Shimadzu ICPE-9000, Instruction Manual

Page: 23 / 116

xxi
7.1.3 Stopping the ICPE-9000 in Daily Use ....................................................... 7-3
7.1.4 Leak Valve Operation (After vacuum pump is stopped) ............................ 7-4
7.2 C
H E C K I N G
O
P E R AT I O N O F
S
AF E T Y
D
E V I C E S
................................................. 7-5
7.3 R
E S P O N S E I N
E
M E R G E N C Y
........................................................................ 7-5
7.3.1 Recovery after Emergency Stop ............................................................... 7-5
7.3.2 Response to Power Failure ...................................................................... 7-5
8. M
AI N T E N AN C E
............................................................................................. 8-1
8.1 R
E P L AC I N G AN D
I
N S P E C T I N G
G
L AS S W AR E
................................................... 8-1
8.1.1 Replacing the Torch ............................................................................... 8-1
8.1.2 Nebulizer ............................................................................................... 8-2
8.1.3 Replacing the Chamber ........................................................................... 8-2
8.1.4 Cleaning Glassware ................................................................................ 8-2
8.2 R
E M O V I N G
G
L AS S
P
AR T S
......................................................................... 8-3
8.2.1 Removing the Chamber and Extension Pipe ............................................. 8-4
8.2.2 Removing the Nebulizer .......................................................................... 8-4
8.2.3 Removing the Leveler ............................................................................. 8-5
8.2.4 Removing the Torch ................................................................................ 8-6
8.3 A
T T AC H I N G T H E
G
L AS S W AR E
.................................................................... 8-7
8.3.1 Attaching the Torch ................................................................................ 8-7
8.3.2 Attaching the Leveler ........................................................................... 8-10
8.3.3 Attaching the Nebulizer ........................................................................ 8-11
8.3.4 Attaching the Nebulizer to the Chamber ................................................ 8-11
8.3.5 Attaching the Chamber ......................................................................... 8-12
8.4 R
E P L AC I N G T H E
S
AM P L E
I
N T R O D U C T I O N
T
U B E
............................................. 8-13
8.5 R
E P L AC I N G T H E
D
R AI N
T
U B E
................................................................... 8-13
8.6 R
E P L AC I N G T H E
L
E V E L E R
E
X H AU S T
T
U B E
................................................... 8-15
8.7 C
L E AN I N G AN D
R
E P L AC E M E N T O F
R
E F L E C T
M
I R R O R I N
C
O O L I N G
J
AC K E T
......... 8-16
8.8 C
L E AN I N G T H E
A
X I AL
-V
I E W
O
B S E R V AT I O N
O
R I F I C E
A
S S E M B L Y
L .................... 8-18
8.9 A
T T AC H I N G AN D
R
E M O V I N G T H E
C
O O L I N G
J
AC K E T
....................................... 8-19
8.10 C
L E AN I N G T H E
E
N T R AN C E
W
I N D O W
......................................................... 8-22
8.11 C
L E AN I N G T H E
R
AD I AL
-V
I E W
O
B S E R V AT I O N
(O
P T I O N
) E
N T R AN C E
W
I N D O W
..... 8-22
8.12 R
E P L AC I N G T H E
M
O L E C U L AR
S
I E V E
(O
I L
A
B S O R B E N T
)
I N T H E
V
AC U U M
P
U M P
.. 8-24
8.13 R
E P L AC I N G T H E
V
AC U U M
P
U M P
O
I L
......................................................... 8-25
8.14 W
AS T E
T
AN K
...................................................................................... 8-26
8.15 C
L E AN I N G T H E
F
AN
F
I L T E R S
.................................................................. 8-26
8.15.1 Cleaning the Side Filter ...................................................................... 8-26
8.15.2 Cleaning the Bottom Filter .................................................................. 8-28
8.16 C
H E C K I N G
O
P E R AT I O N O F
S
AF E T Y
D
E V I C E S
.............................................. 8-29