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Operation

Automatic Boat Drive

18

Figure 7 Quartz boat with the carrier material inserted

NOTICE

Only use a single undamaged piece of quartz fleece as carrier material! When using sev-
eral small or damaged pieces, correct functionality cannot be ensured.

5.3

Manual sampling

Solid sample

Prerequisite: System components have been switched on, the multiWin control and
analysis software is running, an appropriate method has been selected.

}

Fill a quartz boat with carrier material 
(→ "Preparing the quartz boat for the analysis" 

 17).

NOTICE

Temper both components or use tempered components. 
As an exception, AOX and EC/OC measurements do not require carrier material.

}

Weigh the solid sample into a quartz boat.

}

When prompted by the software to do so, use tweezers to insert the quartz boat into
the open sample sluice, making sure that the eye is placed onto the hook.

}

Click on [OK] to confirm that the quartz boat has been inserted.

ü

The sample sluice closes. After a rinsing time has elapsed, which can be config-
ured in a method, the quartz boat is transported into the combustion tube ac-
cording to the parameters specified in the method.

Liquid sample

Prerequisite: System components have been switched on, the multiWin control and
analysis software is running, an appropriate method has been selected.

}

Fill a quartz boat with carrier material 
(→ "Preparing the quartz boat for the analysis" 

 17).

NOTICE

Temper both components or use tempered components.
If no quartz fleece is used, uncontrolled spontaneous evaporation of the complete sam-
ple or splashing of the sample may occur. In the worst case, the system is contaminated!

Summary of Contents for 450-126.416

Page 1: ...Operating Manual Automatic Boat Drive...

Page 2: ...se Stra e 1 07745 Jena Germany Phone 49 3641 77 7407 Fax 49 3641 77 9279 Email service analytik jena com General Information http www analytik jena com Documentation Number 11 889 687 Edition B 01 202...

Page 3: ...sluice with flap and injection port 12 3 1 5 ABD connection piece 12 3 1 6 Control elements 13 3 1 7 Type plate 14 3 2 Principle of operation 14 4 First commissioning 15 4 1 Location requirements 15...

Page 4: ...of the ABD 29 7 6 Cleaning the ABD connection piece 29 7 7 Cleaning and replacing the hook at the ABD 30 7 8 Cleaning or replacing the guide tube 31 8 Transport and storage 33 8 1 Transport 33 8 1 1 P...

Page 5: ...of the equipment and potential causes and reme dies of any faults Conventions Instructions for actions which occur in chronological order are numbered and combined in action units Warnings are indica...

Page 6: ...the sample sluice it is also possible to introduce gaseous samples The ABD can only be used in conjunction with the multi EA 5000 multi EA 5100 or the multi X 2500 The modules are controlled by the mu...

Page 7: ...arkings The warning labels and safety symbols attached to the device are an integral part of the device and must be strictly observed CAUTION Danger of incorrect actions leading to personal injury and...

Page 8: ...nnect the ABD to a properly grounded mains outlet in accordance with the voltage specifications on the type plate Observe in particular the notes in the Elec trical safety notes chapters of the user m...

Page 9: ...nance and repair The device is generally maintained by the customer service department of Analytik Jena or specialist personnel trained and authorized by them Unauthorized maintenance can damage the d...

Page 10: ...r The boats can accept liquid or solid substances The ABD can also be used for the analysis of gas or liquid gas samples refer to the user manuals of the gas samplers The ABD consists of the following...

Page 11: ...pler interface and the con nection for the connection cable of the flame sensor are in the center at the rear of the device 1 2 3 4 5 6 7 Figure 2 Rear of the device 1 Equipotential bonding connection...

Page 12: ...s boat is not required In addition for liquids in the sample sluice the used quartz glass boats are cooled to room temperature after combustion cooling time at least 200 s to prepare them for the next...

Page 13: ...ntrol elements The two buttons on the device cover have the following functions port button Actuating the button opens or closes the sample sluice Note The button is locked during measurements stop bu...

Page 14: ...d according to the parameters chosen in multiWin without flame sensor control The following parameters can be configured Hold points max 3 Waiting times max 3 Feed speeds before and between hold point...

Page 15: ...vice is prevented Pushing or moving the device can cause the ABD connection piece or the combustion tube to break Never cover the air vents of the ABD with other equipment or installations Keep a saf...

Page 16: ...can endanger the user and the operational safety of the equipment and limits or completely invalidates any warranty claims NOTICE Retain the transport packaging Return transport for maintenance must...

Page 17: ...s and the quartz fiber material prior to first use to avoid prob lems with blank values Only touch the tempered boats with gloves Keep the boats free from contamination in the exsiccator or in a screw...

Page 18: ...en prompted by the software to do so use tweezers to insert the quartz boat into the open sample sluice making sure that the eye is placed onto the hook Click on OK to confirm that the quartz boat has...

Page 19: ...to the metering head refer to the user manual of the sampler Adjust the sampler Fill a quartz boat with carrier material Preparing the quartz boat for the analysis 17 NOTICE Temper both components or...

Page 20: ...lashing of the sample may occur In the worst case the system is contaminated Open the sample sluice by pressing the port button Using tweezers insert the quartz boat into the open sample sluice making...

Page 21: ...he cor respond files to the service department via email for fault diagnosis address on inside of the front cover NOTICE For information on error messages and status displays of the control and analys...

Page 22: ...luice if necessary loosen the clamping ring correct the position and firmly re tighten the clamping ring Screw connection be tween ABD connection piece and combustion tube leaking Check screw connecti...

Page 23: ...th sample Remove sample material from the sample sluice wipe out the sluice lid and injection port with al cohol and allow them to dry ABD connection piece contaminated Clean the ABD connection piece...

Page 24: ...kage hardening change in shape or transparency analytic problems blank value Table 3 Maintenance overview NOTICE When performing maintenance or care work always wear appropriate protective gloves In p...

Page 25: ...tighten the PEEK clamping rings at the sample sluice 7 3 1 Installing the ABD at the combustion tube NOTICE During all work on the combustion tube or the ABD connection piece the pneumatic seal must...

Page 26: ...ustion furnace into the horizontal position and insert the combustion tube in the furnace Carefully move the ABD towards the basic module until the ABD connec tion piece and the combustion tube almost...

Page 27: ...e of the ABD has been mounted 7 3 2 Disconnecting the ABD from the combustion tube NOTICE During all work on the combustion tube or the ABD connection piece the pneumatic seal must be depressurized Ot...

Page 28: ...forces occur when closing the sample sluice of the ABD Do not reach into the sluice area during closing Replace septum If necessary replace the septum at the injection port of the sample sluice as fol...

Page 29: ...ple sluice Re install the ABD at the basic module Installing disconnecting the ABD at the combustion tube 25 The sealing ring in the sample sluice has been replaced 7 6 Cleaning the ABD connection pie...

Page 30: ...nection cables on the rear of the ABD flame sensor sampler cable These could easily tear off Remove the protective cover from the guide tube Push the magnetic coupling with hook carefully up to the st...

Page 31: ...tube see user manual Multi Matrix Sampler If the guide tube needs cleaning or replacing proceed as follows Switch the ABD off from the equipment switch Disconnect the ABD from the basic module Disconn...

Page 32: ...k without jamming Push the magnetic coupling into the guide tube The short piece of the magnetic coupling in front of the metal ring must face the block of the gas supply Attach the guide tube in reve...

Page 33: ...cessary remove the sampler from the ABD and prepare it separately for trans port refer to the user manual of the sampler Disconnect the ABD from the basic module Disconnecting the ABD from the combust...

Page 34: ...arately in the lab see user manual of the sampler Disconnect the ABD from the furnace of the basic module Disconnecting the ABD from the combustion tube 27 Securely hold the device with both hands fro...

Page 35: ...ing make sure that the equipment switches at the equipment backplates of the ABD and the analyzers are in the 0 position Only use the mains cable included in the scope of delivery for the connection t...

Page 36: ...ial interface cable to the analyzer RS 232 sampler interface at the rear of the ABD 1 Interface Sampler at the rear of the analyzer 2 or via another sampler module If the optional flame sensor is used...

Page 37: ...e on the ABD Connection out ABD at the rear of the analyzer 2 The ABD is now connected to the analyzer If required install the sampler to the ABD refer to the user manual of the sampler Install the AB...

Page 38: ...e ground The ap plicable regulations for disposal must be meticulously observed Dispose of materials used during sampling carrier material quartz boats septums in accordance with the legal and local r...

Page 39: ...boat with fully automated control of the combustion via evaluation of the flame sensor Automatic plus Supply of the sample in the quartz glass boat with time optimized combustion fully automated cont...

Page 40: ...ns and noise immunity It meets the requirements for transient emissions according to EN 61326 1 EN 55011 group 1 class B The device meets the requirements for noise immunity according to EN 61326 1 re...

Page 41: ...stances subject to regulation according to the directive GB T 26572 2011 Analytik Jena guarantees that if the device is used as intended these substances will not leak within the next 25 years and the...

Page 42: ...ure 1 ABD main components 10 Figure 2 Rear of the device 11 Figure 3 LED displays 12 Figure 4 Sample sluice injection port 12 Figure 5 ABD connection pieces 13 Figure 6 Control elements push buttons 1...

Page 43: ...Drive Index 43 Index C Clamping ring 25 D Devitrification 24 G guide rail 10 guide tube 10 H hook 10 I injection port 10 L LED displays 10 P protective cover 8 10 S Safety symbol 7 sample sluice 10 W...

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