FTS LYOSTAR 3, Operator'S Manual

Page: 73 / 82

Rev 006, 01/14 63
© SP Scientific 2014
Appendix
A
Appendix A: Sample Recipe
The sample recipe is provided as a general reference only. The format is based on
the Recipe screen of the LyoS™ control system.
The following recipe parameters are intended for use with one (1) liter of water. Before
you begin, fill one bulk-processing tray with water, place it on one of the product
shelves in the chamber and close the door. Enter the following recipe parameters and
run a freeze dry cycle.
Freezing / Thermal Treatment
Step 1 2 3 4 5 6 7 8 9 10 11 12
✓ ✓
X X X X X X X X X X
Temp 20 -20 0 0 0 0 0 0 0 0 0 0 °C
Ramp 0 80 0 0 0 0 0 0 0 0 0 0 min
Hold 10 30 0 0 0 0 0 0 0 0 0 0 min
Control with CM ✓
Guaranteed Soak X
Product Driven Mode
X
Product Temperature
20 °C
Shelf Load
X
Extra Freeze
Product Temp SP -40 °C Hold Time 60 min Condenser SP -45 °C Initial Vacuum SP 100 mTorr
Drying Phase
Step 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17
✓ ✓ ✓ ✓ ✓ ✓
X X X X X X X X X X
✓
Temp -40 0 10 20 40 0 0 0 0 0 0 0 0 0 0 0 25 °C
Ramp 0 80 20 0 0 0 0 0 0 0 0 0 0 0 0 0 0 min
Hold 60 120 240 600 360 0 0 0 0 0 0 0 0 0 0 0 30 min
Vacuum 0 0 100 200 0 0 0 0 0 0 0 0 0 0 0 0 0 mTorr
V.Ramp 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 min
PRISE 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 mTorr
PVG/C
M
0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 mTorr
Product Storage Backfill/Stoppering
Product Temp SP 50 °C Backfill X PVG/CM Diff. X
Vacuum SP 0 mTorr Stoppering X Pressure Rise X Retest Time 2 min
End Cycle Control Action X Closure Time 20 sec