TA Instruments DSC Autosampler CE, Operator'S Manual

Page: 86 / 190

Calibrating the Autosampler CE
4–18 TA I
NSTRUMENTS
DSC A
UTOSAMPLER
CE
16. When the turret stops moving, close and
open the grippers again and check your
calibration against the criteria in Figure 4.2.
Remember to release the pan. If the position
is correctly calibrated, go on to step 17. If it
is not, repeat steps 4 through 16.
17. Press the
LOAD
key. The screen displays:
Load (1) or
Unload (2) ? 1
18. Select option 1 (Load) by pressing
ENTER
.
The screen displays:
Load Ref (1) or
Sample (2) ? 1
19. Select option 2 (Sample) by pressing 2 then
ENTER
. The screen displays:
Sample Pan
Number ? 1
20. Select tray position 2 (press the 2 key then
press
ENTER
). The Autosampler CE picks
up the pan in tray position 2 and begins
moving toward the cell.
21. Press
ESCAPE/CLEAR
when the Au-
tosampler CE reaches the DSC cell area.
22. Use the motion keys to position the pan in its
correct calibration position (see Table 4.1).
Press the
RELEASE
and
GRIP
keys repeat-
edly to ensure that the fingers can firmly
grasp the pan, and watch carefully
to ensure that each finger contacts the pan
at the same time (see Figure 4.2).