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Bruker SampleXpress User Manual Download Page 9

9

Z31900_00_01

2

Introduction

The new Bruker sample changer SampleXpress allows automatic measurement of NMR
samples with Bruker NMR spectrometers. It is the successor of the B-ACS sample
changer system. Its compact, exceptionally integrated design, drastically reduces sam-
ple transfer distances, delivering exchange times of just a few seconds, making Sam-
pleXpress ideal for optimizing throughput in standard NMR service laboratories running
30-200 samples per day. In addition, efficiency is maximized thanks to exchangeable,
easy-fill, cassette modules that can be loaded off-system and in parallel with current
experiments.

2.1

Concept

SampleXpress is controlled by TopSpin or ICON-NMR, Bruker’s graphical user interface
for fully-automated acquisition and processing.

The system is also equipped with integrated barcode reader registration, which is under
control of SampleTrack, Bruker‘s information and data management software.

"Design and Function" on page 35

for a complete description of the design and

function of SampleXpress.

Figure 2.1

SampleXpress

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Summary of Contents for SampleXpress

Page 1: ...Version Bruker BioSpin think forward NMR Spectroscopy SampleXpress 001 Sample Changer User Manual ...

Page 2: ... their respective holders This manual was written by Volker Reiss Gilbert Cyppel Stanley J Niles July 15 2010 Bruker Biospin GmbH Rheinstetten Germany P N Z31900 DWG Nr Z4D11037 For further technical assistance on the SampleXpress unit please do not hesitate to contact your nearest BRUKER dealer or contact us directly at BRUKER BioSpin GMBH am Silberstreifen D 76287 Rheinstetten Germany Phone 49 7...

Page 3: ...s 16 3 3 3 Instruction 16 3 4 Personal Protective Equipment 16 3 5 Basic Dangers 17 3 5 1 Position of the Safety Devices 17 3 5 2 Description of the Installed Safety Devices 17 3 5 3 General Workplace Dangers 18 3 5 4 Dangers from Electric Power 19 3 5 5 Mechanical Dangers 21 3 5 6 Dangers from Gases Under Pressure 22 3 5 7 Dangers from Radiation 23 3 5 8 Dangers Due to High or Low Temperatures 24...

Page 4: ...mmissioning 55 8 Operation Overview 57 8 1 Safety 57 8 1 1 Emergency Shutdown 57 8 2 General Operating Guidelines 58 8 2 1 Switching On the Device 59 8 2 2 Switching Off the Device 59 8 2 3 Sample Adjustment and Maximum Sample Height 60 9 Operation 61 9 1 Operation Modes 61 9 2 Main Display 62 9 2 1 Main Menu Touch Screen Buttons in Single Access Mode 65 9 3 Starting the Application Software 66 9 ...

Page 5: ...ent Parts 91 10 3 Preventative Maintenance 91 10 4 Lift Adjustment 92 10 5 Magnet Service 93 10 5 1 Refilling 93 10 5 2 After a Quench 93 10 6 Maintenance Schedule 93 10 7 Software 94 10 7 1 Service File 94 10 7 2 Firmware Upgrade 96 10 7 3 Device Report File 99 10 8 Cleaning 101 10 8 1 Before Cleaning 101 10 8 2 Cleaning the Outside of the SampleXpress Chassis and Units 102 10 8 3 Cleaning the Ou...

Page 6: ...ety 117 13 2 Dismantling 118 13 3 Disposal 118 14 Contact 121 Appendix A 123 A 1 Safety Notices 123 A 2 Avertissements De Sécurité 133 A 3 Sicherheitshinweise 145 Appendix B 157 B 1 Repair Declaration 157 Appendix C 159 C 1 Warning Signs 159 C 2 Figures 161 C 3 Tables 165 C 4 Glossary 167 C 5 Index 169 ...

Page 7: ...pplies must be available and adhered to 1 2 Policy Statement It is the policy of Bruker to improve products as new techniques and components become available Bruker reserves the right to change specifications at any time Every effort has been made to avoid errors in text and figure presentation in this publica tion In order to produce useful and appropriate documentation we welcome your com ments ...

Page 8: ...tion which could result in death or serious injury unless avoided CAUTION This combination of symbol and signal word indicates a possibly hazardous situation which could result in minor or slight injury unless avoided NOTICE This combination of symbol and signal word indicates a possibly hazardous situation which could result in damage to property or the environment unless avoided DANGER This comb...

Page 9: ...ies running 30 200 samples per day In addition efficiency is maximized thanks to exchangeable easy fill cassette modules that can be loaded off system and in parallel with current experiments 2 1 Concept SampleXpress is controlled by TopSpin or ICON NMR Bruker s graphical user interface for fully automated acquisition and processing The system is also equipped with integrated barcode reader regist...

Page 10: ...ditions and Terms of Delivery and the legal regulations applicable at the time of the conclusion of the contract shall apply 2 3 Copyright This manual is protected by copyright and intended solely for internal use This manual must not be made available to third parties duplicated in any manner or form whether in whole or in part and the content must not be used and or communi cated except for inte...

Page 11: ...11 Z31900_00_01 Introduction 2 6 EC Declaration of Conformity ...

Page 12: ...12 Z31900_00_01 Introduction 2 7 EG Konformitätserklärung ...

Page 13: ...een designed and constructed solely for the intended use described here The SampleXpress must only be used for keeping NMR samples in a cassette module inserting them into the NMR spectroscopy magnet and ejecting them after measurement back into the magazine Intended use also includes compliance with all specifications within this manual Any use which exceeds or differs from the intended use shall...

Page 14: ... intervals The owner must provide the personnel with the necessary protective equipment The owner must warrant that the SampleXpress is operated by trained and autho rised personnel as well as all other work such as transportation mounting start up the installation maintenance cleaning service repair and shutdown that is carried out on the device All personnel who work with or in the close proximi...

Page 15: ...rements 3 3 1 Qualifications i Note Only trained Bruker personnel are allowed to mount retrofit repair adjust and dis mantle the unit This manual specifies the personnel qualifications required for the different areas of work listed below Laboratory Personnel Laboratory personnel are health care professionals technicians and assistants staffing a research or health care facility where specimens ar...

Page 16: ...the laboratory Always comply with the instructions governing personal protective equipment posted in the work area WARNING Risk to life for unauthorized personnel due to hazards in the danger and working zone Unauthorized personnel who do not meet the requirements described in this manual will not be familiar with the dangers in the working zone Therefore unauthorized per sons face the risk of ser...

Page 17: ...in the following chapters of this manual 3 5 1 Position of the Safety Devices EMERGENCY STOP Button The position of the EMERGENCY STOP button is indicated in the illustration by an arrow Figure 3 1 Position of the Emergency Stop 3 5 2 Description of the Installed Safety Devices EMERGENCY STOP Button Pressing the EMERGENCY STOP button triggers an emergency stop After the emer gency stop button has ...

Page 18: ...dable hazards using marking tape CAUTION Accident hazard from falling from ladder It is possible to fall from a ladder when it is used to reach the SampleXpress on some magnets f Do not use a ladder f Use an approved platform to reach the device on the magnet f Wear non slip shoes NOTICE Material damage due to a software error Samples or SampleXpress may be damaged due to a software error causing ...

Page 19: ...and maintenance Using genuine samples during installation and maintenance may result in material damage f Use only dummy samples during installation and maintenance DANGER Danger to life from stored charges Electric charges may be stored in electrical components even after the system has been switched off and disconnected from the power supply Contact with these com ponents may result in serious o...

Page 20: ...ply before opening the device Use a voltmeter to verify that the device is not under power f Be sure that the power supply cannot be reconnected without notice f The housing must be closed during operation WARNING Danger to life from residual electrostatic potentials Friction between material being conveyed may result in significant development of electrostatic potential Contact with parts immedia...

Page 21: ...essary assembly disassembly the device in multiple parts f Use a platform with railings instead of a ladder to reach the assembly area f Avoid working over the head When this can not be avoided wear a protective hard hat f Follow the mounting instructions in the installation manual CAUTION Accident hazard from loose clothing or long hair becoming caught in magazine chain Wearing loose clothing or ...

Page 22: ...ried out by trained pneumatics technicians f Before starting work on the pneumatics system ensure that it has been com pletely depressurised The pressure accumulator must be completely relieved WARNING Accident hazard from asphyxiation A break in the pneumatic hose may result in the uncontrolled exit of nitrogen into the laboratory f An oxygen warning device should be present in the laboratory if ...

Page 23: ...may heat up or be subject to magnetic attraction f Ferromagnetic materials and electromagnets must be kept away from the mag netic source Such materials could be subject to magnetic attraction and may fly around the room injuring or killing people Minimum distance 3 meters f Remove magnetic items jewelry watches pens etc before carrying out mainte nance work f Keep electronic equipment away from t...

Page 24: ...esult in serious burns f Do not touch device parts of cooled or heated units f Do not use damaged samples f After removing a sample or cassette allow it to cool or thaw before coming in con tact NOTICE Material damage hazard from overflow of cryogens Material damage may result from the overflow of cryogens f Turn off the SampleXpress during magnet servicing f Cover the SampleXpress with a protecti...

Page 25: ...ntenance work remove the samples and use dummy samples if necessary f Strictly observe the correct sample adjustment i e the maximum sample height f Always transport the cassette with the cover Never turn the cassette upside down or on it s side The laboratory supervisor is responsible for f Establishing and enforcing standard sample handling and cleaning procedures f Establishing and enforcing th...

Page 26: ... for repair of damaged parts NOTICE Material damage hazard from heavy samples Samples may be damaged due to incorrect sample lift pressure adjustment f Adjustment is valid only for 1 sample configuration and weight f Personal must be trained WARNING Danger to life from nonfunctional safety devices If safety devices are not functioning or are disabled there is a danger of serious injury or death f ...

Page 27: ...ury or death f Before the initial commissioning of the appliance connect the main power supply to the socket and verify the complete functionality of the protective earth conduc tor NOTICE Danger to the environment from incorrect handling of pollutants Incorrect handling of pollutants particularly incorrect waste disposal may cause seri ous damage to the environment f Always observe the instructio...

Page 28: ... high concentrations Disposal of the empty gas cylinders must be performed by a specialized disposal company Coolants When released coolants develop decomposition products which are hazardous to the environment Maximum care and caution are required when handling coolants Always observe the safety data sheet issued by the manufacturer Ensure that personnel handling coolants are regularly informed a...

Page 29: ...ht Warning indicating a danger spot in work rooms Keep hands away from areas bearing this warning sign There is a danger that hands could be crushed drawn in or other wise injured There is a danger that the sample breaks if the sample exceeds the maximum sample height ...

Page 30: ...rom the manufacturer See Contact on page 121 for manufacturer s address 3 9 Location of Safety Label Figure 3 3 Location of Cassette Warning Label NOTICE Material damage hazard from glass tube breakage or sample blockage in the BST Material damage from glass breakage or samples becoming stuck in the BST may result if non OEM replacement parts are used f Replacement parts must meet OEM standards ...

Page 31: ...cassette 17 kg Weight with 60s cassette without any sample 25 kg Length 85 cm Width 65 cm Height 50 cm Table 4 1 Technical Data General Information Data Value Unit Voltage 208 230 V C Apparent power consumption maximum 120 VA Circuit protection 2 x 1 0 Slow Blow A Frequency 50 60 Hz Table 4 2 Electrical Connection Values ...

Page 32: ...Data Value Unit Operating pressure 4 7 bar Compressed air requirement minimum 100 l min Oiling maximum 0 005 mg m3 Table 4 3 Pneumatic Connection Values Data Value Unit Temperature range 5 30 C Relative humidity at 31 C maximum 80 Decreasing linear till relative humidity 50 at 40 C maximum 50 Table 4 4 Operating Environment Manual Bruker Part Number Site Planning for AVANCE Systems 300 700 MHz UM ...

Page 33: ...Rating Plate The rating plate is located at the power input and includes the following information Manufacturer Type Voltage Frequency Apparent power consumption maximum Year of Production PN Part Number SN Serial Number Va Variant ECL Engineering Change Level ...

Page 34: ...dard spinner geometry Standard NMR tubes 3 10 mm Melted reference samples Match spinner 1 1 7 2 2 5 3 4 4 25 5 mm Shuttle POM for sample tubes 1 1 7 mm Dummy samples Samples with or without horizontal barcode The sample is handled at the spinner only Figure 4 2 Samples Allowed Maximum Height 7 180 mm ...

Page 35: ... Z31900_00_01 5 Design and Function 5 1 Overview Figure 5 1 Overview 1 Status Light 2 Base Unit 3 NMR Access Position 4 Cassette Guide 5 Emergency Stop 6 Touch Panel 7 Control Panel 8 Magnet 9 Base Plate ...

Page 36: ...e cassette Thereby it is possible to remove the cassette for filling removing samples The cassette has a capacity of 60 samples Operation of the unit is controlled by the application software The SampleXpress will not automatically move an actor during a running NMR measure ment unless it is desired by the operator e g to move to another position 1 Cassette Cover 2 Sample Conveyor Chain 3 Spinner ...

Page 37: ...op side of the base plate The mechanical tolerances are fixed there is no need to adjust any thing between the base plate and the base unit Pneumatic Cylinders All actuators except the motor driving the sample conveyor chain are pneumatic cylin ders All cylinders are single acting this means they will move to their home position without electrical power or sufficient air supply Under normal operat...

Page 38: ... parts As an option for very strong magnetic fields the motor can be placed outside the 5 Gauss line Cassette Clamp Mechanism Figure 5 4 Clamp Closed 1 Gripper Figure 5 5 Clamp Open When a cassette is moved into the Sam pleXpress it is fixed by a clamping mecha nism This is a special kind of gripper adapted to a pneumatic gripper cylinder The gripper Figure 5 4 1 is placed behind a metal shield to...

Page 39: ...nto the mag net they have to be safely led into the proper position The sample guide is driven by a pneu matic cylinder placed in the base unit The pneumatic cylinder fits into the opening in the rear side of the cassette Figure 5 7 In this opening there is a movable half shell and a fixed half shell which interact with the sample guide Figure 5 7 Cassette 1 Movable Half Shell ...

Page 40: ...it to align on the correct position When the conveyor chain link is stopped near the correct posi tion the sample guide is activated and works as a conveyor chain block lever whereas the movable half shell Figure 5 9 2 clasps the lower part of the conveyor chain link and fixes it in the precise NMR access position required above the BST Figure 5 8 Sample Guide 1 Guide inactivated 2 Guide activated...

Page 41: ...k has a small hole Figure 5 11 2 into which the sample release lever Figure 5 11 3 fits When the conveyor chain link is positioned above the BST the sample release lever is led through the opening in the conveyor chain link and thus releases the sample The sample falls through the con veyor chain link into the magnet Figure 5 10 Base Unit 1 Sample Release Lever Figure 5 11 Conveyor Chain Link 1 Le...

Page 42: ...n Single Access mode the cassette is connected to the base unit and the cassette cover is installed The cassette can then be filled with samples one by one at the operator access position This is the standard operation mode when SampleTrack is used as the control software Random Access Mode In Random Access mode the cassette cover is removed The samples can be filled in any available position This...

Page 43: ...ed with a touch screen which controls the application software i Battery Note The Control Panel contains a battery which is responsible for the correct function ing of the date and time The expected life time of the battery is about six years Replacement of the battery must only be carried out by employees of the manufacturer Figure 5 13 Control Panel 1 Push button Power 2 Touch screen 3 EMERGENCY...

Page 44: ... 2 BST Interface Cable to BST 3 Gas Interrupt future feature 4 Lift Adjustment Knob 5 Status and Control 6 Pressure Gauge 7 Air Supply Adjustment Knob 8 Air Supply 9 External R232 future feature 10 Console RS232 11 CAN Network to Control Panel 12 External Signal 1 future fea ture 13 External Signal 2 future fea ture 14 External Signal 3 future fea ture 1 2 3 4 6 5 7 8 9 10 11 12 13 14 ...

Page 45: ...45 Z31900_00_01 Design and Function Figure 5 15 Connections Right Side 1 Power Control from Control Panel 2 Fuse Cartridge 3 DC In future feature 4 Power Supply 1 4 2 3 ...

Page 46: ...ervice Mode orange The orange indicator lamp is illuminated when the device is in service mode or when the system is booting 3 Operating readiness green The green indicator lamp is illuminated when the device is accessible 4 Operating readiness blue The blue indicator lamp is illuminated when user interaction is required for example when the cassette is absent cassette is processed cassette is emp...

Page 47: ... Function 5 6 Work and Danger Zones NMR Access Position Figure 5 17 NMR Access Position The arrow indicates the danger zone When no cassette is present it is pos sible that the device operator may be caught in the gripper claws ...

Page 48: ...ette and Control Panel Figure 5 18 Cassette and Control Panel The arrow indicates the danger zones It may be possible that the device oper ators bang their heads against the SampleXpress due to the height of the control panel or the cassette ...

Page 49: ...d to cover the SampleXpress with the fol lowing cover Barcode Collar Set Shortened Status Cupola for Cryofit and HR MAS Changer Adaptation Stair Part Number Stair with 2 steps Z106255 Stair with 4 steps Z106254 Accessory Part Number BACS2 Protective Cover Magnet Service 1804420 Accessory Part Number Barcode Collar Set H10113 Accessory Part Number Shortened Status Dome HZ17007 ...

Page 50: ...0_00_01 Design and Function Cryofit Mounting Kit External Control Panel Figure 5 19 External Control Panel Accessory Part Number Cryofit Mounting Kit HZ16826 Accessory Part Number External Control Panel H118947 ...

Page 51: ...ing The following symbols are affixed to the packaging material Always observe the sym bols during transport and handling Top Fragile Protect Against Moisture The arrow tips on the sign mark the top of the package They must always point upwards otherwise the content may be damaged Marks packages with fragile or sensitive contents Handle the package with care do not allow the package to fall and do...

Page 52: ... packages Note the location of the center of gravity when lifting and trans porting Indicates the weight of packages Handle the marked package in accordance with its weight Indicates packages which are partially stackable Do not exceed the maximum load bearing capacity specified on the symbol in order to avoid damaging or destroying the content The packaging is air tight Damage to the barrier laye...

Page 53: ...ation Note the extent of the damage on the transport documentation or the shipper s delivery note Initiate complaint procedures i Issue a complaint in respect to each defect immediately following detection Damage compensation claims can only be asserted within the applicable complaint deadlines The packaging contains components which are sensitive to an electrostatic charge Only allow packaging to...

Page 54: ...ckaging material in accordance with the relevant applicable legal require ments and local regulations 6 4 Storage Storage of the Packages Store the packages under the following conditions Do not store outdoors Store in dry and dust free conditions Do not expose to aggressive media Protect against direct sunlight Avoid mechanical shocks Storage temperature 15 to 35 C Relative humidity max 60 If sto...

Page 55: ...ion and Initial Commissioning i Installation initial commissioning retrofitting repairs adjustments or dismantling of the device must only be carried out by employees of the manufacturer or persons authorised by the manufacturer ...

Page 56: ...56 Z31900_00_01 Installation and Initial Commissioning ...

Page 57: ... a restart 5 Keep access routes clear for emergency service vehicles 6 If warranted by the gravity of the emergency notify the responsible authorities 7 Delegate specialist personnel to rectify the fault 8 Before the restart check the device and ensure that all safety devices are installed and fully functional WARNING Danger of injury from improper operation Improper operation can result in seriou...

Page 58: ...ored sample loading unloading or place the cassette on a desk before loading unloading samples The laboratory supervisor should define who should be allowed to load or unload sam ples from cassettes and when The operator should work carefully and optimally use tube ID barcode collars ID Barcode When the sample ID barcode is dirty it should be cleaned according to established instruction or the sam...

Page 59: ... off the device or Cancel to continue operation Note Pressing and holding the Power button for 5 seconds will also shut down the SampleXpress Figure 8 1 Power Button Press the Power button on the control panel Bruker screen appears If a cassette is inserted the SampleXpress starts initialization The device checks if a sample is in the cassette The indicator lamp switches over to blue see also page...

Page 60: ...mple is too long do not use it in the SampleXpress DANGER Danger of injury due to glass tube breakage Broken glass tubes may cause minor to severe injuries as well as material damage Substances escaping the broken glass tubes may be hazardous or allergenic and therefore cause minor or severe injuries or even death f Wear protective equipment f Refer to the corresponding precautions and cleaning di...

Page 61: ...ts of three modes of operation Single Access Mode In the Single Access Mode the cassette is used with the cover and the only way to fill the casette is at the Operator Access Position A correct assignment of sample and posi tion is only possible in this mode which leads to high throughput operation The operating description in the following sections refer to this operation mode Random Access Mode ...

Page 62: ...creen in Single Access Mode Figure 9 1 Main Screen Example in Single Access Mode 2 1 3 4 Position Function 1 Message display 2 Displays the cassette with its 60 positions Gray positions are empty positions White positions are loaded with samples 3 Information about Operator Access Position and Sample Down 4 Touch screen buttons ...

Page 63: ... also Working in Random Access Mode on page 87 2 1 3 4 Position Function 1 Message display 2 Displays the cassette with its 60 positions Only gray positions are displayed The system does not show which positions are empty or filled 3 No information is displayed in Random Access Mode 4 Touch screen buttons ...

Page 64: ...easurement Each position can be displayed in different colors with different meanings Figure 9 2 Cassette 1 Operator Access Position 2 NMR Access Position Icon Color Function Blue A sample has been transferred from the NMR Access Position to the BST and is in measurement White A sample occupies this position Gray The position is empty and available Green Indicates the measurement is finished Orang...

Page 65: ...s For device configuration See also chapter The Settings Window on page 82 When the button text is black with a blue frame it means the function is enabled and available for use When the button text is gray with italic letters and a gray frame it means the function is disabled and not available for use Use the Back button in the upper right corner of the screen to return to the previous menu This ...

Page 66: ...to green otherwise the indicator lamp switches to red indicating an error has occurred The initialization display appears Figure 9 4 SampleXpress Device Initialization 9 3 1 Program Start After starting the program several messages are displayed in the message display Figure 9 5 Message Display Adapting cassette Figure 9 6 Message Display Scanning all samples When no cassette has been inserted the...

Page 67: ...ns and displays them as white Empty positions are displayed as gray 9 4 Displaying Position Information The Info button in the main menu opens a screen showing all the positions which are filled with a sample 1 Press the Info button in the main screen The sample information screen is displayed Figure 9 8 Information Screen 2 Press on a position to view the position details ...

Page 68: ...9 5 Add or Remove Samples in Single Access Mode With this function it is possible to add or remove samples from the cassette All actions with the Add or the Remove button apply to the Operator Access Position Figure 9 2 1 i The laboratory supervisor is responsible for adding removing samples Never add or remove samples without the permission of the laboratory supervisor Figure 9 9 Main Menu Touch ...

Page 69: ...gure 9 10 The Add Selection Window 2 Press the Go To Position button to choose the sample position The Position selection screen appears Figure 9 11 Position Selection Screen 3 Select an empty gray position to insert the sample into white positions are loaded with samples The conveyor chain rotates the selected position to the Operator Access Position during which a message is displayed on the scr...

Page 70: ...g message is displayed Figure 9 13 Insert Sample Screen 4 Insert the sample into the Operator Access Position Figure 9 14 1 Figure 9 14 Operator Access Position i Note Make sure the sample height is within the limits set in Sample Adjustment and Maximum Sample Height on page 60 The selection screen Figure 9 11 will be displayed again ...

Page 71: ...e position The following message is displayed Figure 9 15 Replacing a Sample 9 5 1 1 Adding Samples Go to Free Position When samples do not need to be in any specific order it is faster to add a sample in the nearest free position 1 Press the Add button in the main screen Figure 9 16 Add Remove Button The Add selection screen is displayed Figure 9 17 Go to free ...

Page 72: ...ert a new sample or press the Skip position button to continue to the next avail able position Figure 9 19 Inserting the Sample When a sample has been inserted the chain rotates automatically to the next free position Exception When the chain has been completely filled an information screen is displayed Figure 9 20 Display No more free positions ...

Page 73: ...ce from Position 1 Press the Add button Figure 9 16 in the main screen The Add selection screen is displayed 2 Press the In sequence from position button The Position selection screen appears 3 Select an empty gray position for adding a sample or a filled position for replacing 4 Add the sample to the position selected The chain rotates in ascending order to the next position whereas another sampl...

Page 74: ...reen 2 Press the Go to position button to choose the sample position The Position selection screen appears Figure 9 23 Position Selection Screen 3 Select a white loaded position for removing gray positions are empty positions While the conveyor chain rotates the selected position to the Operator Access Position a message is displayed on the screen Figure 9 24 Going to Position ...

Page 75: ... Figure 9 26 Operator Access Position The selection screen Figure 9 11 will be displayed again 5 To finish this function f Press the Back button or To remove another sample f Press a white position 9 5 2 1 Removing All the Samples To remove all the samples individually through the Operator Access Position 1 Press the Remove button Figure 9 16 in the main screen The Remove selection screen is displ...

Page 76: ... The chain rotates to the next position filled with a sample This procedure will be repeated until all samples are removed from the cassette To skip a sample press the Skip position button When all samples have been removed a message is displayed that no more samples are in the cassette apart from any skipped samples Figure 9 29 No more samples in the cassette 4 Press the Back button to return to ...

Page 77: ...te is Finished Figure 9 30 Finished Samples To remove all measured samples individually through the Operator Access Position 1 Press the Remove button Figure 9 16 in the main screen When measured samples exist the Measured button is enabled 2 Press the Measured button Figure 9 31 Remove Measured The chain rotates the nearest measured sample to the Operator Access position Figure 9 32 Removing Meas...

Page 78: ...with a measured sample This procedure will be repeated until all measured samples are removed from the cas sette To skip a measured sample press the Skip Sample button When all finished samples have been removed a message is displayed that no more finished samples are in the cassette apart from any skipped samples Figure 9 34 No more measured samples in the cassette 4 Press the Back button to retu...

Page 79: ...ition for removing gray positions are empty positions Use the Skip Sample button to skip a sample Use the Back button to return to the main menu See also the figures in chapter Removing Samples on page 74 9 5 3 Security Eject The Security Eject function is only active when no BST Sample Down Detection Sensor was configured in the setup After inserting a new cassette or when rebooting the system th...

Page 80: ...emoving the Cassette To remove the cassette 1 Press the Remove button in the main menu Figure 9 36 Main Screen The Remove selection screen is displayed 2 Press the Cassette button The conveyor chain link 1 moves to the Operator Access Position An information screen is displayed Figure 9 37 Question for removing the cassette The lamp indicator switches to blue The program will ask for confirmation ...

Page 81: ... message will be displayed Figure 9 38 Information Screen 4 Lift the cassette using the hand holds You should feel a slight resistance 5 Remove the cassette carefully The buttons will no longer be accessible gray colored and a message is displayed Figure 9 39 Message Screen ...

Page 82: ...ed i The cassette can be used without a cover In this mode the control display may not be accurate because samples can be inserted or removed without program control 9 7 The Settings Window The Settings button opens a settings window containing two tabs A User tab for touch screen calibration and for setting the date and time A Service Bruker tab which is password protected and can only be used by...

Page 83: ...e device 3 Select the Touch Screen tab and press the Start Calibration button A calibration screen will appear Figure 9 42 Calibration Screen 4 Follow the information on the screen using your fingers to move the cross for cali bration i It is important to press the middle of the cross where it appears on the screen After the calibration is complete the program will automatically return to the gene...

Page 84: ...Settings button in the main menu The Settings User screen will appear Figure 9 43 Settings Screen 2 Press the General button on the User tab 3 Press the Date Time tab Figure 9 44 Date and Time Screen 4 Change the date and time The Set Date and Time button will be activated and will change to black 5 Save the settings by pressing the Set Date and Time button ...

Page 85: ... Identification Device type Model number Serial number ECL Engineering Change Level Software Others Firmware Network 1 Press the Settings button in the main menu The Settings screen will appear Figure 9 45 Settings Screen 2 Press the General button on the User tab 3 Select the About device tab to display the device data ...

Page 86: ...86 Z31900_00_01 Operation Figure 9 46 About Device Screen 4 Press the Back button to return to the previous screen ...

Page 87: ...Access Mode Use the Left and Right buttons to move the conveyor chain left or right By pressing one of these buttons for a short interval the chain moves one position Likewise by pressing one of the buttons for a longer interval the chain moves for as long as the button is pressed During this time only gray positions are displayed the system does not show which positions are empty or filled For th...

Page 88: ...9 4 The sample can be inserted manually into the BST at the sample NMR Access Posi tion just as it was inserted before the SampleXpress device was mounted WARNING Danger of injury from an unexpected restart In the event of an unexpected restart of the power supply during manual mode there is a danger of serious injuries for persons in the danger zone The gripper grips the spinner with the sample w...

Page 89: ... sample adjustment i e the maximum sample height f Always transport the cassette with the cover Never turn the cassette upside down or on it s side The laboratory supervisor is responsible for f Establishing and enforcing standard sample handling and cleaning procedures f Establishing and enforcing the use of protective clothing and equipment f Training laboratory personnel f Preparing an emergenc...

Page 90: ... Before putting the device back into operation Make sure that all maintenance work has been performed and completed fol lowing the instructions and information provided in this manual Make sure that no persons are still in the danger zone of the device Make sure that all covers and safety devices have been installed and function properly WARNING Danger to life from an unauthorized restart In the e...

Page 91: ... by Bruker Service staff The only exception is the cassette Only original parts from Bruker are to be used for the SampleXpress Use of any parts other than from Bruker invalidates all warranty Parts which are returned to Bruker for repair or disposal must be accompanied by a repair declaration see Repair Declaration on page 157 10 3 Preventative Maintenance All parts in the SampleXpress have been ...

Page 92: ... set to change the linear speed NOTICE Material damage hazard from heavy samples Samples may be damaged due to incorrect sample lift pressure adjustment f Adjustment is valid only for 1 sample configuration and weight f Personal must be trained Figure 10 1 Connections Left Side 1 BST Interface Cable from SLCB BSMS 2 BST Interface Cable to BST 3 Gas Interrupt future feature 4 Lift Adjustment Knob 5...

Page 93: ... supply cable 4 Restart the SampleXpress 10 5 2 After a Quench 1 Disconnect the SampleXpress from the power supply 2 Contact Bruker service immediately In the event of a quench it is possible that the SampleXpress may be damaged In this case the SampleXpress should be returned to Bruker for repair 10 6 Maintenance Schedule The sections below describe the maintenance work required to ensure optimal...

Page 94: ... that the USB memory stick has enough free space and is FAT32 formatted If the USB memory stick is disconnected wait 5 seconds until the stick is reconnected 1 Stop all automatic operations 2 Plug the USB memory stick in the USB port at the right side of the control panel A screen appears and the indicator lamp switches over to yellow The device searches service files on the USB memory stick This ...

Page 95: ...indow i The file is saved in the directory Bruker Automation logs on the USB stick The file name consists of device name model number serial number date YYYYMMDD and time hhmmss e g X Bruker Automation logs SampleXpress_modelno_serialno_YYYYMMDD_hhmmss log 5 Press the OK button 6 Disconnect the USB memory stick from the device 7 Send the log file to the customer service See Contact on page 121 for...

Page 96: ...cut off during the entire procedure Otherwise you will have to send for a service technician Make sure that the USB memory stick has enough free space and is FAT32 formatted 1 Stop all automatic operations 2 Plug the USB memory stick in the USB port at the right side of the control panel A screen appears and the indicator lamp switches over to yellow Figure 10 4 Service File The application softwa...

Page 97: ...button After searching for the USB memory stick a selection screen appears Figure 10 5 Firmware Versions Several firmware versions may be displayed 4 Select the firmware version which you want to update on the device If you are not sure which to use contact Bruker service The selected firmware is highlighted purple Figure 10 6 Firmware Versions 5 Press the Update button ...

Page 98: ...0_01 Maintenance Figure 10 7 Confirm Screen 6 Press the Yes button Firmware is being updated and a notice appears on the touch screen 7 After the update is finished disconnect the USB memory stick from the device ...

Page 99: ...tick has enough free space and is FAT32 formatted If the USB memory stick is disconnected wait 5 seconds until the stick is reconnected 1 Stop all automatic operations 2 Plug the USB memory stick in the USB port at the right side of the control panel A screen appears and the indicator lamp switches over to yellow The application software searches service files on the USB memory stick This may take...

Page 100: ...ocess is finished write down the name and the path of the log file Fig ure 10 10 i The file is saved in the directory Bruker Automation logs on the USB stick The file name consists of device name model number serial number date YYYYMMDD and time hhmmss e g X Bruker Automation logs SampleXpress_modelno_serialno_YYYYMMDD_hhmmss log 5 Press the OK button 6 Disconnect the USB memory stick from the dev...

Page 101: ...the device 10 8 Cleaning 10 8 1 Before Cleaning 1 Stop the submitted jobs in the IconNMR automation mode 2 Stop the SampleXpress from doing any actions 3 Switch the power off see Switching Off the Device on page 59 4 Disconnect the power supply Figure 10 11 3 Figure 10 11 Connections Right Side 1 Power Control from Control Panel 2 Fuse Cartridge 3 DC In Future feature 4 Power Supply 1 4 2 3 ...

Page 102: ... until the unit is completely dry before you reconnect the power cable 10 8 3 Cleaning the Outer Shell of the Device i Use only water as a cleaning fluid Do not disassembly the device for cleaning Do not use acetone for cleaning Clean only the outer shell of the device with a lint free cloth dampened in water 10 8 4 Cleaning the Magazine Light Barrier i Excessive dust or dirt at the lens surface o...

Page 103: ... used containing radioactive or other hazardous materials In case of an accident with toxic radioactive explosive or biologically active sub stances the device and associated equipment must be cleaned in such a way that no danger emanates from the device and associated equipment especially for all unin formed personnel If a device has to be cleaned of all remains of a substance for safety reasons ...

Page 104: ...104 Z31900_00_01 Maintenance ...

Page 105: ...e following information Part number and serial number of the SampleXpress Spectrometer type and order number Magnet type With this information contact the customer service See Contact on page 121 for con tact details Also contact the manufacturer in the event of faults which cannot be rectified in accor dance with the instructions found in this chapter 11 1 Safety Electrical System WARNING Electri...

Page 106: ...fitted and completely functional f Do not unlock the EMERGENCY STOP button until the danger is no longer pres ent f For a software restart the green Restart Button on the control panel display must also be pressed NOTICE Before you restart the device after an error make sure that no samples are in an incorrect position for example stuck part way down into the magnet or at an incor rect level in th...

Page 107: ...executed troubleshooting work may result in serious injury and significant damage to property f Ensure sufficient assembly space before starting work f Pay attention to orderliness and cleanliness in the assembly location Loosely stacked or scattered components and tools could cause accidents f If components have been removed pay attention to correct assembly refit all fix ing elements and comply ...

Page 108: ...nsists of 9 digits The code has the following form xxx xxx xxx shown in Figure 11 3 Figure 11 3 Error Message NOTICE Contact Bruker customer service In the event of a fault an error message may appear on the touch screen f Do not use the device anymore f Contact the customer service of Bruker see Contact on page 121 for contact details and follow the instructions of the customer service ...

Page 109: ...cator lamp indicates the various operating statuses using different colored light signals Refer to the section Indicator Lamp on page 46 for details NOTICE Contact Bruker customer service In the event of a fault an information about a device failure may appear on the touch screen f Contact the customer service of Bruker see Contact on page 121 for contact details and follow the instructions of the...

Page 110: ...tion After rectifying the fault perform the following steps to restart the system 1 Acknowledge the fault at the controller 2 Ensure that no persons are in the danger zone 3 Reset the emergency stop devices Screens appear on the touch screen A new initialization will begin ...

Page 111: ...Clean replace the barcode collar used 103 310 130 Unknown Tube ID The requested Tube ID is not recognized by the device Check if there is a sample in the sample pool available with this Tube ID Clean the barcode reader detec tion surface Clean replace the barcode collar used 103 310 001 103 310 005 117 310 021 Cassette is missing or could not be iden tified correctly The cassette is missing or the...

Page 112: ... sample back into the magazine The sample detection sensors work well 103 310 094 103 310 096 117 310 058 117 310 038 117 310 124 Missing empty posi tion for eject The position where the sample from the magnet should be ejected to is occupied Allow at least 1 empty position in the cassette Check if there is really a sample Clean sensor surfaces Adjust sample detection threshold Bruker service only...

Page 113: ...op active The emergency stop button is currently pressed Be sure that the device and all of its samples are in a secure state before you release the emergency stop button and restart the device 117 310 022 117 310 023 117 310 024 117 310 025 117 310 113 117 310 115 117 310 116 117 310 117 Moving to destination position failed The requested destination posi tion could not be reached Check if someth...

Page 114: ...he sample pool which are marked as measured 117 310 111 Adapting cassette failed The cassette could not be adapted successfully Try again 117 310 112 Closing Clutch failed The mechanical adaptation of the driving unit failed The clutch could not be closed Try again Use another cassette 117 310 114 Open Cassette Clamp failed The cassette clamp which fixes the cassette could not be opened successful...

Page 115: ...117 410 014 Sensor Error Sam ple Guide both sen sors active The internal plausibility check of the sensors failed The system stopped to avoid any damage to the equipment Contact Bruker for replacing the defective parts 117 410 015 Sensor Error Sam ple Release both sensors active The internal plausibility check of the sensors failed The system stopped to avoid any damage to the equipment Contact Br...

Page 116: ...116 Z31900_00_01 Error Codes ...

Page 117: ...ed out by employees of the manufacturer or persons authorised by the manufacturer 13 1 Safety Electrical System WARNING Electrical hazard from electrical shock A life threatening shock may result when the housing is open during operation f Disconnect the device from the electrical power supply before opening the device Use a voltmeter to verify that the device is not under power f Be sure that the...

Page 118: ...nd the dismantled components for recycling Scrap metals Send plastic elements for recycling Sort and dispose of other components in accordance with their material composi tion WARNING Danger of injury due to improper dismantling Stored residual energy angular components points and edges on and in the device or on the tools needed can cause injuries f Ensure sufficient space before starting work f ...

Page 119: ... waste disposal may cause seri ous damage to the environment f Always observe the instructions below regarding handling and disposal of pollut ants f Take the appropriate actions immediately if pollutants escape accidentally into the environment If in doubt inform the responsible municipal authorities about the damage and ask about the appropriate actions to be taken ...

Page 120: ...120 Z31900_00_01 Dismantling and Disposal ...

Page 121: ...ontact our NMR service centers Bruker BioSpin NMR provide dedicated hotlines and service centers so that our special ists can respond as quickly as possible to all your service requests applications ques tions software or technical needs Please select the NMR service center or hotline you wish to contact from our list avail able at http www bruker biospin com hotlines_nmr html ...

Page 122: ...122 Z31900_00_01 Contact ...

Page 123: ...light f Do not look into the ray of light f Switch off the equipment before maintenance work WARNING Biological chemical hazard Infection contamination or other health endangerment as a result of contact with biological or chemical substances e g from broken samples f Clean the device before maintenance work and or returning to Bruker for repair f Prepare a list of materials in which the device ca...

Page 124: ...vy samples Samples may be damaged due to incorrect sample lift pressure adjustment f Adjustment is valid only for 1 sample configuration and weight f Personal must be trained CAUTION Accident hazard from hazardous materials An allergic reaction may be caused by sample substances f Protective clothing should be used as directed by the laboratory supervisor f Proper handling of sample substances mus...

Page 125: ... equipment damage f Use a platform with railings instead of a ladder to reach the assembly area f Where appropriate clothing e g slip free shoes NOTICE Material damage hazard from illicit sample movement Material damage may result from illicit sample movement during installation and maintenance f Use only dummy samples during installation and maintenance WARNING Accident hazard from suffocation A ...

Page 126: ...may be pinched due to movement of mechanical parts f Shut off the device before accessing the device CAUTION Accident hazard from loose clothing or long hair becoming caught in magazine chain Wearing loose clothing or long hair around the magazine chain may result in the clothing or hair being pulled into the magazine chain causing injury f Do not wear loose clothing or jewelry in the vicinity of ...

Page 127: ... on a side The laboratory supervisor is responsible for f Establishing and enforcing standard sample handling and cleaning procedures f Establishing and enforcing the use of protective clothing and equipment f Training laboratory personnel f Preparing an emergency plan NOTICE Material damage hazard from glass tube breakage or sample blockage in the BST Material damage from glass breakage or sample...

Page 128: ...ure that personnel are aware of this risk f Refer to the BST or probe manual for more information WARNING Risk to life for unauthorized personnel due to hazards in the danger and working zone Unauthorized personnel who do not meet the requirements described in this manual will not be familiar with the dangers in the working zone Therefore unauthorized per sons face the risk of serious injury or de...

Page 129: ...rom the power supply Contact with these com ponents may result in serious or fatal injury f Before working on the specified components ensure that they have been com pletely disconnected from the power supply Allow 10 minutes to elapse in order to ensure that the internal capacitors have been fully discharged WARNING Danger of injury due to movements caused by stored pneumatic forces Pneumatically...

Page 130: ...m distance 3 m f Remove magnetic items jewelry watches pens etc before carrying out mainte nance work f Keep electronic equipment away from the magnetic source Such equipment could be damaged f Keep storage media credit cards etc away from the magnetic source Data could be erased WARNING Danger of injury from vapor formation During the work process vapors may form which cause serious injury if inh...

Page 131: ...rth conductor may result in contact voltage This may pose a risk of injury or death f Before the initial commissioning of the appliance connect the main power supply to the socket and verify the complete functionality of the protective earth conduc tor NOTICE Danger to the environment from incorrect handling of pollutants Incorrect handling of pollutants particularly incorrect waste disposal may c...

Page 132: ...nd significant damage to property f Carry out all operating steps in accordance with the specifications and instructions in this manual f Before starting work ensure that all covers and safety devices are installed and functioning properly no persons are in the danger zone f Never disable or bypass safety devices during operation ...

Page 133: ...vant d effectuer les tâches de maintenance AVERTISSEMENT Risque biologique ou chimique Risque d infection ou de contamination ou autre risque d exposition préjudiciable à la santé en conséquence du contact avec des substances biologiques ou chimiques par ex à cause d échantillons brisés f Nettoyez l appareil avant d effectuer les tâches de maintenance et ou de retourner l appareil à Bruker pour ré...

Page 134: ...asque de protection f Respectez les instructions de montage figurant dans le manuel d installation MISE EN GARDE Risque d endommager le matériel à cause d échantillons trop lourds Des échantillons peuvent être endommagés à cause d un réglage incorrect de la pression de levage des échantillons f Chaque réglage n est valide que pour un seul poids et un seul type de configura tion d échantillon f Le ...

Page 135: ...ager le matériel à cause d un choc sur l aimant Tout choc sur l aimant peut provoquer un quench f Installez avec précaution l appareil sur l aimant f Evitez de cogner l aimant au cours de l installation et du fonctionnement par ex lorsque vous remettez la cassette d échantillonnage en place MISE EN GARDE Risque d endommager le matériel à cause d un manque de sûreté dans les pratiques d assemblage ...

Page 136: ...zote f Veuillez noter qu une fuite au niveau du circuit principal d alimentation ne peut pas être stoppée à l aide du SampleXpress MISE EN GARDE Risque d endommager le matériel à cause d un débordement de cryo gènes Le débordement de cryogènes peut endommager le matériel f Eteignez l appareil pendant les opérations d entretien de l aimant f Recouvrez l appareil avec un capot de protection pour évi...

Page 137: ...s Ils risquent d être happés par la chaîne du magasin f Ne portez pas de vêtements amples ni de bijoux si vous travaillez à proximité de la chaîne du magasin f Toutes les personnes portant les cheveux longs doivent rester à distance de la chaîne du magasin ATTENTION Risque d accident à cause du contact avec des surfaces chaudes ou froides de la cassette Le contact avec les surfaces chaudes ou froi...

Page 138: ...e réglage de la hauteur maxi mum d échantillon f Transportez toujours la cassette avec son couvercle Ne tournez jamais la cas sette sur un côté et ne la retournez pas tête en bas Le superviseur du laboratoire est tenu f d établir des procédures standards pour la manipulation des échantillons et le net toyage et se doit de les faire appliquer f d instaurer l usage de vêtements et d équipements de p...

Page 139: ...er les parties endommagées ATTENTION Risque d accident pour cause de chute de l escabeau Sur certains aimants il est nécessaire d utiliser un escabeau pour atteindre l appar eil ce qui rend possible le risque de chute f N utilisez pas d escabeau f Utilisez une plateforme approuvée pour atteindre l appareil sur l aimant f Portez des chaussures à semelles antidérapantes ATTENTION Risque d accident à...

Page 140: ...ure par trébuchement si les sols sont encrassés ou encombrés Les sols encrassés et encombrés peuvent provoquer des chutes par glissade ou tré buchement et entraîner par conséquent des blessures f Maintenez toujours la zone de travail propre f Retirez de la zone de travail tous les objets qui n y sont plus indispensables et dégagez plus particulièrement le sol f Signalez les dangers qui ne peuvent ...

Page 141: ...alentour f Les personnes dotées d un stimulateur cardiaque doivent être tenues à l écart de l appareil Le fonctionnement du stimulateur cardiaque pourrait être compromis f Les personnes dotées d implants métalliques doivent être tenues à l écart de l appareil Ces implants pourraient s échauffer ou subir l attraction magnétique f Les matériaux ferromagnétiques et les électroaimants doivent être ten...

Page 142: ... rectement installés avant de commencer à travailler f Ne désactivez jamais les dispositifs de sécurité et ne les bypassez pas f Veillez à ce que l ensemble des dispositifs de sécurité soient à tout moment accessibles AVERTISSEMENT Danger de mort à cause d une remise en route non contrôlée La remise en route non contrôlée de l appareil peut causer des blessures graves ou la mort f Avant toute remi...

Page 143: ...nt la manipulation et l élimination des polluants f Prenez les mesures immédiates appropriées dans le cas où des polluants s échapperaient accidentellement dans l environnement En cas de doute informez les autorités municipales responsables du sinistre et renseignez vous sur les actions appropriées à entreprendre AVERTISSEMENT Danger de blessure à cause d une action impropre Toute opération incorr...

Page 144: ...144 Z31900_00_01 Avertissements De Sécurité ...

Page 145: ...t in den Lichtstrahl f Schalten Sie das Gerät vor Wartungsarbeiten aus WARNUNG Biologische und chemische Gefahren Gefahr von Infektion Ansteckung oder anderer Gesundheitsgefährdung durch den Kontakt mit biologischen oder chemischen Substanzen z B bei zerbrochenen Probenbehältern f Reinigen Sie das Gerät vor allen Wartungsarbeiten bzw bevor Sie es zur Repara tur an Bruker einsenden f Erstellen Sie ...

Page 146: ... möglich ist sollten Sie einen Schutzhelm tragen f Beachten Sie die Montageanweisungen im Installationshandbuch HINWEISE ZUM BETRIEB Gefahr von Sachschäden durch schwere Proben Die Proben können bei einer falschen Einstellung des Drucks am Probenlift beschä digt werden f Die Einstellung gilt jeweils nur für eine Probenkonfiguration und ein bestimmtes Gewicht f Es dürfen nur entsprechend geschulte ...

Page 147: ...en HINWEISE ZUM BETRIEB Gefahr von Sachschäden durch Anstoßen am Magnet Beim Anstoßen am Magnet besteht die Gefahr dass Teile eingequetscht werden f Gehen Sie bei der Montage am Magneten besonders vorsichtig vor f Vermeiden Sie es bei der Installation und im Betrieb z B beim Austausch der Probenkassette den Magneten hart anzustoßen HINWEISE ZUM BETRIEB Gefahr von Sachschäden durch unsicheres Arbei...

Page 148: ... sein f Beachten Sie dass der Austritt von Stickstoff an der Hauptversorgungsleitung von Seiten des SampleXpress nicht abgestellt werden kann HINWEISE ZUM BETRIEB Gefahr von Sachschäden durch überlaufendes Kühlmittel Gefahr von Sachschäden durch überlaufendes Kühlmittel f Schalten Sie das Gerät während Servicearbeiten am Gerät aus f Decken Sie das Gerät mit einer Schutzabdeckung ab um die Berührun...

Page 149: ...ngsgefahr dadurch dass Haare oder Kleidungsstücke in die Magazinkette geraten f Tragen Sie bei Arbeiten in der Nähe der Magazinkette keine lose herabhängende Kleidung oder Schmuckstücke f Personen mit langen Haaren sollten sich nicht in der Nähe der Magazinkette auf halten VORSICHT Unfallgefahr durch Berühren heißer oder kalter Oberflächen an der Kas sette Beim Berühren heißer oder kalter Oberfläc...

Page 150: ...ben f Beachten Sie unbedingt die Angaben zur korrekten Einstellung der Proben d h die maximale Probenhöhe f Transportieren Sie die Kassette nur mit der Abdeckung Stellen Sie die Kassette nicht auf den Kopf und drehen Sie sie nicht auf die Seite Der Laborleiter ist verantwortlich für f die Festlegung und Durchsetzung von Standardverfahren zur Handhabung der Proben und zur Reinigung f die Festlegung...

Page 151: ...ker wenden VORSICHT Unfallgefahr durch Sturz von der Leiter Beim Versuch das Gerät an einigen Magneten mit einer Leiter zu erreichen besteht Sturzgefahr f Benutzen Sie keine Leiter f Benutzen Sie stattdessen eine zugelassene Arbeitsbühne um das Gerät am Magneten zu erreichen f Tragen Sie Schuhe mit rutschfesten Sohlen VORSICHT Unfallgefahr durch aus dem BST austretende heiße oder kalte Luft Beim E...

Page 152: ...usrutschen auf Verschmutzungen oder Stolpern über herumliegende Gegenstände Schmutz und herumliegende Gegenstände führen zu Gefahren durch Ausrutschen oder Stolpern Bei einem Sturz besteht Verletzungsgefahr f Halten Sie den Arbeitsbereich jederzeit sauber f Entfernen Sie alle Gegenstände die nicht mehr benötigt werden aus dem Arbe itsbereich und insbesondere vom Boden f Machen Sie unvermeidliche G...

Page 153: ...plantaten aus Metall dürfen sich nicht in der Nähe der Anlage auf halten Die Implantate könnten sich erwärmen oder vom Magnetfeld angezogen werden f Ferromagnetische Werkstoffe und Elektromagnete dürfen nicht in die Nähe der Quelle des Magnetfelds gebracht werden Derartige Werkstoffe könnten angezo gen werden und durch den Raum fliegen Dabei bestände die Gefahr von schw eren oder sogar tödlichen V...

Page 154: ...eht die Gefahr schwerer oder sogar tödlicher Verletzungen f Prüfen Sie vor dem Wiedereinschalten dass die Ursache der Notabschaltung behoben worden ist dass alle Sicherheitseinrichtungen vorhanden sind und dass diese einwandfrei funktionieren f Entriegeln Sie die NOT AUS TASTE erst dann wenn keine Gefahr mehr besteht f Für einen Neustart der Software muss außerdem die grüne Neustart Taste auf dem ...

Page 155: ...nformieren Sie in Zweifelsfällen die zuständigen örtlichen Behörden über den Schaden und erfragen Sie dort die erforderlichen Maßnahmen WARNUNG Verletzungsgefahr bei nicht sachgemäßer Bedienung Bei nicht sachgemäßer Bedienung besteht die Gefahr schwerer Verletzungen und erheblicher Sachschäden f Führen Sie alle Schritte bei der Bedienung entsprechend den Spezifikationen und Anweisungen in diesem H...

Page 156: ...156 Z31900_00_01 Sicherheitshinweise ...

Page 157: ...157 Z31900_00_01 Appendix B B 1 Repair Declaration The Equipment Clearance Form on the following page needs to be used for Service Repair Disposal or Transfer of the SampleXpress ...

Page 158: ......

Page 159: ...s should be included in the manual 28 Notice Contact customer service 108 109 Material damage due to a software error 18 Material damage due to the use of genuine samples during installation and mainte nance 19 Material damage hazard due to impacting the magnet 19 Material damage hazard from glass tube breakage or sample blockage in the BST 30 Material damage hazard from heavy samples 26 92 Materi...

Page 160: ...160 Z31900_00_01 Warning Signs ...

Page 161: ...e 40 Figure 5 10 Base Unit 41 Figure 5 11 Conveyor Chain Link 41 Figure 5 12 Sample Brake 42 Figure 5 13 Control Panel 43 Figure 5 14 Connections Left Side 44 Figure 5 15 Connections Right Side 45 Figure 5 16 Indicator Lamps 46 Figure 5 17 NMR Access Position 47 Figure 5 18 Cassette and Control Panel 48 Figure 5 19 External Control Panel 50 Figure 8 1 Power Button 59 Figure 8 2 Operator Access Pos...

Page 162: ... Remove Selection Screen 74 Figure 9 23 Position Selection Screen 74 Figure 9 24 Going to Position 74 Figure 9 25 Remove Sample Screen 75 Figure 9 26 Operator Access Position 75 Figure 9 27 Remove All 76 Figure 9 28 Removing the sample 76 Figure 9 29 No more samples in the cassette 76 Figure 9 30 Finished Samples 77 Figure 9 31 Remove Measured 77 Figure 9 32 Removing Measured 77 Figure 9 33 Removi...

Page 163: ...re 10 3 Information Screen 95 Figure 10 4 Service File 96 Figure 10 5 Firmware Versions 97 Figure 10 6 Firmware Versions 97 Figure 10 7 Confirm Screen 98 Figure 10 8 Service File 99 Figure 10 9 Export Device Report 100 Figure 10 10 Export Device Report 100 Figure 10 11 Connections Right Side 101 Figure 10 12 Magazine Light Barrier 102 Figure 11 1 Sample Stuck in Magnet 106 Figure 11 2 Sample Too D...

Page 164: ...164 Z31900_00_01 Figures ...

Page 165: ...ical Connection Values 31 Table 4 3 Pneumatic Connection Values 32 Table 4 4 Operating Environment 32 Table 4 5 Bruker Site Planning Guides 32 Table 5 1 Indicator Lamps 46 Table 9 1 Cassette Color Symbols and Their Meanings 64 Table 10 1 Bruker Replacement Parts 91 Table 10 2 Maintenance Schedule 94 ...

Page 166: ...166 Z31900_00_01 Tables ...

Page 167: ...167 Z31900_00_01 Glossary C 4 Glossary BSMS Bruker Smart Magnet Control System BST Bruker Sample Transport NMR Nuclear Magnetic Resonance SLCB Sample Level Control Board ...

Page 168: ...168 Z31900_00_01 Glossary ...

Page 169: ...g 82 missing 111 modes 42 removing 80 Cassette clamp mechanism 37 Chain link deliberate play in 40 Cleaning liquids 28 Contamination 103 Conveyor chain 37 Conveyor chain link 41 Copyright 10 Cylinder supply connections 92 D Danger zone 47 cassette and control panel 48 Dangerous situations 57 Device Identification 85 Dismantling 118 E Emergency Shutdown 57 Environmental protection 91 F Firmware ver...

Page 170: ...R access position 40 NMR glass tubes 58 NMR measurement Influence on 38 O Operator Access Position 64 75 P Packaging 54 Personal protective equipment 16 Pneumatic cylinder 39 Pneumatic cylinders 37 Pollutants 28 Product liability 13 R Random Access Mode 61 Recycling 118 Relative humidity 54 Repair Declaration Form 103 Replacement parts 91 Restart 57 106 Risk assessment 14 S sample 67 Sample guide ...

Page 171: ...6 Spare parts 30 Standard Operating Procedure 14 Storage temperature 54 Strong magnetic fields 38 Swivel arm 43 T Temperature changes 58 Terms and Conditions 10 Terms of Delivery 10 TopSpin 9 61 Touch screen 43 calibration 82 Transport damage 53 Tube ID changed unexpectedly 113 invalid 111 Unknown 111 U Untrained personnel 10 V Valves 57 ...

Page 172: ...172 Z31900_00_01 Index ...

Page 173: ......

Page 174: ... solution package fromour comprehensive range or even collaborate with you on new developments Our ongoing efforts and considerable investment in research and development illustrates our long term commitment to technological innovation on behalf of our customers With more than 40 years of experi ence meeting the professional scientific sector s needs across a range of disciplines Bruker BioSpin ha...

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