Varian 4000 GCMS, Installation Procedures Manual

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Appendix A. 4000 MS Installation
Specifications and Test Samples
Ionization Mode Test Sample Amount of
Analyte
Measured m/z RMS S/N
Specification
Library
Match (any
search
type)
Internal EI 10:1 split or dilution of
03-931126-01 (2 pg/µL
OFN, 5 pg/µL BZP) 200 fg OFN 272 ≥ 20:1 ≥ 500
Internal CI 03-931126-01 (2 pg/µL
OFN, 5 pg/uL BZP) 5 pg BZP 183 ≥ 50:1 N/A
Internal EI with a
Quick Switch Valve
in the GC 10:1 split or dilution of
03-931126-01 (2 pg/µL
OFN, 5 pg/uL BZP) 200 fg OFN 272 ≥ 10:1 ≥ 500
External EI 10:1 split or dilution of
03-931127-02 (5 pg/µL
OFN) 500 fg OFN 272 ≥ 30:1 ≥ 500
External PCI 03-920305-00
(50 pg/µL BZP) 50 pg BZP 183 ≥ 20:1 N/A
External NCI 03-931130-01 (1 pg/µL
DFB) 1 pg DFB 362 ≥ 50:1 N/A
External EI with a
Quick Switch Valve
in the GC 10:1 split or dilution of
03-931127-02 (5 pg/µL
OFN) 500 fg OFN 272 ≥ 15:1 ≥ 500