SEM manual ETHZ v1.4
51
Appendix
A1) Adjusting the SNS (Sample Navigation System)
The SNS image is not very accurate, yet it should drive the stage within a couple millimetres of the target. The
calibration of this system is regularly checked by the manager. However, if you want to check and possibly
adjust it (because someone screwed it up…), please,
strictly
follow this procedure:
•
You MUST load the 32 mm sample holder
(for round mount)
. NEVER use the THIN SECTION
holder
, as it will result in a wrong calibration of the SNS!
•
Ensure the
sample chamber is fully opened
, up to the back stop.
•
You MUST first press the button “Snap”
before “Adjust”!
It will move the stage and take a snapshot.
•
An adjustment is only required if the sample is not centred
(yellow line NOT in the middle of the
stage holder). To perform the adjustment (see also
Fig. A1
):
o
Press the button “Adjust”. Ensure the Holder Size “32 mm” is selected.
o
Adjust the X and Y position of the stage using the button on the console (in X/Y mode) and
recentre the holder (yellow line is in the exact middle of the 32 mm holder.
o
Move the horizontal and vertical green lines so that it matches the edges of the round mount.
o
Try rotating the sample using the rotation knob. If the adjustment is properly done, the sample
should remain in the centre and the green lines should always touch the round mount edges.
o
Press “Set” when the holder is perfectly centred.
•
Press again “Snap” to take another picture with the new adjustment, and then “OFF” to turn off SNS.
•
Lower again the stage to Z = 30 mm
before closing the chamber!
Figure A1.
Adjusting the Sample Navigation System (SNS).
Содержание JSM-6390 LA
Страница 2: ......
Страница 9: ...SEM manual ETHZ v1 4 5 Figure 5 Overview of the main buttons in the TOP section of the SEM program...
Страница 12: ...8 J M Allaz March 14 2021 Figure 9 Preparing the sample holder for thin section or for 1 round mount...
Страница 14: ...10 J M Allaz March 14 2021 Figure 10 Opening the sample chamber to remove or place a sample...
Страница 15: ...SEM manual ETHZ v1 4 11 Figure 11a Loading a new sample and taking an overview image of your sample SNS...
Страница 16: ...12 J M Allaz March 14 2021 Figure 11b Evacuating pumping the sample chamber after un loading a sample...
Страница 18: ...14 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Страница 23: ...SEM manual ETHZ v1 4 19 Figure 13 Complete procedure for beam alignment...
Страница 25: ...SEM manual ETHZ v1 4 21 Figure 15 Detail on the beam alignment procedure to obtain the best image quality...
Страница 30: ...26 J M Allaz March 14 2021 Figure 18 Creating a new NSS project or opening an existing one...
Страница 32: ...28 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Страница 34: ...30 J M Allaz March 14 2021 Figure 20 Electron Imaging mode acquire a single image in Thermo NSS...
Страница 36: ...32 J M Allaz March 14 2021 Figure 21 Electron Imaging mode acquire a mosaic image in Thermo NSS...
Страница 38: ...34 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Страница 41: ...SEM manual ETHZ v1 4 37 Figure 23 Loading standards into your project for quantitative EDS analysis...
Страница 43: ...SEM manual ETHZ v1 4 39 Figure 24 Spectrum Acquiring a single EDS spectrum over the currently scanned area...
Страница 45: ...SEM manual ETHZ v1 4 41 Figure 25 Point Shoot Acquiring multiple EDS analyses selected on an electron image...
Страница 48: ...44 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Страница 52: ...48 J M Allaz March 14 2021 Figure 27 Processing and extracting element maps...
Страница 53: ...SEM manual ETHZ v1 4 49 Figure 28 Calculating and extracting phase maps...
Страница 62: ...58 J M Allaz March 14 2021 A6 Thermo NSS toolbars from the NSS manual...