Bruker Anton Paar, User Manual

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List of Figures
DOC-M88-EXX268_V1_12.2016 9
Figure 8.10: Z-scan at 25 °C over a wide range to determine roughly the height position .......... 82
Figure 8.11: Z-scan at 25 °C with determination of height position ............................................. 83
Figure 8.12: Rocking-curve scan at 25 °C with determination of rotation error ........................... 84
Figure 8.13: Inserting the temperature depending Z-positions and activating them .................... 86
Figure 8.14: Rocking curve to align the angle theta (or omega in HR mode) between source
and sample ..............................................................................................................
87
Figure 8.15: TwoTheta scan to align the Bragg angle ................................................................. 88
Figure 8.16: Psi scan to align the diffracting plane normal in the diffraction plane ...................... 89
Figure 8.17: Transmit drive positions from COMMANDER to WIZARD ...................................... 90
Figure 8.18: Create an HR-XRD measurement for your sample ................................................. 90
Figure 8.19: Selecting the aligned sample reflection ................................................................... 91
Figure 8.20: Import the centered values from COMMANDER ..................................................... 91
Figure 8.21: Defining a sequence of measurements ................................................................... 92
Figure 8.22: Setting the drives for alignment for the each temperature....................................... 93
Figure 8.23: Create a job using the MeasureAlign.cs script ........................................................ 94
Figure 9.1: Fixing screws for the BTS 150/500 adapter............................................................. 96
Figure 9.2: USB connection of the BTS 150/500 to the CPU1 board in the USB1 slot ............. 97
Figure 10.1: Import template from file ......................................................................................... 101
Figure 10.2: Select template ........................................................................................................ 102
Figure 10.3: Import sections ........................................................................................................ 102
Figure 10.4: Section for HTK1200N in Goniometer/Center/PAAR_Z_HTK1200 ......................... 103
Figure 10.5: Section HTK1200N in Goniometer/Center/PAAR_Z_HTK1200/HTK1200 .............. 104
Figure 10.6: Section for NonAmbient Controller .......................................................................... 104
Figure 10.7: Subsection TCU1000_Controller for NonAmbient Controller .................................. 105
Figure 10.8: Setting a new temperature and heating rate with COMMANDER ........................... 106
Figure 10.9: Selecting SerialLine/Power X1_RS232_I/-II for SerialConnector ............................ 106
Figure 10.10: Selecting SerialLine/Full X2_RS232_I/-II for SerialConnector................................. 107
Figure 10.11: Import Section Stage_PAAR_CHCplus_LN2Cooling.bfscn..................................... 108