SEM manual ETHZ v1.4
3
A.4) Overview of the JEOL console
The JEOL SEM has a
console
that is used to control the stage motion (X, Y), and the
electron imaging capabilities (magnification, brightness & contrast, etc.;
Fig. 3
):
•
The left side
of the console controls the stage motion.
Leave the “Stage” setting
to “X/Y”!
You can then use the joystick to move along the X and/or Y axis.
•
The top-right side
of the console “Scanning mode” has several options for the
different scanning rate. You will most likely use only
“Scan2”
(full-frame fast scan,
ideal for navigating in the sample) or
“Scan1”
during the alignment (fast scan over a
reduced area). Other scanning options (Scan3 or 4, Photo) are not recommended;
Thermo NSS (
Section H
) is used for acquiring and saving high-quality images.
•
The middle-right side
controls either the brightness and contrast (when STIG is
OFF) or the astigmatism correction (when STIG is ON). In any case, prefer the use
of the buttons atop of the electron image to adjust these parameters.
•
The bottom side
of the console has 2 similar knobs for magnification (left) and focus
(right).
Pay attention to which one you twist!
o
Left-one
is the
MAGNIFICATION knob
. It controls the field of view of the
electron image, from 20-40x to 300,000x.
o
Right-one
is the
ELECTRON BEAM FOCUS knob
. It controls the focus point
of the electron beam through the objective lens and defines the
working
distance (WD)
. Activate the “coarse” button for large changes in the focus
(e.g., rough focussing), and DE-activate this “coarse” button for fine tuning.
Figure 3. Overview of the SEM console.
Содержание JSM-6390 LA
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Страница 9: ...SEM manual ETHZ v1 4 5 Figure 5 Overview of the main buttons in the TOP section of the SEM program...
Страница 12: ...8 J M Allaz March 14 2021 Figure 9 Preparing the sample holder for thin section or for 1 round mount...
Страница 14: ...10 J M Allaz March 14 2021 Figure 10 Opening the sample chamber to remove or place a sample...
Страница 15: ...SEM manual ETHZ v1 4 11 Figure 11a Loading a new sample and taking an overview image of your sample SNS...
Страница 16: ...12 J M Allaz March 14 2021 Figure 11b Evacuating pumping the sample chamber after un loading a sample...
Страница 18: ...14 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Страница 23: ...SEM manual ETHZ v1 4 19 Figure 13 Complete procedure for beam alignment...
Страница 25: ...SEM manual ETHZ v1 4 21 Figure 15 Detail on the beam alignment procedure to obtain the best image quality...
Страница 30: ...26 J M Allaz March 14 2021 Figure 18 Creating a new NSS project or opening an existing one...
Страница 32: ...28 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Страница 34: ...30 J M Allaz March 14 2021 Figure 20 Electron Imaging mode acquire a single image in Thermo NSS...
Страница 36: ...32 J M Allaz March 14 2021 Figure 21 Electron Imaging mode acquire a mosaic image in Thermo NSS...
Страница 38: ...34 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Страница 41: ...SEM manual ETHZ v1 4 37 Figure 23 Loading standards into your project for quantitative EDS analysis...
Страница 43: ...SEM manual ETHZ v1 4 39 Figure 24 Spectrum Acquiring a single EDS spectrum over the currently scanned area...
Страница 45: ...SEM manual ETHZ v1 4 41 Figure 25 Point Shoot Acquiring multiple EDS analyses selected on an electron image...
Страница 48: ...44 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Страница 52: ...48 J M Allaz March 14 2021 Figure 27 Processing and extracting element maps...
Страница 53: ...SEM manual ETHZ v1 4 49 Figure 28 Calculating and extracting phase maps...
Страница 62: ...58 J M Allaz March 14 2021 A6 Thermo NSS toolbars from the NSS manual...