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SEM manual ETHZ v1.4
7
B) Starting your session
1.
Check if a notice with special instructions is on the table
(e.g., in case of an
outage, a problem with a detector, etc.).
2. Turn ON both computer screens.
3. Ensure that nothing is currently running (e.g., overnight EDS element map work). If
an analysis is still running
(e.g., mosaic BSE or EDS mapping on the right computer)
, contact the former
user, and see if you can wait for the completion or if you can cancel the analysis.
4. Turn ON the infrared camera (“Deben”, small screen on the left;
Fig. 8
).
Figure 8.
Main SEM detectors and components visible on the Deben infrared camera.
5. If a sample is currently loaded in the SEM, you will need to remove it (
Section C
).
6. Prepare your sample (
Fig. 9
): choose the thin-section or the 1-inch round mount.
WARNING!
If your sample does not fit the thin section or the 1’’ round holder, you MUST
contact the lab manager or the assistant before continuing!
7. Proceed to the sample loading (see
Section C
).
Summary of Contents for JSM-6390 LA
Page 2: ......
Page 14: ...10 J M Allaz March 14 2021 Figure 10 Opening the sample chamber to remove or place a sample...
Page 18: ...14 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Page 23: ...SEM manual ETHZ v1 4 19 Figure 13 Complete procedure for beam alignment...
Page 30: ...26 J M Allaz March 14 2021 Figure 18 Creating a new NSS project or opening an existing one...
Page 32: ...28 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Page 38: ...34 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Page 48: ...44 J M Allaz March 14 2021 Page left blank intentionally a good place for your notes J...
Page 52: ...48 J M Allaz March 14 2021 Figure 27 Processing and extracting element maps...
Page 53: ...SEM manual ETHZ v1 4 49 Figure 28 Calculating and extracting phase maps...
Page 62: ...58 J M Allaz March 14 2021 A6 Thermo NSS toolbars from the NSS manual...