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Chapter 7: Purging the System
Glove-Box systems either newly installed or opened for reasons of service contain ambient air. For building up
an absolutely pure gas atmosphere within the box
,
a nitrogen, argon or helium atmosphere of medium purity is
the prerequisite for the gas purification. Thus, prior to the system’s commissioning
,
the ambient air should be
replaced by nitrogen, argon or helium.
Displacing the ambient air from the system is called purging. Working gas is used as purging gas.
On
average
, a system should be purged when the O2 portion in the box atmosphere exceeds 250 ppm.
The reasons for
excessive
oxygen values are as follows:
- first commissioning of a system
- servicing
- air influx due to faulty operation
- air influx due to damage (leaks)
Caution!
A Glove-Box system should be purged using working gas until the O
2
portion within the box
atmosphere has decreased to a value of <100 ppm. Operating the system with higher oxygen
value
s
may result in damaging the gas purification system.
Working gas is used for purging the system;
Nitrogen, argon or helium - medium purity - from bottles or any gas supply facilities.
Example
of
the purge gas consumption of a
n
MBRAUN System
!
General information
Chapter 7
Purging the System
When is purging necessary?
Purge gas
0.00
0.00
0.50
1.00
1.50
c = 1 vpm
c = 10 vpm
c = 100 vpm
c = 500 vpm
c = 1000 vpm
5.00
10.00
15.00
20.00
25.00
Purge gas consumption [cbm
]
Boxvolume [cbm]
30.00
gc = f (v,c)
35
Summary of Contents for MB 120B-G
Page 6: ...OPERATING INSTRUCTIONS Chapter 1 General Information MBRAUN 1...
Page 10: ...OPERATING INSTRUCTIONS Chapter 2 Transport Site Selection Modification MBRAUN 2...
Page 13: ......
Page 14: ...OPERATING INSTRUCTIONS Chapter 3 Preparing the Connections MBRAUN 3...
Page 20: ...OPERATING INSTRUCTIONS Chapter 4 Installation MBRAUN 4...
Page 24: ...OPERATING INSTRUCTIONS Chapter 5 Activating and Deactivating the System MBRAUN 5...
Page 28: ...OPERATING INSTRUCTIONS Chapter 6 OP 17 Operation Panel MBRAUN 6...
Page 32: ...OPERATING INSTRUCTIONS Chapter 7 Purging the System MBRAUN 7...
Page 36: ...OPERATING INSTRUCTIONS Chapter 8 Pressure Control System MBRAUN 8...
Page 40: ...OPERATING INSTRUCTIONS Chapter 9 Circulation Mode MBRAUN 9...
Page 45: ......
Page 46: ...OPERATING INSTRUCTIONS Chapter 10 Regeneration MBRAUN 10...
Page 51: ......
Page 52: ...OPERATING INSTRUCTIONS Chapter 11 Settings and Display Patterns MBRAUN 11...
Page 59: ......
Page 60: ...OPERATING INSTRUCTIONS Chapter 12 Antechamber Operation MBRAUN 12...
Page 73: ......
Page 74: ...OPERATING INSTRUCTIONS Chapter 13 Dust Filters MBRAUN 13...
Page 77: ......
Page 78: ...OPERATING INSTRUCTIONS Chapter 14 Analyzers MBRAUN 14...
Page 90: ...OPERATING INSTRUCTIONS Chapter 15 Maintenance and Service MBRAUN 15...
Page 94: ...OPERATING INSTRUCTIONS Chapter 16 Spare Parts List MBRAUN 16...
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Page 105: ......