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Vapodest 45s
8 Execution of method
This chapter describes the execution of a distillation. However, we can only give
you a general overview how to work with Vapodest in this manual. Should you need
any specific methods we will send you the respective application on request. These
data sheets contain detailed info about the sample preparation and programming.
Make sure to always wear protective clothes (gloves, protective glasses, lab coat)
when working with Vapodest.
When you take out the digestion tube, make sure to wear protective glove or have
glass tongs at hand and wear protective glasses. The glass container is very hot
and there is the danger of burns!
Be careful when handling acids and alkalis! Please observe the safety regulations
according to the current laws regarding handling of dangerous goods!
8.1. Prior to the analysis
Check set of tanks
Check the level of reservoirs and the connections at regular intervals.
Turn on faucet
The system is only working when the faucet is turned on.
Test run
In order to make sure to obtain reproducible results, we kindly ask you to run a
distillation without sample every day prior to the first analysis. In order to do so,
insert the digestion tube and start
Program M00 Test run
.
8.2. Distilling a sample without external titrator
Whenever using an external titrator, make sure to read chapter "8.3. Start
analysis with external titrator".
1.
Place an Erlenmeyer flask into position
2.
Press down quick clamping device and insert the digestion tube.
3.
Check correct fit of the tube.
4.
Close protection door and turn on equipment.
Warnung vor
einer Gefahrenstelle
Warnung vor
einer Gefahrenstelle
Warnung vor
einer Gefahrenstelle
Vapodest 45s
Standby
turn
5.
The display shows the standby mode
