Dionex MSQ, User Manual

Page: 131 / 132

Index__________________________________________________________________________________
system overwiew, 1-2 sample infusion system
MSQ Instrument Tuning and Calibration Wizard flow rate (Note), 4-2
figure, 1-30 introduction, 4-i
probe temperature (Note), 4-4, 4-6
setup, 4-3
T
schedule, maintenance, 5-2
self cleaning source, 1-3, 1-23
tetrahydrofuran, THF
Sequence Setup, 1-29
use, 3-5
server, 1-29
use (Caution), 3-5
setup
thermal fragmentation
cone wash, 3-7
figure, 1-20
sample infusion system, 4-3
TIC chromatogram, 1-30
sheath gas, 1-11, 1-14
total ion current chromatogram. See TIC
chromatogram
shutting down the system
full shutdown, 7-5
triethylamine, TEA, 3-5
in between analytical runs, 7-2
trifluoroacetic acid, TFA, 1-1, 3-5
one month or more, 7-4
tubing
up to one month, 7-3
PEEK, 6-6
SIM, 1-35
PEEK color coding (table), 6-6
singly charged ions, 1-12, 1-15
Teflon, 6-5
sodium adduct
tune diagnostics
mass spectrum (figure), 1-12
dialog box (figure), 6-4
software, Xcalibur, 1-28
running, 6-4
solvents, 3-3
running (Note), 6-4
source
tune diagnostics completed (figure), 6-4
APCI (figure), 1-14
ESI (figure), 1-11
U
introduction, 1-8
schematic (figure), 1-9
self-cleaning, 1-3
UV detectors, 6-7
source block
cleaning, 5-16
V
cleaning (Caution), 5-16
replacing, 5-19
vacuum
source block assembly
pumping down, 7-8
cleaning (Warning), 5-11
starting vacuum pumps (Note), 7-7
cleaning procedure, 5-13
MSQ under vacuum (Note), 7-3
removing, 5-13
vacuum system
source fragmentation, 1-16
introduction, 1-27
spares, 8-4
vent, 1-30
spectrum, 1-30
volatile buffer systems, 1-1
square quadrupole RF lens
overview, 1-26
W
status light, 1-5
status light panel
indications (table), 1-6
Warnings
stick spectrum, 1-32
adding rotary pump oil, 5-24
sulfuric acid, 3-5
APCI probe removal, 5-8
surface active agents, 3-4
changing ionization modes, 2-2, 2-4, 5-15
MSQ
changing the rotary pump oil, 5-25
analyzer and detector schematic (figure), 1-26
ESI probe removal, 5-4
APCI source (figure), 1-14
heater removal, 5-21
components (figure), 1-2
lifting rotary pump, 5-25
doors open (figure), 1-6
source block assembly cleaning, 5-11
ESI source (figure), 1-11
using concentrated nitric acid, 5-6, 5-9
exterior features, 1-5
water, 3-3
front view (figure), 1-5
introduction, 1-1
X
power supply requirements, 6-3
rear view (figure), 1-7
Xcalibur
schematic (figure), 1-3
Home Page, 1-28
source schematic (figure), 1-9
IV
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