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Spectris Particle Measuring Systems LiQuilaz II E, Operation Manual

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LiQuilaz II E and S Operations Manual

Page 1-1

Chapter 1
Getting Started

The LiQuilaz® II E and S Series Liquid Particle Counters are sensors designed to 
measure particles in liquids. A sensor contains a liquid handling and optical system as 
well as electronics that measure the size of the particles sampled and transmit data to 
the data display system. 

The sensor requires AC power, connections to bring the liquid to the sensor, and a 
connection to a data display system. Particle Measuring Systems supplies several 
software packages that support the LiQuilaz II, including Facility Net, Pharmaceutical 
Net, SamplerSight, or SamplerSight-Pharma software.

The LiQuilaz II E Series Liquid Particle Counter has the following variations:

LiQuilaz II E20P 

A 20 mL per minute version that is intended for use with the SLS-2000 sampler.

LiQuilaz II E20 

A 70 mL per minute version that is intended for an online installation.

LiQuilaz II E15P 

A 20 mL per minute version that is intended for use with the SLS-2000 sampler or 
online installation.

The LiQuilaz II S Series Liquid Particle Counter has the following variations:

LiQuilaz II S05

A 80 mL per minute version with 0.5 µm sensitivity.

LiQuilaz II S03

A 80 mL per minute version with 0.3 µm sensitivity.

LiQuilaz II S02

A 50 mL per minute version with 0.2 µm sensitivity.

NOTE:

 

All S units are also available in a 20 mL per minute flowrate version.

Summary of Contents for Particle Measuring Systems LiQuilaz II E

Page 1: ...LiQuilaz II E and S Liquid Particle Counters P N 1000023550 OPERATIONS MANUAL Without measurement there is no control ...

Page 2: ...6 E pmsfrance pmeasuring com GERMANY T 49 6151 6671 632 E pmsgermany pmeasuring com ITALY T 39 06 9053 0130 E pmssrl pmeasuring com JAPAN T 81 3 5298 8175 E pmsjapan pmeasuring com KOREA T 82 31 286 5790 E pmskorea pmeasuring com MEXICO T 52 55 2271 5106 E pmsmexico pmeasuring com NORDIC T 45 707 028 55 E pmsnordic pmeasuring com PUERTO RICO T 1 787 718 9096 E pmspuertorico pmeasuring com SINGAPOR...

Page 3: ...served No part of this document may be reproduced distributed or transmitted in any form without the prior written consent of Particle Measuring Systems The information contained in this document is subject to change without notice Quality Statement The Quality Policy of Particle Measuring Systems is to strive to meet or exceed the needs and expectations of our customers and to align the activitie...

Page 4: ...inside the instrument to alert you to potentially hazardous conditions Please familiarize yourself with this information WARNING A warning in the text is used to notify the user of the potential for bodily injury or death A caution in the text is used to highlight an item that if not done or incorrectly done could damage the instrument and or any materials or devices affected by the instrument NOT...

Page 5: ...oma ITALY Distributor s Telephone FAX 39 06 90530130 39 06 9051315 Type of Equipment Particle Counter Model No LiQuilaz II I the undersigned hereby declare that the equipment specified above conforms to the above Directive s and Standard s Signature Signature Full Name Scott MacLaughlin Full Name Giovanni Scialo Position Director of Engineering Position Vice President Life Sciences Place Boulder D...

Page 6: ...ponents and Connections 2 6 Liquid Connections 2 6 Indicator Lights 2 6 Communications Connectors 2 7 Installation Requirements 2 8 AC Fuse 2 8 Online Version Installation 2 9 Installation Requirements 2 9 Required Items That Are Not Provided 2 9 Communication Options 2 11 Facility Net 2 11 SamplerSight or SamplerSight Pharma 2 11 Modbus TCP 2 11 RS 232 2 11 Chapter 3 Maintenance 3 1 Capillary Cle...

Page 7: ...tion Commands B 1 Instrument Initialization B 1 Sample Initialization B 2 Data Processing B 2 Slow Polling B 2 Fast Polling B 3 Slow Protocol B 3 First Logical Step B 3 Second Logical Step B 4 Third Logical Step B 4 Slow Protocol Commands B 5 Detailed Description of Slow Protocol Commands and Responses B 6 Fast Protocol B 10 Formatting Data B 11 Appendix C Modbus TCP Protocol C 1 Modbus Overview C...

Page 8: ...Required Hardware and Software E 1 RS 232 Cable E 2 Setting Configuration Addresses for Ethernet E 3 Configuration Commands E 4 Viewing Configuration Settings E 6 Connecting the Ethernet Cable E 6 Appendix F Serial Communications Overview F 1 Adapters and Cables F 2 USB Serial Port Adapter F 2 USB driver for Windows F 2 Serial Cable F 3 RJ 12 Cable and Adapter F 3 Connector Signals F 4 Communicati...

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Page 10: ... 2 11 LiQuilaz II Liquid Particle Counter Online version 2 6 Figure 2 12 LiQuilaz II Liquid Particle Counter rear panel 2 7 Figure 2 13 Flared tubing 2 9 Figure 2 14 LiQuilaz II tube connections 2 10 Chapter 3 Maintenance 3 1 Figure 3 1 LiQuilaz II fittings 3 3 Figure 3 2 Capillary Cleaning Kit syringes 3 3 Figure 3 3 Pumping cleaning solution through the capillary 3 4 Figure 3 4 Screws near the t...

Page 11: ...w D 8 Figure D 5 Internet Protocol TCP IP Properties window D 9 Appendix E Configuring for Ethernet E 1 Appendix F Serial Communications Overview F 1 Figure F 1 USB serial adaptor F 2 Figure F 2 Serial cable with DE 9 male and female connectors F 3 Figure F 3 RJ 12 adaptor and cable F 3 Figure F 4 HyperTerminal window F 5 Figure F 5 PuTTY Configuration window F 6 Figure F 6 PuTTY Main window F 6 F...

Page 12: ...aceutical Net SamplerSight or SamplerSight Pharma software The LiQuilaz II E Series Liquid Particle Counter has the following variations LiQuilaz II E20P A 20 mL per minute version that is intended for use with the SLS 2000 sampler LiQuilaz II E20 A 70 mL per minute version that is intended for an online installation LiQuilaz II E15P A 20 mL per minute version that is intended for use with the SLS...

Page 13: ...e sample viscosity and dissolved gases in the sample 20 mL min 10 70 mL min 10 20 mL min 10 Size channels User adjustable from 1 to 15 Resolution Less than 10 at 10 µm Wetted surfaces Fused silica black quartz Kalrez and Kel F Liquid connections 3 mm flare or 1 4 inch Flaretek Pressure range 0 100 psi Sample temperature 50 122 F 10 50 C Maximum concentrationb b Greater than 90 accuracy less than 1...

Page 14: ... w h 12 75 4 25 4 5 in 32 4 10 8 11 4 cm Weight 6 1 lb 2 8 kg Communication modes 5 wire RS 485 DB 9 connectors PMS serial communications protocol 10 100BaseT Ethernet PMS Ethernet Protocol Modbus TCP Calibration fluid DI water Calibration Materials used are traceable to USA NIST and or Japanese Institute of Standards JIS Table 1 3 Common specifications of the LiQuilaz II E and S series Utility Re...

Page 15: ...Page 1 4 LiQuilaz II E and S Operations Manual Chapter 1 Getting Started This page is intentionally left blank ...

Page 16: ...instrument for calibration or repair This is important because an inadequate shipping container could void your warranty If anything is missing contact Particle Measuring Systems Customer Response Center at 1 877 475 3317 or support pmeasuring com If all of the materials are included and undamaged store the packing materials It is important to keep these materials because warranties may not apply ...

Page 17: ...hipkit Accessories The following accessories are included with the instrument 1 Ethernet cable P N 1000011477 Figure 2 1 Ethernet cable 2 USB to RS 232 adaptor P N 1000023262 Figure 2 2 USB to RS 232 adaptor 3 RS 232 to RJ 12 cable P N PMS CD1995 Figure 2 3 RS 232 DB 9 to RJ 12 cable ...

Page 18: ...le power cord US 5 Capillary Cleaning Floss S models only P N 1000009363 Figure 2 5 Pre cut floss 6 Capillary Cleaning Kit one of the following included as appropriate for the model ordered a Capillary Cleaning Kit for sensors with no adaptor or 3 mm on line adaptor S and E P N CK400 Figure 2 6 Capillary Cleaning Kit for sensors with no adaptor ...

Page 19: ...aning Kit for sensors with adaptor 7 LiQuilaz II Operations Manual this document P N 1000023550 Optional Accessories The following accessories are optional purchases 1 USB to opto isolated RS 485 LiQuilaz adaptor P N 1000021389 Figure 2 8 USB to RS 485 converter with 10 ft cable 2 Cable Network OUT to Network IN 10 ft P N PMS CD1050 00 Figure 2 9 Cable Network OUT to Network IN 10 ft ...

Page 20: ... E and S Operations Manual Page 2 5 3 Liquid Installation Kit P N 90351040 which includes a 1 25 feet of 1 4 inch PFA tubing b 1 Flaretek flaring tool c 5 PVDF 1 4 inch flare nuts d 1 Male flare connector a b d c Figure 2 10 Liquid Installation Kit ...

Page 21: ...ine will typically utilize 1 4 inch 6 mm Flaretek fittings Figure 2 11 LiQuilaz II Liquid Particle Counter Online version Indicator Lights An Activity LED and a Status LED are located on the front panel next to the liquid connections The ActivityLED is illuminated upon detection of each particle and failure of the laser This indicator is used to easily verify proper operation of theunit The Status...

Page 22: ...with custom solutions TwoDB 9 femaleandmale connectorswhich support RS 485 and hardware sampling arealsoavailable Thesecondconnectorisavailablefordaisychainingtoothersensors on thenetwork An RJ 12 connector is available for RS 232 setup and communications This connector attaches to the PMS CD1995 adaptor which can be connected to a standard 9 pin PC serial port A standard IEC AC power entry module...

Page 23: ... connections 3 mm zero dead volume fitting or 1 4 inch Flaretek AC Fuse To replace a fuse 1 Unplug the power cord from rear panel of the LiQuilaz II Liquid Particle Counter 2 Use a small blade screwdriver or similar tool toremove the cover fuse drawer from the power entry module located on the instrument rear panel 3 Choose the following 250 V 5x20 mm T 0 75 A 4 Reinstall the cover fuse drawer ass...

Page 24: ...ations cable Ethernet OR Ethernet Crossover cable included To connect the LiQuilaz II Online version 1 Place the particle counter unit where it will have sturdy support and be free of drips and spray 2 Position the PC at the location from which the LiQuilaz II Online will be controlled and monitored 3 Connect a standard IEC AC power cord to the rear panel power module 4 Connect a communications ca...

Page 25: ... device capable of controlling the sample flow rate to the specified sensor flow rate NOTE Installation set up and procedures must follow the appropriate chemical safety regulations for your facility NOTE The flow control device must be made of material compatible with the specific fluid or chemical being sampled 11 Ensure the liquid particle counter power switch is in the OFF position 12 Connect ...

Page 26: ...time If more than one sensor must be connected via RS 485 via daisy chain use FacilityNet software instead Modbus TCP Connect using Ethernet Communication settings and options must be set via RS 232 setup commands in Appendix E Configuring for Ethernet Modbus protocol is an industry standard protocol that is provided for customers who need to interface to a custom computer program or SCADA system ...

Page 27: ...Page 2 12 LiQuilaz II E and S Operations Manual Chapter 2 Unpacking and Connection This page is intentionally left blank ...

Page 28: ...ses Replacing the tubing Capillary Cleaning This section is a basic guide to capillary cleaning for LiQuilaz II sensor capillaries Occasional cleaning is required of the liquid capillary and it is the customer s responsibility to perform the cleaning when necessary The need for capillary cleaning and the general health of the capillary can be improved by continuously running water through the syst...

Page 29: ...s can be easily remedied using high quality laboratory glassware cleaner such Micro 90 or Radiacwash A 5 solution of glassware cleaner in ultra pure DI water should be used CAUTION Do NOT remove the 4 40 socket head screws from the fittings Doing so will compromise the capillary seal and result in fluid leaking onto circuit boards and extensive damage Only remove 3mm zero dead volume fittings from...

Page 30: ... and outlet fittings OUT IN Figure 3 1 LiQuilaz II fittings 4 Fill each syringe from the capillary cleaning kit with 5 ml of cleaning solution mixed to the recommended strength Figure 3 2 Capillary Cleaning Kit syringes 5 Connect the filled syringes to the particle counter s sample inlet and outlet connections 6 Press one syringe plunger all the way into the syringe cylinder 7 Force the cleaning s...

Page 31: ...tubing and run the particle counter while checking the DC Light level 12 If the DC Light remains out of the instrument s designated specification repeat the cleaning process 13 If after further cleaning the DC Light remains outside the instrument s designated specification please contact your local Particle Measuring Systems Service Center DC Light Specifications LiQuilaz II S liquid particle coun...

Page 32: ...es the source of contamination is aggressively attached to the surface of the capillary When these rare events occur using cleaning syringes will not be sufficiently effectivetoreturntheDCLightvaluetoacceptablelimits Underthesesituations using a product called Super Floss manufactured by Oral B can sometimes dislodge the contamination CAUTION Do NOT use floss on the LiQuilaz II E20P particle count...

Page 33: ...enance 2 Carefully remove the top locking pin using a pair of needle nose pliers Figure 3 5 Locking pin removal 3 Use the 3 prong wrench P N 1000014376 supplied in the ship kit to unscrew the fitting from the top capillary mount Figure 3 6 3 prong wrench placement ...

Page 34: ...onto the gaps between the metal sections of the LiQuilaz II housing Immediately wipe up any spills Figure 3 7 Tubing removed from capillary mount 5 Remove the bottom locking pin and use the 3 prong wrench to remove the fitting from the bottom capillary mount Figure 3 8 Locking pin removal from bottom capillary mount 6 Remove a single strand of Super Floss from its package ...

Page 35: ... sampled last bacteria or particles are the most likely sources of contamination If solvents were sampled last optical hazing due to chemical impurities is most likely Both of these situations can be easily remedied using high quality laboratory glassware cleaner such Micro 90 or Radiacwash A 5 solution of glassware cleaner in ultra pure DI water should be used 9 Gently pull the wetted portion of ...

Page 36: ... locking pins into each fitting 14 Connect the liquid particle counter inlet to a source of ultra pure deionized water 15 Direct the liquid particle counter outlet to a drain suitable for cleaning fluid 16 Flush cleaning fluid from the liquid particle counter with DI water for 3 5 minutes a Check all fittings for leaks Correct as required prior to testing unit on chemicals 17 Check the DC Light us...

Page 37: ...l screw driver Fuses 250 V 5 x 20 mm T 0 75 A To replace the fuses 1 Use the LiQuilaz II Liquid Particle Counter power switch located where the power cable connects to turn off power 2 Disconnect the power cable from the particle counter s power entry module NOTE The black plastic assembly that the power cable connects to is called the power entry module The power entry module also contains the fu...

Page 38: ...er version of a LiQuilaz II instrument is connected to the PC through its sampler An Online version of a LiQuilaz II is connected to the PC directly with a communications cable After configuration the user interface software controls all operating functions including the following Sampling parameters sample volume and sample interval the interval between samples Data collection Data display Alarms...

Page 39: ...or set led 1 Flashing green No Ethernet connection to host computer Green Laser OK AND connected to host via Ethernet Red Laser error OR Ethernet protocol error The status LED can be configured via a serial setup command see set led n on page G 2 When communicating via RS 485 use set led 0 Otherwise the LED will flash green since there is no Ethernet host attached Activity LED An activity LED loca...

Page 40: ...ukt der Klasse 1 welches den Normen US 21 CFR 1040 10 und EN 60825 1 entspricht Das Justieren der Lasereinheit das Verändern des Gerätes oder Einsatzbereiche die nicht den Vorgaben dieser Anleitung für das Gerät entsprechen können dazu führen dass gefährliches Laserlicht austritt ATTENZIONE Lo strumento è classificato come prodotto laser di Classe 1 e rispetta l US 21 CFR 1040 10 e l EN 60825 1 L ...

Page 41: ...Symboles de risque Des symboles représentant les risques sont placés sur l appareil Leur signification est la suivante Symbole Nature du risque Attention consulter les documents d accompagnement Danger Electricite Avertissement Rayonnement laser Éviter toute exposition au faisceau Warnschilder Die an dem Gerat angebrachten Warnschilder haben folgende Bedeutungen Symbol Gefahrenart Achtung In den b...

Page 42: ...nte Simbolo Natura del pericolo Attenzione Consultare i documenti allegati Tensione Pericolosa Avvertenza Radiazione laser Evitare l esposizione ai raggi Simbolos de peligro Los simbolos de peligro que aparecen en el equipo significan Símbolo Naturaleza del Peligro Atención consultar los documentos adjuntos Peligro alto voltaje Advertencia Radiación láser Evite exponerse al rayo ...

Page 43: ...Page A 4 LiQuilaz II E and S Operations Manual Appendix A International Precautions This page is intentionally left blank ...

Page 44: ...m specific operations The operations may be one time command sequences i e instrument initialization or command sequences that are performed repeatedly i e polling for data A detailed explanation of each command is contained in the protocol section Instrument Initialization The following command sequence is typical during initialization or re initialization of the instrument CSR CDT CMODE This seq...

Page 45: ... its data queue This is done by transmitting the CQC command The instrument responds with a RQC and two values If the first value is 1 the instrument is not sampling and needs to be re initialized and started as outlined in the Instrument Initialization on page B 1 and Sample Initialization on page B 2 sections If the instrument responds with a value of 0 there is no data at this time send another...

Page 46: ...dure has a command response sequence For each command directed to a LiQuilaz II Liquid Particle Counter a response is generated by the unit The format of the response depends on the particular command See Slow Protocol Commands on page B 5 for a complete listing of the LiQuilaz II Liquid Particle Counter commands These commands and responses are formatted and packeted to ensure error free communic...

Page 47: ...Value of Byte Character s transmitted i e byte 1H byte 2H byte 20H 7BH byte 20H 7B byte 80H 7CH byte 5BH 80H byte COH 7DH byte 60H COH byte 7EH byte AOH otherwise byte A typical command and response packet at this point in the formatting and packeting process will have the following appearance Command CQC Response RQC This particular LiQuilaz II has an address of 1 Command transmitted to LiQuilaz ...

Page 48: ...Q Delete all untransmitted reports CQC RQC n s Return the number of reports on the transmission queue and the sampling status CSR RSR Software reset CSS RSS Start time based sampling mode CTS RTS Terminate current sample and stop sampling CVER RVER Request LiQuilaz II software version CSATH RSATH n Set absolute PHA thresholds CRATH RRATH Read absolute PHA thresholds CSPHA RSPHA n Set the PHA param...

Page 49: ...ing 1 n 28800 CDT yyyy mm dd hh mm ss Sets date and time for the LiQuilaz II If the instrument is sampling when this command is issued the sample will be aborted and the LiQuilaz II will stop sampling CTD Transmit the report currently on the top of the transmission queue The detailed format of the report is shown below Note that this is the unformatted data report STX Begin report flag The STX cha...

Page 50: ...ment is currently sampling it will abort the sample and start a new sample CTS Terminate sampling causes the LiQuilaz II to stop continuous time mode sampling and return to the idle state This command has no effect during Sampler mode CVER The LiQuilaz II will return the original version string of the software currently running since it is used by the DOS calibration program and then appends the c...

Page 51: ... locations greater than n nc The maximum values for nc and n are 31 and 8191 respectively for the LiQuilaz II Liquid Particle Counter CSPHA Stores the current state of the PHA The values are stored in battery backup RAM The last values used will be the default values on power up The response to the command is RSPHA n where n 1 is a valid state of the PHA and n 0 is an invalid state The detailed fo...

Page 52: ...channel sizes were set with the CSIZE command CSTAB nc a1 b1 a2 b2 a nc b nc Set table values The first number nc is the number of table entries There are then nc actual table entry pairs Each pair of values represents size 1000 and a corresponding threshold value Returns 1 if entries are acceptable or 0 if sampling or the entries are incorrect CRTAB Read table values The response is RRTAB nc a1 b...

Page 53: ...te Bad bit n 4 Not Used bit n 5 Not Used bit n 6 Not Used bit n 7 Not Used bit n 8 Not Used NOTE The bit n 3 is only valid in the time based mode The bit n 3 is the sample signal line for the sample based mode 4 SAMPLE_STATUS Time base mode only A 1 byte number The most significant bit represents the sampling status The low 7 bits represents the Queue Count The Queue Count in the Slow and Fast pro...

Page 54: ...ate a Fast protocol transmission by sending a single 8 bit address character on the network The lower 7 bits of this character will have a value between 0 and 99 that corresponds to the node s main network address The upper most significant bit of the address character will be a 1 indicating that a Fast protocol response is being requested After recognizing its address the node responds with the f...

Page 55: ... be assumed by the host computer Example NOTE All numbers are in hexadecimal Address transmitted by Data Display System 81 Response from LiQuilaz II E20 0281000000000100FF7F000F000000000000000000000000000000000000000000000000000000000000900103 This LiQuilaz II E20 responded with the following information STX 02 ADDRESS 81 SAMPLE_INTERVAL 00000000 LASER FLOW STATUS 01 SAMPLE_STATUS 00 DC_LIGHT FF7F...

Page 56: ...n the Modbus map is defined to be 16 bits The map can contain three distinct sections 1 Input registers Read Only information for ID and data collection 2 Holding registers Read Write parameters for configuring the device 3 Coils Read Write individual bits to control the device The supported functions include 1 Read Coils 3 Read Holding Registers 4 Read Input Registers 5 Write Single Coil 6 Write ...

Page 57: ... This setting can be made in the setup interface and saved in non volatile storage or set real time via the associated coil Even though the Modbus protocol itself is standard the contents of the registers are application specific A description of the register map is the definitive specification for that application interface The following Modbus register map has comments and notes to help with its...

Page 58: ...ng ASCII bytes and positioned as shown in the map The power of 10 multiplied to the flow rate and then entered into registers 30013 30014 and 30222 30223 Used when the floating point representation is disabled The LiQuilaz II uses a value of 3 to represent a fixed scaling factor of 1000 for flow rate The power of 10 multiplied to the volume and then entered into registers 30224 30225 Used when the...

Page 59: ...ale Volume Multiplier in fixed Volume 2 100 30013 dual Flow Rate high Flow 10Scale Float Mode 30014 dual Flow Rate low Flow 10Scale Float Mode 30015 unary Number of Particle Channels Fixed number of sizes 16 fixed 30016 unary Number of Analog Channels Fixed number of analogs 1 fixed 30017 dual Channel 1 Size high nanometers 30018 dual Channel 1 Size low nanometers Variable 30019 dual Channel 2 Siz...

Page 60: ...nometers Variable 30039 dual Channel 12 Size high nanometers 30040 dual Channel 12 Size low nanometers Variable 30041 dual Channel 13 Size high nanometers 30042 dual Channel 13 Size low nanometers Variable 30043 dual Channel 14 Size high nanometers 30044 dual Channel 14 Size low nanometers Variable 30045 dual Channel 15 Size high nanometers 30046 dual Channel 15 Size low nanometers Variable 30047 ...

Page 61: ...he data A separate coil read would not be required Values are defined in Table C 5 on page C 17 30214 Device State Least Significant byte LSB is State Most Significant Byte MSB is sub state Values are defined in Table C 5 30215 Number of Data Samples in the Queue A value of zero is identical to no data available coil 00 02 read as zero The queue size setting will determine if the data register sec...

Page 62: ...ger or float depending on mode selected The integer representation uses scale factor from register 30012 30226 Location Index of location value associated with data packet Not used for LiQuilaz II 30227 Number of Particle Channels Processed as a variable since the LiQuilaz II can queue data packets which were collected using a varying number of selected channels If a varying number of size channel...

Page 63: ... unary Device Status low Device Status Mask 30214 unary Device State Device State 30215 unary Number of data samples in queue Number of samples in queue 30216 dual Time Stamp high time_t 30217 dual Time Stamp low time_t 30218 dual Sample Time high Seconds 100 Float Mode 30219 dual Sample Time low Seconds 100 Float Mode 30220 dual Data Packet Status high Bit Mask 30221 dual Data Packet Status low B...

Page 64: ...9 low Cumulative Raw Ch9 30247 dual Particle Channel 10 high Cumulative Raw Ch10 30248 dual Particle Channel 10 low Cumulative Raw Ch10 30249 dual Particle Channel 11 high Cumulative Raw Ch11 30250 dual Particle Channel 11 low Cumulative Raw Ch11 30251 dual Particle Channel 12 high Cumulative Raw Ch12 30252 dual Particle Channel 12 low Cumulative Raw Ch12 30253 dual Particle Channel 13 high Cumula...

Page 65: ...me This register is only used in the Sample Interval mode for LiQuilaz II This register represents the number of seconds to run each sample The allowed sample interval is 1 to 28800 seconds 8 hours 40004 Hold Tare Time Time in seconds processed between the start command and starting the first sample The allowed tare time is 0 to 28800 seconds 8 hours 40005 Repeat Count Number of samples to process...

Page 66: ...ometers 40036 dual Channel 02 Size high nanometers 40037 dual Channel 02 Size low nanometers 40038 dual Channel 03 Size high nanometers 40039 dual Channel 03 Size low nanometers 40040 dual Channel 04 Size high nanometers 40041 dual Channel 04 Size low nanometers 40042 dual Channel 05 Size high nanometers 40043 dual Channel 05 Size low nanometers 40044 dual Channel 06 Size high nanometers 40045 dua...

Page 67: ...low nanometers 40058 dual Channel 13 Size high nanometers 40059 dual Channel 13 Size low nanometers 40060 dual Channel 14 Size high nanometers 40061 dual Channel 14 Size low nanometers 40062 dual Channel 15 Size high nanometers 40063 dual Channel 15 Size low nanometers 40064 dual Channel 16 Size high nanometers 40065 dual Channel 16 Size low nanometers Table C 3 Holding Registers Continued Holding...

Page 68: ...ill be deleted 00 03 The data clear coil will delete all data in the queue Read Always 0 Write 1 Delete all queued data 0 No effect 00 04 The reset sensor coil will reset the sensor Read Always 0 Write 1 Reset sensor 0 No effect 00 05 Green Status LED Read 1 LED On 0 LED Off Write 1 LED On 0 LED Off 00 06 Red Status LED Read 1 LED On 0 LED Off Write 1 LED On 0 LED Off 00 07 External Alarm Not appl...

Page 69: ...e Queue Control 00 03 Data Clear Toggle Data Queue Delete 00 04 Reset Sensor Toggle Reset control 00 05 Status LED Green On Off Status LED Green Control 00 06 Status LED Red On Off Status LED Red Control 00 07 External Alarm On Off External alarm n a 00 08 IEEE 754 Float On Off Modbus Float representation 00 09 Volume Mode On Off Sample Volume or Interval n a Spare 22 spare coils Reserve common co...

Page 70: ...s set to one then the data shown is always the last data processed and is representative of real time data only Since the queue is circular the next sample will replace the single one in the queue If the queue is set to a value greater than one then the data shown is the oldest in the queue Any data collected once the queue is full will cause the oldest data to be discarded Queued data will always...

Page 71: ... numbers Example 32 Bit Unsigned Reg 16 Bit Low Unsigned 65536 16 Bit High Unsigned Use arithmetic OR and left shift operation Example 32 Bit Unsigned Reg 16 Bit High Unsigned 16 bit left shift arithmetic OR 16 Bit Low Unsigned Never combine the values as signed integers or floating point value If the final value is signed convert the 32 Bit Unsigned value to a 32 Bit signed value after combining ...

Page 72: ...0001 Data Collection Matches the common coil settings 0x0002 Data Available 0x0004 Data Clear 0x0008 Reset 0x0010 Green Status 0x0020 Red Status 0x0040 External Alarm 0x0080 IEEE Float mode 0x0100 Volume Mode n a Device State Entries LSB 0 Idle 1 Sampling Device SubState Entries MSB 0 Idle Normal 0 Sampling Normal 1 Sampling Hold Tare Data Packet Status Entries Low Register 0x0001 Laser Good 0x000...

Page 73: ...to be a starting point It does not detail error handling and does not provide other functionalities which may be desired The Optional Processing shown at the start of the flowchart sets the instrument channels These may be set by the serial setup interface The channel settings are non volatile so they only need to be set once when the instrument is first installed and configured Figure C 1 Modbus ...

Page 74: ...e for assigning fixed addresses Ethernet Addressing Basics Particle Measuring Systems instruments must be properly configured for Ethernet communications in order to work There are multiple numeric parameters required to properly configure an instrument and a small error in one or more of these parameters can result in no communications or worse sporadic communications All instruments support the ...

Page 75: ... 255 255 C 16 Bit Range 192 168 0 0 192 168 255 255 Particle Measuring Systems provides a unique default address in the Class A range for every instrument Whenever the instrument is set to default parameters or factory defaults this address is restored Network Mask The network mask is used to discern the network portion of the IP address from the location portion From a telephone number analogy it...

Page 76: ... addresses in the 224 0 X X range should not be used as many of them are reserved for other communications Particle Measuring Systems assigns a factory default multicast address of 224 100 100 1toallinstruments Thisaddressgenerallydoesnotneedtobechanged The exception is when sensors are integrated into a large network In this situation IT may recommend an alternative multicast address to avoid net...

Page 77: ...IP address i e DHCP or Dynamic Host Configuration Protocol In order for dynamically configured devices and statically configured devices to be mixed on the same network some mechanism must be used to segregate the DHCP address range from the static address range This mechanism is a standard configuration parameter set in the router The IT Department is typically responsible for delineating the add...

Page 78: ...e Does a known good device work when connected instead 2 Verify the device can talk using PING a Open a command shell on a PC and type PING aaa bbb ccc ddd where aaa bbb ccc ddd is the address of the device If there is no response then there is an addressing problem Figure D 2 Example for PING test b Make sure the PC and the device being talked to are on the same network c Check the PC s address b...

Page 79: ...ig command d Does an LED on the device s Ethernet connector blink when a PING is transmitted to it If not there may be an addressing error with the device or a configuration problem with the router or switch the device is attached to d 1 Try re powering the device to re establish communications with the router or switch ...

Page 80: ... Method 1 Modifying the IP Settings on a PC This method allows using the existing instrument address At the end of the communications session the laptop will contain an address that will prevent normal communications to the corporate network The procedure must be undone after the session 1 Retrieve the network address parameters from the instrument This can be done using a HyperTerminal serial lin...

Page 81: ...ies A window similar to that shown in Figure D 4 on page D 8 should be displayed Figure D 4 Local Area Connection Properties window b Select the item Internet Protocol TCP IP If given an option for Version 4 or Version 6 select the one titled Internet Protocol Version 4 c Click the Properties button in the Local Area Connection Properties window The Internet Protocol TCP IP Properties window appea...

Page 82: ...he Internet Protocol TCP IP Properties window to use the network address and mask determined above See Figure D 5 on page 9 for an example The Default gateway and DNS server values should be left blank f Click the OK button to close the Internet Protocol TCP IP Properties window g Click the OK button to close the Local Area Connection Properties window 4 The PC is now configured 5 Attach a network...

Page 83: ...instrument it will talk one to one with a Windows machine without setting an address on the Windows machine The address range of 169 254 0 1 through 169 254 255 254 is reserved for APIPA 1 Attach the instrument to a HyperTerminal link 2 Set the instrument addresses as follows IP address 169 254 0 1 Mask 255 255 0 0 Gateway 0 0 0 0 or blank 3 After setting the addresses use the write command to sav...

Page 84: ... working knowledge of terminal emulation software such as HyperTerminal When to Configure the Sensor The sensor should have the appropriate Ethernet settings configured before it is wired to a network This can be performed either before fluidic installation if access to the back of the sensor is problematic or in situ if back panel access is not an issue Required Hardware and Software RS 232 cable...

Page 85: ...or Ethernet RS 232 Cable A suitable cable PMS CD1995 is provided in your shipment The wiring for this cable is as follows Table E 1 RS 232 Pin Outs RJ 12 jack Pin 1 DSR Pin 2 Transmit Pin 3 Receive Pin 4 RTS Pin 5 CTS Pin 6 GND NOTE Pins 1 4 and Pin 5 are shorted together ...

Page 86: ...ect the LiQuilaz II Liquid Particle Counter to a computer that has terminal emulation software 2 StarttheterminalemulationsoftwareandselecttheappropriateSerialPortonyour PC Windows Device Manager may be used to find the required setting 3 Set the following communication parameters Table E 2 Terminal Emulator Communications Parameters Baud Rate 9600 Data Bits 8 Parity N Stop Bits 1 Flow Control Off...

Page 87: ...a value of 0 255 separated by a period character An example of a valid IP address is 010 255 000 060 Set mas k aaa bbb ccc ddd Sets the network mask address using a decimal notation form of aaa bbb ccc ddd Each three digit series is a value of 0 255 separated by a period character The mask separates the network address from the host address This address is common to all devices on the logical netw...

Page 88: ...when reconnected The LiQuilaz II Liquid Particle Counter will Continue sampling if it was initially started and then disconnected Queue up to the number of samples defined by the queue size Once full older data will be overwritten by newer data Unload the queued data in chronological order when reconnected Periodically delete elements of the queue for which Facility Net has received the data Set m...

Page 89: ...lay screen the terminal emulator may be set up incorrectly or the cable may be improperly connected or faulty Connecting the Ethernet Cable The LiQuilaz II Liquid Particle Counter communicates with Facility Net or third party Modbus applicationbymeansofaCAT 5 UTPEthernetcable Thesensorisdesignedto work best with a CAT 5 UTP cable Other types of Ethernet cable may produce excess noise An Informatio...

Page 90: ...be set up and troubleshooting for serial communications Adapters and Cables on page F 2 USB Serial Port Adapter on page F 2 Serial Cable on page F 3 RJ 12 Cable and Adapter on page F 3 Connector Signals on page F 4 Communication Software Options on page F 5 HyperTerminal on page F 5 PuTTY on page F 6 Tera Term on page F 7 Communications Configuration on page F 8 ENODE Specific Settings on page F 8...

Page 91: ...e USB Serial Port Adapter Newer computers especially laptops no longer include a serial port USB to Serial adapters are available to resolve this issue Particle Measuring Systems has P N 1000023262 see Figure F 1 Figure F 1 USB serial adaptor USB driver for Windows Windows machines will require a driver to be installed for the USB serial adaptor The drivers are specific to the model of adaptor use...

Page 92: ...r cables In addition some cables have DB 25 or other less useful connectors The recommended straight cable will not require male male or male female or null modem adapters for most Particle Measuring Systems instruments RJ 12 Cable and Adapter Some Particle Measuring Systems instruments usually those with smaller form factors use an RJ 12 modular adaptor for serial communication The adaptor and ca...

Page 93: ...Out RTS Request to Send 8 In CTS Clear to Send 9 In RI Ring Indicator Table F 2 shows the RJ 12 connector pinout for many Particle Measuring Systems instruments Pins shown as instrument dependent are not usually available On some instruments the pins may be tied together to simulate hardware flow control On other instruments the pins are not used at all See instrument specific documentation to ver...

Page 94: ...s program The following alternative utilities available as downloads are discussed HyperTerminal this page PuTTY on page F 6 Tera Term on page F 7 HyperTerminal Due to its use in Windows XP as well as older versions HyperTerminal remains the most ubiquitous program available for serial communications It is available for Windows 7 users as a purchased download from Hilgraeve http www hilgraeve com ...

Page 95: ...g or here http www chiark greenend org uk sgtatham putty download html PuTTY software interface screen shots are shown in Figure F 5 and Figure F 6 The default color scheme uses a black terminal window This can be changed to a white terminal window by going to the Colours setup and then clicking the box titled Use system colours Figure F 5 PuTTY Configuration window Figure F 6 PuTTY Main window ...

Page 96: ...larger download than PuTTY described above It is available at http en sourceforge jp projects ttssh2 releases Tera Term also uses a black main window It can be reversed under the Setup Window option Tera Term software interface screen shots are shown in Figure F 7 and Figure F 8 Figure F 7 Tera Term Setup window Figure F 8 Tera Term Main window colors reversed ...

Page 97: ...isted in Table F 3 Table F 3 Communication parameters Baud 9600 This can be changed on the LiQuilaz II Liquid Particle Counter front panel Parity None Data Bits 8 Stop Bits 1 Flow Control Xon Xoff none is also OK ENODE Specific Settings The ENODE requires additional settings for communications These are not covered in this appendix In addition not all the settings are supported by PuTTY or Tera Te...

Page 98: ...correct COM port Are the communication settings correct Is the software set for 9600 N 8 1 If the problem is with a LiQuilaz II check the instrument s communications setup screen Is hardware flow control enabled If so disable it Dropped Characters or Strange Characters Is the baud rate correct Verify that hardware flow control is not enabled Is there a problem with the serial port on the PC Bad US...

Page 99: ...Page F 10 LiQuilaz II E and S Operations Manual Appendix F Serial Communications Overview This page is intentionally left blank ...

Page 100: ...et gateway ddd ddd ddd ddd TCP sets the gateway address set ip ddd ddd ddd ddd TCP sets the IP address in decimal set led n Sets LED mode 1 connection 0 status set mask ddd ddd ddd ddd TCP sets the network mask set mode n Ethernet Mode 0 PMS 1 Modbus set multicast ddd ddd ddd ddd TCP sets the multicast address set ntp ddd ddd ddd ddd TCP sets NTP Server address set queue n Set data queue between 1...

Page 101: ...imits 0 255 Set Ethernet gateway address The values ddd represent decimal entries for each address octet Do not use leading zeros This setting will be saved after the write command is issued set ip aaa bbb ccc ddd Range Limits 0 255 Set Ethernet IP Internet Protocol address The values aaa bbb ccc ddd represent decimal entries for each address octet Do not use leading zeros This setting will be sav...

Page 102: ...00 The units are in seconds The unit will stop sampling if this parameter is changed during a run state This setting will be saved after the write command is issued set serdump n Set the unit to dump serial data If n is 1 then serial dump is enabled otherwise it is disabled This setting will be saved after the write command is issued Unlike the associated data command this feature allows a method ...

Page 103: ... 255 002 172 Multicast Address 224 100 100 001 Net Mask 255 000 000 000 Gateway 010 255 000 060 NTP Address 000 000 000 000 After Write IP Parameters IP Address 010 255 002 172 Multicast Address 224 100 100 001 Net Mask 255 000 000 000 Gateway 010 255 000 060 NTP Address 000 000 000 000 Sample Interval 5 Connected to Not Connected When not connected the led flashes green Data Queue set at 480 Ethe...

Page 104: ...ame 捷ↅ 䱿 㦘㹡㒥㦘 䤓䓸德 侯 杔 Pb 㻭 Hg 柘 Cd ↆ杻 Cr VI 䅃勣啾 PBB 䅃勣啾搩 PBDE 䟄䄟 ㄣ X O X O O O Ⓠ䟄恾孔揜 X O X O O O ⷵ ↅ X O X O O O 䉏 X O X O O O 㧉㬿捷ↅ X O X O O O 䟄冕 X O X O O O 㧉䟄 X O X O O O O 嫷䯉䞷ℝ捷ↅ䤓㓏㦘 㡞䓸德 㓏 䤓㦘㹡㒥㦘 䓸德 ℝSJ T11363 2006屓 䤓棟 ㄵ尐㻑ᇭ X 嫷䯉䞷ℝ捷ↅ䤓咂 䱜 㡞䓸德 㓏 䤓㦘㹡㒥㦘 䓸德浧ℝSJ T11363 2006屓 䤓棟ㄵ尐㻑ᇭ ...

Page 105: ...Page H 2 LiQuilaz II E and S Operations Manual Appendix H 㦘㹡㒥㦘 䤓䓸德 侯 This page is intentionally left blank ...

Page 106: ...al F 9 unexpected characters F 9 components 2 6 Configuration Commands E 4 Configuration Defined E 1 Configuring the Airnet for Ethernet E 1 configuring the Airnet when E 1 connecting to standard PC serial port F 4 Connecting the Ethernet Data Cable E 6 connections 2 6 liquid connections 2 6 connections liquid 1 2 connector signals F 4 control flow setting F 8 CPQ command B 2 CPQ Slow protocol com...

Page 107: ...ow rate and cavitation 1 2 formatting data B 11 fuses 1 3 2 8 3 10 G gateway address D 3 H HyperTerminal F 5 communications software F 5 HyperTerminal window F 5 I indicator lights 2 6 initialization instrument B 1 sample B 2 installation 2 8 2 9 installation requirements 2 9 instrument initialization B 1 international precautions A 1 Internet Protocol TCP IP Properties window D 9 IP address Ether...

Page 108: ...iguration Addresses E 3 slow polling B 2 Slow protocol B 2 B 3 commands B 5 B 6 details B 6 summary B 5 first logical step B 3 second logical step B 4 third logical step B 4 software Facility Net D 1 D 2 D 3 Pharmaceutical Net 2 9 SamplerSight 2 9 specifications 1 2 status E 4 stop bits F 8 T TCP IP protocol D 8 Tera Term communications software F 5 terminal emulator F 7 Tera Term Main window F 7 ...

Page 109: ...Index 4 LiQuilaz II E and S Operations Manual PuTTY Configuration F 6 PuTTY Main F 6 Tera Term Main F 7 Tera Term Setup F 7 X Xon Xoff F 8 ...

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