Appendix A
Using the ModulyoD as a cold trap
Scope
By utilizing the pipeline adapter accessory, the ModulyoD may be used as a low temperature
vapor trap for a variety of devices. These include vacuum concentrators, rotary evaporators
and vacuum ovens.
CAUTION:
Do not attempt to connect vacuum devices directly to the isolation valve on
a column or drum manifold. Caustic vapors may damage the rubber portion
of the isolation valve and discolor or corrode the manifold.
CAUTION: The ModulyoD is suitable for use with most organic solvents. It is not
recommended for use with acids.
Installation
The pipeline adapter (Appendix B, item 12) is positioned directly over the stainless steel acces-
sory flange with the long end of the pipeline adapter extending down into the condenser cham-
ber. The rubber gasket surrounding the flange on the pipeline adapter forms the vacuum seal
with the accessory flange on the top of the ModulyoD. Once in position, vacuum tubing from
the desired device is connected to the pipeline adapter and secured with a hose clamp. The
vacuum hose connecting the ModulyoD to the vacuum source is connected in the manner
described in Section 3.4.
Operation
The ModulyoD must be pre-cooled to operate as a vapor trap. The fridge button must be
switched on and the temperature progress display must be in the green range. Switch on the
vacuum source and begin to monitor the vacuum progress display. This indicator should grad-
ually progress progress from a reading of ‘Hpr ’ to green as the vacuum pressure drops.
26
Thermo
Electron
freeze drying products (except glassware) are warranted against
defects in material and workmanship for one year after the date of delivery to the origi-
nal purchaser. Thermo
Electron
’s warranty is limited to defective materials and work-
manship, and does not cover incidental or consequential damages. Warranty work is
the responsibility of the distributor. The warranty obliges you to follow the precautions
in this manual. It is the responsibility of the user to dispose of ALL materials in a man-
ner in accordance with all federal, state and local regulations. ALL RETURNED UNITS
MUST BE DECONTAMINATED AND FREE OF RADIOACTIVITY. Under no circum-
stances shall Thermo
Electron
be liable for damages due to the improper handling or use
of its products. Thermo
Electron
assumes no liability, express or implied, for your use of
this equipment.
7.0
WARRANTY AND LIABILITY
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