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Table of contents

XD 7500

ba77191e01 - 71310060

04/2018

Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

4.1

Switching on or off the photometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

4.2

General operating principles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
4.2.1

Navigating with function keys and menus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

4.2.2

Display of navigation paths in short form . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

4.2.3

Entry of numerals, letters and characters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

4.2.4

Detailed operating example: Changing the language

. . . . . . . . . . . . . . . . . . . 31

4.2.5

Inserting a cell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32

4.2.6

Usable cells . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

4.3

Photometer settings and system administration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
4.3.1

Language . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

4.3.2

Date/Time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

4.3.3

Display settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

4.4

Zero adjustment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

4.5

Measuring in

Concentration

mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40

4.5.1

Measuring cell tests with barcode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40

4.5.2

Measuring reagent tests, external barcode reader . . . . . . . . . . . . . . . . . . . . . . . . 41

4.5.3

Measuring user-defined methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42

4.5.4

Exceeding the upper or lower limits of the measuring range . . . . . . . . . . . . . . . . 43

4.5.5

Selecting a method manually . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

4.5.6

Settings for

Concentration

mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

4.5.7

Measuring diluted samples . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46

4.5.8

Sample blank value . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48

4.5.9

Reagent blank value . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50

4.5.10 User calibration (standard adjustment)  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .  54
4.5.11 Automatic Turbidity correction   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .  61
4.5.12 Programming / modifying user-defined methods   . . . . . . . . . . . . . . . . . . . . . . . . . 61

4.6

Measuring the Absorbance / % Transmission . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
4.6.1

General information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72

4.6.2

Measuring the absorbance or transmission . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72

4.6.3

Measuring against the Reference absorbance . . . . . . . . . . . . . . . . . . . . . . . . . . . 73

4.7

Special / Multi wavelengths methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76
4.7.1

Basic information on Special / Multi wavelengths measurements . . . . . . . . . . . . 76

4.7.2

Programming / modifying the Special / Multi wavelengths methods . . . . . . . . . . . 76

4.7.3

Selecting a Special / Multi wavelengths method . . . . . . . . . . . . . . . . . . . . . . . . . . 83

4.7.4

Carrying out Special / Multi wavelengths measurements . . . . . . . . . . . . . . . . . . . 84

4.8

Spectrum . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87
4.8.1

General information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87

4.8.2

Recording a Spectrum . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88

4.8.3

Loading/editing a spectrum . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 90

4.8.4

Saving / exporting a spectrum . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93

Содержание 15150001

Страница 1: ...Lovibond Water Testing Tintometer Group EN Quick Start Guide Photometer XD 7000 Instruction manual www lovibond com ba77191e01 71310060 04 2018...

Страница 3: ...f hazardous substances 9 2 Overview 11 2 1 Overview of the instrument 11 2 2 Keypad 12 2 3 Display 13 3 Commissioning 15 3 1 Scope of delivery 15 3 2 General notes on handling 15 3 3 Initial commissio...

Страница 4: ...mits of the measuring range 43 4 5 5 Selecting a method manually 44 4 5 6 Settings for Concentration mode 45 4 5 7 Measuring diluted samples 46 4 5 8 Sample blank value 48 4 5 9 Reagent blank value 50...

Страница 5: ...xporting files 119 4 12 1 Copying all measurement data files to a USB memory device 119 4 12 2 Copying user defined methods profiles to a USB memory device 120 4 12 3 Copying files to a PC 121 4 12 4...

Страница 6: ...1 Cleaning the enclosure 156 5 2 2 Cleaning the cell shaft 156 5 2 3 Cleaning the detector lens 157 6 What to do if 158 6 1 Actions in the case of a broken cell 158 6 2 Error causes and remedies 159...

Страница 7: ...ng manual provides important information on the safe operation of the product Read this operating manual thoroughly and make yourself familiar with the product before putting it into operation or work...

Страница 8: ...carrying out of photometric measurements according to this operating manual Follow the technical specifications of the cells in Chapter 7 TECHNICAL DATA Any other use is considered unauthorized 1 3 2...

Страница 9: ...eter pays close attention to as safe an execution as possible Some hazards by dangerous substances how ever cannot always be avoided If self produced tests or solutions are used the responsibility con...

Страница 10: ...Safety XD 7500 10 ba77191e01 71310060 04 2018...

Страница 11: ...Shaft for rectangular cells 4 Turn up lid 5 Shaft for round cells 6 Cell shaft cover 7 Shaft for round cells 24 mm Figure 2 1 Front of the instrument with operating elements F4 2 1 3 5 7 6 4 8 Connec...

Страница 12: ...ion Functions ON OFF Switches on and off the photome ter HOME Switches to the main menu from any operating situation Actions that are not completed are can celed PRINT Outputs the measured value dis p...

Страница 13: ...Opens a selected menu Confirms a selection or entry Corresponds to the Test key in the method description Arrow keys or Moves the selection in menus and lists one position up or down Deletes the chara...

Страница 14: ...2018 Symbols in the status line Symbol Designation Function Save The STORE key is active You can store the displayed data with STORE see Section 4 11 Printer The PRINT key is active You can store the...

Страница 15: ...rument against hard shocks if it has to be transported The original packing is also required for the proper return of the instru ment if it has to be repaired Note that damage caused by improper trans...

Страница 16: ...time see Section 3 3 5 Carry out a zero adjustment see Section 3 3 1 Inserting the buffer batteries Four buffer batteries type AA or Mignon included in the scope of delivery supply the integrated cloc...

Страница 17: ...t is undamaged If the power cable is damaged the instrument must not be operated Connect the power pack For operation with a mobile 12 V power supply unit You can also operate the XD 7500 on the move...

Страница 18: ...nstrument automatically guides you to the setting of the time and date after the setting of the language 1 Press ON OFF The photometer is switched on The display switches to the setting of the languag...

Страница 19: ...e The input field for the current date pops up 2 Enter the current date with 0 9 and confirm The input field closes The date is accepted 3 Select and confirm Time The input field for the current time...

Страница 20: ...PC see Section 3 4 2 Printer see Section 3 4 2 USB storage media see Section 3 4 3 USB PC keyboard see Section 3 4 4 Barcode reader see Section 3 4 5 12 V auto charging cable see Section 3 4 6 Etherne...

Страница 21: ...interface Interface PC Printer Functions USB A The data is printed out with PRINT USB B Enables the direct connection of photom eter and PC With this you can transmit measurement data to the PC see Se...

Страница 22: ...USB A interface In addition the barcode reader can be used for method selection There is a barcode for each method description If the instrument is in concentration mode the instrument jumps directly...

Страница 23: ...the power supply unit and technical data for the spectrophotometer Configure the barcode reader before operation with the pho tometer to use code 128 see operating instructions for your barcode reader...

Страница 24: ...er instrument type Example Operating time with a type 12 V 19 Ah battery in optimum condition approx 16 h 12 V connection Suitable are connection cables with the following properties The spectrophotom...

Страница 25: ...ogin dialog with activated user manage ment With activated user management 2 Login Enter user name and password or register as a guest see Section 4 16 4 Then the photometer displays the Self test dia...

Страница 26: ...the photometer a note is displayed The automatic wavelength calibration only starts if the cell shaft is empty If a cell is in the cell shaft the wavelength calibration is carried out only after the c...

Страница 27: ...n keys F1 F4 Press the function key F1 Setup The General setup submenu pops up Press the key The menu selec tion moves in the corresponding direction To navigate further use and START ENTER Press STAR...

Страница 28: ...tion the START ENTER key is also used for other operations Opening a selection list or input field Confirming a selection Confirming entries of text and numerals Executing a command directly or with i...

Страница 29: ...he photometer except function keys Press the Home key The main menu is called up Square brackets in this operating manual indicate a function key F1 to F4 The text between the brack ets corresponds to...

Страница 30: ...similar to a mobile phone When pressing a key that is assigned to several characters once the respective numeral appears first To enter a numeral one key pressing is always sufficient When pressing th...

Страница 31: ...cond the character is taken over and the selection line closed 2 Complete the ID with A 9 and confirm Enter ID 8 8 T U V t u v Enter ID T 8 T T U V t u v Enter ID Test_ 1 Call up the main menu with th...

Страница 32: ...enu level Language 16 01 17 9 52 German English French Spanish Italian Bulgarian Czech Chinese Traditional Chinese Greek Indonesian German 1 Open the cell shaft cover 2 Close the inner turn up lid 3 I...

Страница 33: ...nually see Section 4 5 5 SELECTING A METHOD MANUALLY and then insert the cell If the inner turn up lid is opened too wide a message prompts you to close the inner turn up lid 1 Open the cell shaft cov...

Страница 34: ...PMMA plas tic cells are not suitable due to their transmission characteristics Therefore use quartz cells or tested single use cells plastic for applications in the UV range 4 3 Photometer settings a...

Страница 35: ...or MM DD YY How to set the language is described in detail in the operating example in Section 4 2 4 The Date Time menu opens 1 Select and confirm Date The input field for the current date pops up 2...

Страница 36: ...n measurements For all Concentrationmode there is a factory zero adjustment already when the instrument is delivered We recommend replacing it with a zero adjust ment of your own If a zero adjustment...

Страница 37: ...rly check the zero cell for visible contamination and scratches If necessary replace them recommended every 24 months Zero adjustment with rectangular cells For rectangular cells the zero adjustment m...

Страница 38: ...LANK key 2 In Concentration mode only Select and confirm Zero adjust ment The zero adjustment window pops up 3 Insert the zero cell see Section 4 2 5 INSERTING A CELL The photometer automatically star...

Страница 39: ...recommend to repeat the zero adjustment in the following cases If the photometer was subject to mechanical stress such as strong shock or transport If the ambient temperature changed by more than 5 C...

Страница 40: ...ter selects the method based on the bar code and automatically starts measur ing 6 Other options Select another citation form with Citation form e g NH4 NH4 N Select another measurement unit with Unit...

Страница 41: ...case the barcode indicates the most frequently used method By scanning this barcode with the external barcode reader the correspond ing method is selected see also Section 3 4 5 1 Open the cell shaft...

Страница 42: ...results can also be called up here Make further settings with Setup see Section 4 5 6 1 Selecting a method manually see Section 4 5 5 The photometer is ready for mea surement Concentration 16 01 17 9...

Страница 43: ...r measurement unit with Unit e g mg l mmol l With multi stage methods par tial results can also be called up here Make further settings with Setup see Section 4 5 6 Concentration 16 01 17 9 52 0 629 m...

Страница 44: ...es Range Display Example MR 10 150 mg l The last method used is selected immediately HOME Concentration Letzte Methode The list of methods is displayed The methods are sorted by method number The arro...

Страница 45: ...9 to enter the charac ter string you want to search for in the search window The list below displays all hits that include the character string With each character input the hit list is updated When...

Страница 46: ...fined blank value If available a user defined reagent blank value is used In the measured value display measurements with a user defined reagent blank value are marked by BV Lot number For further ins...

Страница 47: ...ut barcode is used Selecting a method manually see Section 4 5 5 The photometer is ready for mea surement 1 Open the settings menu with Setup 2 Select and confirm Dilution 3 Enter the dilution 0 9 and...

Страница 48: ...blank value is determined with the same procedure as the corre sponding analysis but without the coloring reagent The sample blank values required are explained in detail in the relevant analysis spe...

Страница 49: ...st single measure ment with Discard 5 To accept the median value press Apply The photometer is ready for mea surement The use of the sample blank value is indicated by SB in the top right corner of th...

Страница 50: ...d can be acti vated at any time The reagent blank values you measured yourself also remain stored in the meter until they are overwritten by a new blank value measurement Single and multiple determina...

Страница 51: ...of value pairs or the measurement and storing of standard solutions for a nonlinear function parabola or polygon line the message No blank value correction is intended for this method appears when th...

Страница 52: ...r the reagent blank value takes place The following data is displayed as the result The measured absorbance from the last single measure ment The median from all single mea surements carried out up to...

Страница 53: ...mber A 9 The blank value measurement is completed The photometer is ready for mea surement The use of the reagent blank value is indicated by BV Lot number in the top right corner of the display Reage...

Страница 54: ...iple measurement the absorbance is calculated as the median from the individual measured values If a method is called up for which a user calibration is possible a query appears asking whether the use...

Страница 55: ...of the last user calibration If no data of a user calibration are available the list to measure the Absorbance for all calibration standards required pops up 3 In the Target value column enter the nom...

Страница 56: ...the median value press Apply The list of the standards required for this method pops up The mea sured absorbance is entered for the standard or reagent blank value E0 8 Select all fields consecutivel...

Страница 57: ...w measure ment 11 Use End to finish calibration The Lot number input field for input of the Lot number of the reagent used pops up 12 Enter the Lot number of the reagent blank value A 9 and confirm Th...

Страница 58: ...ion 4 5 5 If data for zero adjustment reagent blank value or a user cali bration are already existing the photometer informs you of this You can accept or discard the existing values 1 Use ZERO BLANK...

Страница 59: ...ion should not be utilized a query with further options pops up Use default calibration The existing user calibration is erased The following measure ments are done with the original calibration that...

Страница 60: ...The photometer is ready to mea sure when all the required data have been confirmed or remea sured Concentration 16 01 17 9 52 Cal BV 2c ZERO 10 01 2012 11 08 To start measurement insert cell or press...

Страница 61: ...en creating the methods Calibration data and calibration function In photometry the calibration function describes the dependency between the measured parameter e g concentration and the photometric m...

Страница 62: ...s of the calibration line In the case of a nonlinear dependency the points of the measuring ranges can be connected to each other as a polygon line or approximated as a parabola Figure 4 2 Example of...

Страница 63: ...eagent blank value with deionized water instead of sample see Section 4 5 9 at least one up to ten standard solutions in different concentrations Based on the entered value pairs the photometer determ...

Страница 64: ...by measuring storing or entering the value pairs see above For entry as a formula you can determine the coefficients of the reverse calibration function by linear regression When doing so the concent...

Страница 65: ...concen tration of the used standard solutions Timer 0 to 3 Up to four analysis timers freely adjustable MCheck target value Any value within the measuring range MCheck tolerance Any Required measure...

Страница 66: ...te the method completely 2 Select the menu item Calibration curve Select the method for the determination of the calibration line The following variants can be selected Measure standard solutions Ente...

Страница 67: ...inal value 4 Create further value pairs with Add as necessary You can delete a highlighted value pair with Delete 5 In the Target value column enter the nominal values of the individ ual standard solu...

Страница 68: ...lank value in the Concentration Setup menu is activated for measuring with this method the value for a0 is determined and replaces the cal culated axis intercept from the programming of the method a0...

Страница 69: ...t value and MCheck tolerance 17 If necessary set the number from how many single measurements the documented measured value will be calculated 18 If necessary specify whether a reagent blank value is...

Страница 70: ...his procedure the value for a0 is determined and replaces the previous value 1 Select and confirm Enter formula Input fields for the coefficients a0 a5 of the formula are displayed 2 Enter and confirm...

Страница 71: ...ther a reagent blank value is required 9 If necessary set whether a user calibration is possible and or required 10 Complete the programming of the method with Complete The method is programmed and se...

Страница 72: ...CE ABSORBANCE 4 6 2 Measuring the absorbance or transmission The settings of the last measure ment are active 1 Using Wavelength change the wavelength as necessary 2 Using Absorbance Trans mission you...

Страница 73: ...cell type is changed the wavelength is changed a new reference value is measured it is deleted manually Reference Delete the Absorbance Transmission measuring mode is exited Single and multiple deter...

Страница 74: ...ollowing data is displayed as the result The measured absorbance from the last single measure ment The median from all single mea surements carried out up to now 3 If necessary make additional sin gle...

Страница 75: ...y for mea surement The reference absorbance is dis played in the top right corner during absorbance or transmis sion measurement Absorbance 16 01 17 9 52 Reference To start measurement insert cell or...

Страница 76: ...a value meets a condition With a condition you can check a value for validity e g absorbance value procedure variable or the result of a formula Formula editor for the convenient programming of any u...

Страница 77: ...into account any influence quanti ties that cannot be measured by the photometer The values for these procedure variables have to be entered for all mea surements with the method e g the temperature o...

Страница 78: ...ble numeric values 1 Enter the general method data here The next available method number is already entered as number You have the following possibilities for filling out the input fields Fill out all...

Страница 79: ...s and move to the next page 6 Use Add to add an additional wavelength or Use Delete to delete the marked wavelength 7 Use Next to take over all entries and move to the next page Wavelength 16 01 17 9...

Страница 80: ...rm The current status of the formula is displayed 10 Insert operator The current status of the formula is displayed Formula entry 16 01 17 9 52 Use the Operators softkey to select an operation functio...

Страница 81: ...lete the formula The current status of the formula is displayed 14 Use 17 to take over all inputs and change to the next page If an error is in the formula an error message appears The formula editor...

Страница 82: ...mplete the condition 17 Complete the programming of the method with Next If the formula includes several measurements for the same wavelength measurement sequence you can assign names for the individu...

Страница 83: ...r Select method 1 Use to select the desired method The current selection is displayed in reverse video 2 Use START ENTER to take over the selection The photometer is ready for mea surement Edit method...

Страница 84: ...Use A 9 to enter the charac ter string you want to search for in the search window The list below displays all hits that include the character string With each character input the hit list is updated...

Страница 85: ...rt cell round cell or rectangu lar cell see Section 4 2 5 INSERTING A CELL Special Multi wavelengths 16 01 17 9 52 V extract ml Press START ENTER to enter the value 2001 Chl a Chlorophyll a 10 mm 0 00...

Страница 86: ...rt measurement insert cell or press START ENTER 2001 Chl a Chlorophyll a 10 mm Setup Cancel Special Multi wavelengths 16 01 17 9 52 V extract ml 10 ml V sample ml 100 ml Measurement 1 A 665 n 0 600 Pr...

Страница 87: ...the expansion of the wavelength range on the Setup menu exiting the Spectrum mode or switching off the photometer Settings You can record a spectrum with standard settings without opening the setting...

Страница 88: ...tal value range Manual selected value range 3 Use Apply to take over all entries A message with operating instruc tions is displayed HOME Spectrum Spectrum 16 01 17 9 52 Wavelength nm Setup Open Absor...

Страница 89: ...LL 7 Start the measurement with START ENTER After recording the spectrum the message Recording of spectrum is completed appears 8 Wait until the spectrum has been recorded completely At the end of the...

Страница 90: ...d starting on Page 92 Loading a stored spectrum The cursor is shown on the abso lute maximum of the spectrum 10 You have the following possibilities Edit the spectrum immediately see Section 4 8 3 Wit...

Страница 91: ...ation Delete The cursor consists of a horizontal and a vertical line which cross at a point of the curve A box displays the x and y values of the curve point With you can move the cursor along the x a...

Страница 92: ...the Delete function key Delete all marks 2 Adjusting the zoom window With and you can specify the lower left corner of the zoom window With xy max you can mark the upper right corner of the zoom windo...

Страница 93: ...ctrum Adds a stored spectrum to the current spectrum Subtract spectrum Subtracts a stored spectrum from the current spectrum Divide spectrum ratio Divides the absorbance or transmission values of the...

Страница 94: ...r face 3 Open the save dialog with STORE 4 If necessary change the storage location with Location Internal DataB folder Exchange folder on the instrument or USB memory connected USB storage medium on...

Страница 95: ...ach measurement assumes an appropri ate profile 4 9 1 Creating editing profiles for Kinetics recordings A profile for a Kinetics recording includes the following details Profiles for Kinetics recordin...

Страница 96: ...tervals seeSection 4 9 6 Catalytic activity only for Mode Absor bance Yes or No Here you determine whether the catalytic activity should be calculated The catalytic activity is a measure for the amoun...

Страница 97: ...number Use Delete to delete the profile completely 2 Use Next to change for additional settings 3 Enter further data for the profile here 4 Use Complete to take over all entries The profile is created...

Страница 98: ...name in the list Search function The list of profiles is displayed The profiles are sorted by profile number Select profile 1 Select the desired profile with The current selection is displayed in rev...

Страница 99: ...Start the measurement with START ENTER The photometer starts recording automatically HOME Kinetics Kinetics 16 01 17 9 52 Zero measurement required Press ZERO BLANK 4001 Demo Absorbance Setup Profile...

Страница 100: ...curve with the cursor and display the mea surement data for each point see Section 4 9 6 With PRINT you can output the kinetics curve as graphic to a connected printer or as pdf file You can store the...

Страница 101: ...e storage location with Location Internal DataB folder Exchange folder on the instrument or USB memory connected USB storage medium on the USB A connection 5 If necessary change the file name 6 Use ST...

Страница 102: ...1 Measurement of absorbance 0 or transmission 1 4 1 Measurement 1x per interval 0 or as often as possible 1 5 525 Wavelength in nm 6 1280913092 Start time internal data format 7 59 Duration in sec 8...

Страница 103: ...ge medium on the USB A connec tion 2 Select the desired Kinetics record ing The curve is loaded You have the following possibili ties You can sample the curve with the cursor and display the mea surem...

Страница 104: ...16 01 17 9 52 4002 Number of measurements 4 Duration 00 00 24 Interval 00 00 06 Time s Setup Edit Open Absorbance Cursor information 1 Use Edit Slope catalytic activ ity to display the slope of the k...

Страница 105: ...me diagram for direct com parison Subtract kinetics With Edit Subtract kinetics you subtract a stored kinetics recording from the current kinetics recording The Compare kinetics function is only avail...

Страница 106: ...the Timer menu is possible in any operating situation Other functions are not disturbed by operation of the timer You exit the time overview with the ESC key When the Timer menu is opened for the fir...

Страница 107: ...method and then add the available analysis timers to the timer overview so they can be started as necessary The timer overview always comprises the free timer and the selected analysis timers The Tim...

Страница 108: ...ght an analysis timer 5 If necessary remove the analysis timer from the list with Remove 6 Start the highlighted timer with Start The status of the timer is Active When the specified time interval has...

Страница 109: ...rement datasets STORE Csv files of these measuring modes cannot be reimported to the photometer Measurement datasets of these measuring modes can also be stored to a pdf file see Section 4 11 11 Spect...

Страница 110: ...the photometer for some time Check whether the stored data is complete e g on a PC Use the USB memory device for data transport but not for permanent data storage 4 11 3 Measurement datasets Elements...

Страница 111: ...ll new measurement values auto matically at the time of measurement AutoStore see Section 4 11 5 Storing with identifi cation ID When storing manually an input field for the identification ID appears...

Страница 112: ...asurement dataset is stored in the data memory only once Activating or deacti vating the AutoStore function Activate or deactivate the AutoStore function as follows 1 If necessary set the filter crite...

Страница 113: ...no checkmark 2 If required give the automatically stored measured values and ID with the menu item AutoStoreID 3 If the menu item Increment Auto StoreID is selected the ID of the automatically stored...

Страница 114: ...red measurement datasets refer to all stored measurement datasets that correspond to the specified fil ter criteria Filter criteria The following filter criteria can be set Concentration Absorbance Tr...

Страница 115: ...ith the Selected values invert selection function see Section 4 11 8 HOME Concentration Absorbance Transmission Special Multi wavelengths Setup Measurement data memory Setup Filter Filter Mode Concent...

Страница 116: ...ce Transmission Special Multi wavelengths Setup Measurement data memory Setup Selected values invert selection Measurement data memory 16 01 17 9 52 15 01 17 14 00 3 50 mg l Ni Administrator AutoStore...

Страница 117: ...17 14 15 3 72 mg l Ni Administrator AutoStore 15 01 17 14 20 3 72 mg l Ni Administrator AutoStore 15 01 17 14 25 3 75 mg l Ni Administrator AutoStore 15 01 17 14 30 3 73 mg l Ni Administrator AutoSto...

Страница 118: ...nted printer symbol on the display can also be saved as a pdf file The pdf file contains the data that are also output to a USB printer Kinetic recordings and spectra are stored in the pdf file as a g...

Страница 119: ...photometer Internal DataB folder to a connected USB memory device Please note the instructions for use of USB storage media see Section 4 11 2 When the data saving procedure is finished a message app...

Страница 120: ...ethods profiles with and remove the checkmark with START ENTER These methods profiles will not be saved 2 Start the save process with Store A message appears when the data have been saved 3 Confirm th...

Страница 121: ...osoft Excel Files containing measurement data can be copied to a PC in the following ways By using a USB memory device as a temporary storage see Section and Section 4 12 1 Subsequently you can connec...

Страница 122: ...IP address most frequent case 1 Select Yes for DHCP 2 Confirm the setting with Apply 3 Connect the cable for the Ethernet connection to the photometer and an Ethernet outlet 4 Wait for a moment then o...

Страница 123: ...otometer are dis played The FFSDISK folder contains the relevant photometer data in the following sub folders FFSDISK DataB General measurement values kinetics spectrum protocols FFSDISK UserMethods U...

Страница 124: ...y spectrum or kinetic recording by open ing an externally stored spectrum or kinetic recording with the Open function of the photometer 4 13 2 Importing methods profiles from a USB memory device When...

Страница 125: ...NTER These methods profiles are excluded from importing 2 Start the import with Import A confirmation prompt appears before any data on the photometer are overwritten A message appears when the data h...

Страница 126: ...sion to a printer or PC Decimal separators for CSV files For the output of CSV files you can select either a comma or a point as the decimal separator The setting is made in the following menu HOME Ge...

Страница 127: ...e blank value measure ment PCheck stamp PCheck protocol no MCheck stamp MCheck protocol no Absorbance Transmission mode Structure of the lines from left to right 1st line Sequential no Date Time Wavel...

Страница 128: ...D 7500 128 ba77191e01 71310060 04 2018 4 14 4 Printing spectra or Kinetics records If you output a spectrum or kinetic record to a USB printer or as a pdf file the current graphic display is shown on...

Страница 129: ...Check test protocol can be iden tified All measured values that are measured outside of the MCheck interval receive as addition the entry expired in the measured value documentation 4 15 2 Checking of...

Страница 130: ...unt the tolerances The steps are described in detail below PCheck Switching on You switch on the PCheckmonitoring on the Mode menu Specifying PCheck Interval The PCheck Interval defines the interval b...

Страница 131: ...e Interval defined for the PCheck check is active HOME DeviceCheck PCheck setup Interval PCheck setup 16 01 17 9 52 Mode Weeks Interval Lock instrument Configuration of tests Interval 2 Weeks 1 Select...

Страница 132: ...g with Switch on or Switch off 3 Confirm the test standard set once again 4 Switch to the adjustment of the nominal values and tolerances with Setup Example Verification Standard Kit XD 5 Using and se...

Страница 133: ...otometer is ready for the zero adjustment 4 Insert the zero cell The cell is automatically recog nized and the zero adjustment is started for all wavelengths After successful zero adjustment the photo...

Страница 134: ...surement if the check failed With successful measurement the display shows the measure ment of the next test standard from the Verification Standard Kit XD e g 430 LM 6 Measure all test standards in t...

Страница 135: ...of checking photome ter and methods The checking of photometer and method MCheck consists of the following parts Configuring the general settings in the MCheck setup menu Select MCheck interval unit...

Страница 136: ...MCheck settings Switching on MCheck monitoring for a method 1 Select and confirm Mode The Mode selection field pops up 2 Select and confirm Weeks or Mea surements For all methods the MCheckinter vals...

Страница 137: ...k setup 3 Select and confirm MCheck on MCheck is active for this method MCheck setup 16 01 17 9 52 Method 65 Ammonium LR TT MCheck MCheck on Interval 12 Weeks Citation form NH4 N Target value 2 00 mg...

Страница 138: ...pleted the result and its evalua tion are displayed If the check failed it is possible to repeat the measurement If the check was successful the MCheck function is finished MCheck check 16 01 17 9 52...

Страница 139: ...nalyte spiking the nominal value for the deter mination is calculated under the assumption that there are no disturbing influ ences in the sample matrix After the photometric determination the measure...

Страница 140: ...ssessment of the recovery rate is determined with the maximum deviation from the nominal value The assessment of the recovery rate is displayed next to the recovery rate after the check has been carri...

Страница 141: ...dard ID input field select the simplified SCheck for a pre parameterized ValidCheck standard solution or enter a desig nation for another standard solu tion used With selection of a ValidCheck no addi...

Страница 142: ...out the measurements Carrying out measurements According to the program the samples are measured top down You can however select the sam ples yourself and thus change the order with 11 Use Measuremen...

Страница 143: ...ce 13 If necessary repeat steps 11 and 12 for the second sample 14 Complete the SCheck with Com plete The Save dialog box pops up 15 If necessary change the storage location with Location Internal Dat...

Страница 144: ...2 2 71 Tintometer 0 14 Administrator SCheck OK Protocol ID 7 Method 130 CSB LR Sample concentration 45 mg l CSB Standard ID 48399612 Standard concentration200 mg lCSB Sample Standard Target valueActua...

Страница 145: ...r top level User user account registered by the administrator Guest user without user account Administrators and users log in to the photometer with their user name and password Guests can optionally...

Страница 146: ...tion You can also switch off the user management and reactivate it as necessary To do so you need administrator rights If the user management is switched off the user name and password do not have to...

Страница 147: ...ted by a user of the Adminis trator user group all user accounts that were set up are lost The password for the administrator is reset to admin The input field for the new user name pops up 1 Enter th...

Страница 148: ...sword pops up 4 If necessary enter A 9 and confirm another password The user account is changed and appears in the list of user accounts User management 16 01 17 9 52 Name User group Administrator Adm...

Страница 149: ...and password for the login After logging in to the Administrator group with a user name you can create further users or administrators or switch off the user management function The Login window with...

Страница 150: ...ssword for their user accounts themselves 2 Enter the password A 9 and confirm If the password is written correctly note upper and lower case the main menu Home opens up The user name that was entered...

Страница 151: ...asured blank val ues are deleted Delivery condition All settings including measurement data memory and user defined methods are deleted and the pho tometer is reset to the delivery con dition Internal...

Страница 152: ...he photometer counts the operating hours of the lamp The information on the operating hours of the lamp is given in the Info menu The meter information and result of the self test are displayed and ca...

Страница 153: ...the photometer Execution The Update folder must be on the top level of the USB memory device The If the user administration is activated only users of the user group Administrator may carry out any so...

Страница 154: ...the USB memory device to the photometer 4 Switch on the photometer if nec essary 5 Using select USB memory device as the source and press START ENTER The update process takes approx five minutes The p...

Страница 155: ...t ment center at the instrument s end of life The instruments are taken to one of those specialized treatment centers via the recycling system set up for this purpose If you leave the photometer switc...

Страница 156: ...follows If the housing surface is dirty wipe it with a soft cloth and mild soapy water Remove any chemicals splashes as soon as possible For disinfection you can use isopropanol for cleaning for a sho...

Страница 157: ...tor lens If the lens is often smudged error Wavelength calibration during the self test check whether the correct operating conditions are observed Follow the details in Section 3 2 for this purpose T...

Страница 158: ...en If after recommissioning an error occurs during the wavelength calibration the detector lens is probably smudged In this case clean the lens according to Section 5 2 3 CLEANING THE DETECTOR LENS 1...

Страница 159: ...ause Remedy Measuring range or method not suitable Select method with suitable mea suring range Dilute the sample In Concentration mode you can display the current absorbance value as an additional in...

Страница 160: ...just dilution Selected method not suitable Select different method Zero measurement incorrect Perform zero measurement Blank value incorrect Remeasure the blank value Cause Remedy Cell shaft cover ope...

Страница 161: ...fter the barcode is scanned no more suffix is transmitted via the USB interface see operating manual for the barcode reader Cause Remedy Printer not suitable Connect a printer that can inter pret the...

Страница 162: ...velength range 190 1100 nm Max scan speed approx 1000 nm min Wavelengths calibration Automatic Accuracy 1 nm Reproducibility 0 5 nm can be checked e g with Holmium oxide fil ter Resolution 1 nm Spectr...

Страница 163: ...h clear or serrated lateral surfaces are not reliably recognized by the automatic cell recognition Especially with plastic single use cells we recommend you test them for suitability prior to carrying...

Страница 164: ...tion by con stants addition of constants addition and subtraction of spectra for mation of the quotient of two spectra Kinetics Absorbance or transmission mode Minimal adjustable scan interval 1 s if...

Страница 165: ...tection for administrators and users Dimensions 422 x 195 x 323 mm width x height x depth Weight approx 4 5 kg without plug in power supply Housing type of protection IP 30 Electrical protec tive clas...

Страница 166: ...Tolerance extension 0 008 E FCC Class A Meter safety EC directive 2006 95 EC EN 61010 1 Climatic class VDI VDE 3540 IP protection class EN 60529 Communication interfaces Ethernet RJ45 USB 1 x USB A fo...

Страница 167: ...lish French Spanish Italian Bulgarian Czech Simplified Chinese Traditional Chinese Dansk Dutch Greek Indonesian Indonesia Japanese Korean Magyar Malay Melayu Macedonian Norsk Polski Portugu se Romania...

Страница 168: ...ll with lid 5 pcs 197629 Rectangular cell 10 mm 601040 Rectangular cell 20 mm 601050 Rectangular cell 50 mm 601070 Rectangular cell quartz 10 mm 661130 Rectangular cell quartz 20 mm 661140 Rectangular...

Страница 169: ...ification Standard Kit 215663 Secondary standard kit VIS with calibration certificate 711160 Secondary standard kit UV with calibration certificate 711161 Zero cell 16 mm 215661 Zero cell 24 mm 215662...

Страница 170: ...the measured value for a concentration The method for the determination of phosphate e g supplies a mea sured value for phosphorous P This measured value can alterna tively be given in the citation fo...

Страница 171: ...ue 20 mg l found 19 7 mg l refinding 0 985 or refinding rate 98 5 Reference absorbance With the reference absorbance the basic absorbance stored in the photometer can be replaced by a measurement of y...

Страница 172: ...Appendix XD 7500 172 ba77191e01 71310060 04 2018 9 2 List of trademarks Trademark Owner Microsoft Microsoft Corporation Excel Microsoft Corporation...

Страница 173: ...Keypad 12 Kinetics 95 M Measured value memory 111 112 113 Measurement dataset 110 Measuring diluted samples 46 Meter information 152 Method 83 Methods update 153 Multi wavelengths methods 76 O Operat...

Страница 174: ...174 ba77191e01 71310060 04 2018 USB memory device 21 User calibration 54 User defined methods Concentration 61 Multi wavelengths 76 Z Zero adjustment 36...

Страница 175: ......

Страница 176: ...a Room 1001 China Life Tower 16 Chaoyangmenwai Avenue Beijing 100020 Tel 86 10 85251111 App 330 Fax 86 10 85251001 China Tintometer South East Asia Unit B 3 12 BBT One Boulevard Lebuh Nilam 2 Bandar B...

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