for example see the initial low readings information below When changing electrodes do...

Page 66: ...glass bulb increases Eventually the aging of the electrode and visible increase in resistance manifests in a slower response rate low slope and reduced immunity to noise At some point the resistance b...

Page 67: ...eter s Electrode Diagnostics Electrode Diagnostics Log Electrode SN Date Temperature Resistance Delta Notes SN 1234 example 1 1 10 350 Initial test SN 1234 example 1 8 10 20 320 Significantly low resi...

Page 68: ...fill solution Rehydrate the electrode by soaking it in the recommended electrode storage solution for one hour prior to use b for sealed electrodes soak the electrode in electrode storage solution for...

Page 69: ...s are present Refer to above note regarding air bubbles if needed iii Rehydrate by soaking the electrode in electrode storage solution for one hour Deionized Water Deionized water should not be used a...

Page 70: ...cleaning solution from the table below and follow the steps below Contaminant Orion Catalog Number Description Protein 900021 pH Electrode Cleaning Solution A Bacteria 900022 pH Electrode Cleaning So...

Page 71: ...ormance 5 Rinse the electrode thoroughly with distilled water and read the resistance of the electrode on the Orion LogR meter Repeat the cleaning procedure if the resistance value has moved closer to...

Page 72: ...er Note The printer must have a 9600 baud rate to be connected to the autosampler The Orion Star printer Cat No 1010006 is recommended for use with the Orion Star LogR meter and AutoTration 500 autosa...

Page 73: ...do not need to be reprogrammed To prevent the meter from losing the programmed parameters in the event of a power failure install four AA alkaline batteries in the meter If a pH electrode will be cali...

Page 74: ...at 3 Review and change the parameters for the autosampler in the setup menu Turn the autosampler function On or OFF Select the beaker tray that will be used Either the 28 beaker or 48 beaker tray can...

Page 75: ...e meter has ISE function and the number of pH calibration points is set to zero Press twice to move the arrow icon to the middle line and press to display the first standard value Press to move the ar...

Page 76: ...a measurement 5 The actual measurements will be shown on the display If a stirrer probe is in use the stirrer will automatically begin stirring when the measurement starts and end stirring when all m...

Page 77: ...Function To disable the autosampler press in the measurement mode to enter the setup menu Press until is displayed on top line Press until the arrow icon points to the middle line and press until is d...

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